• Patent Title: Method for manufacturing heat-ray shielding fine particle-containing composition and heat-ray shielding fine particle-containing composition, a heat-ray shielding film using the heat-ray shielding fine particle-containing composition and a heat-ray shielding laminated transparent base material using the heat-ray shielding film
  • Application No.: US14009873
    Application Date: 2012-04-12
  • Publication No.: US09726796B2
    Publication Date: 2017-08-08
  • Inventor: Kenichi FujitaHiroshi Kobayashi
  • Applicant: Kenichi FujitaHiroshi Kobayashi
  • Applicant Address: JP Tokyo
  • Assignee: SUMITOMO METAL MINING CO., LTD.
  • Current Assignee: SUMITOMO METAL MINING CO., LTD.
  • Current Assignee Address: JP Tokyo
  • Agency: Oliff PLC
  • Priority: JP2011-090514 20110414; JP2011-119470 20110527
  • International Application: PCT/JP2012/002548 WO 20120412
  • International Announcement: WO2012/140896 WO 20121018
  • Main IPC: G02B5/20
  • IPC: G02B5/20 B82Y30/00 C09C1/00
Method for manufacturing heat-ray shielding fine particle-containing composition and heat-ray shielding fine particle-containing composition, a heat-ray shielding film using the heat-ray shielding fine particle-containing composition and a heat-ray shielding laminated transparent base material using the heat-ray shielding film
Abstract:
To provide a heat-ray shielding film and a method for manufacturing the same, capable of exhibiting excellent optical characteristics and high weather resistance, mainly composed of polyvinyl acetal resin and using composite tungsten oxide fine particles with high heat-ray shielding effect, the method comprising: a first step of obtaining a dispersion liquid by dispersing composite tungsten oxide fine particles expressed by a general formula MyWOz and having a hexagonal crystal structure, and dispersing a dispersant into an organic solvent with a boiling point of 120 deg C. or less; a second step of obtaining a mixture by mixing metal carboxylate into the dispersion liquid obtained by the first step; and a third step of drying the mixture obtained by the second step to thereby obtain a heat-ray shielding fine particle-containing composition, and setting a content of the organic solvent remained in the heat-ray shielding fine particle-containing composition to 5 mass % or less.
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