Invention Grant
- Patent Title: Method for removing impurities from dinitrotoluenes
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Application No.: US15323800Application Date: 2015-04-30
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Publication No.: US09738592B2Publication Date: 2017-08-22
- Inventor: Jürgen Pöhlmann , Heinrich Hermann , Mirko Händel , Jürgen Gebauer , Tim Bergmann
- Applicant: Josef Meissner GmbH & Co. KG
- Applicant Address: DE Köln
- Assignee: Josef Meissner GmbH & Co. KG
- Current Assignee: Josef Meissner GmbH & Co. KG
- Current Assignee Address: DE Köln
- Agency: Brannon Sowers & Cracraft PC
- Agent Edward E. Sowers
- Priority: DE102014009948 20140707; DE102015003743 20150325; DE102015004242 20150407
- International Application: PCT/EP2015/059493 WO 20150430
- International Announcement: WO2016/005070 WO 20160114
- Main IPC: C07C201/16
- IPC: C07C201/16 ; B01D11/04 ; B01D19/00 ; B01J19/24 ; C07C205/06

Abstract:
The present invention relates to a method for purifying raw dinitrotoluenes resulting from dinitration of toluene in the presence of a nitric acid/sulfuric acid/nitrating acid mixture, and a device or plant for performing the method, and a corresponding production plant for producing dinitrotoluene, characterized in that (a) the raw dinitrotoluenes are first subjected to a wash with at least one washing medium after separation of the nitrating acid mixture, followed by a separation of the washing medium; and that (b) subsequently the washed dinitrotoluenes resulting from method step (a) are subjected to stripping (stripping gas treatment) with at least one gas (stripping gas).
Public/Granted literature
- US20170166514A1 METHOD FOR REMOVING IMPURITIES FROM DINITROTOLUENES Public/Granted day:2017-06-15
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