Invention Grant
- Patent Title: Magneto-carbonization method for production of carbon fiber, and high performance carbon fibers made thereby
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Application No.: US13833834Application Date: 2013-03-15
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Publication No.: US09725829B2Publication Date: 2017-08-08
- Inventor: Amit K. Naskar , Soydan Ozcan , Claude C. Eberle , Mohamed Gabr Abdallah , Gail Mackiewicz Ludtka , Gerard Michael Ludtka , Felix Leonard Paulauskas , John Daniel Kennedy Rivard
- Applicant: UT-Battelle, LLC
- Applicant Address: US TN Oak Ridge
- Assignee: UT-BATTELLE, LLC
- Current Assignee: UT-BATTELLE, LLC
- Current Assignee Address: US TN Oak Ridge
- Agency: Scully Scott Murphy & Presser
- Main IPC: D01F9/12
- IPC: D01F9/12 ; D01F9/22 ; D01F9/14 ; C01B31/02 ; D01F9/145 ; D01F9/127 ; B29C47/00

Abstract:
Method for the preparation of carbon fiber from fiber precursor, wherein the fiber precursor is subjected to a magnetic field of at least 3 Tesla during a carbonization process. The carbonization process is generally conducted at a temperature of at least 400° C. and less than 2200° C., wherein, in particular embodiments, the carbonization process includes a low temperature carbonization step conducted at a temperature of at least or above 400° C. or 500° C. and less than or up to 1000° C., 1100° C., or 1200° C., followed by a high temperature carbonization step conducted at a temperature of at least or above 1200° C. In particular embodiments, particularly in the case of a polyacrylonitrile (PAN) fiber precursor, the resulting carbon fiber may possess a minimum tensile strength of at least 600 ksi, a tensile modulus of at least 30 Msi, and an ultimate elongation of at least 1.5%.
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