Invention Application
WO1997038058A1 PROCESS FOR PREPARING AGGLOMERATE-FREE NANOSCALAR IRON OXIDE PARTICLES WITH A HYDROLYSIS-RESISTANT COATING
审中-公开
PROCESS FOR与水解COVER PRODUCING附聚物的纳米级氧化铁颗粒
- Patent Title: PROCESS FOR PREPARING AGGLOMERATE-FREE NANOSCALAR IRON OXIDE PARTICLES WITH A HYDROLYSIS-RESISTANT COATING
- Patent Title (中): PROCESS FOR与水解COVER PRODUCING附聚物的纳米级氧化铁颗粒
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Application No.: PCT/EP1997001758Application Date: 1997-04-09
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Publication No.: WO1997038058A1Publication Date: 1997-10-16
- Inventor: INSTITUT FÜR NEUE MATERIALIEN GEM. GMBH
- Applicant: INSTITUT FÜR NEUE MATERIALIEN GEM. GMBH , LESNIAK, Christoph , SCHIESTEL, Thomas , NASS, Rüdiger , SCHMIDT, Helmut
- Assignee: INSTITUT FÜR NEUE MATERIALIEN GEM. GMBH,LESNIAK, Christoph,SCHIESTEL, Thomas,NASS, Rüdiger,SCHMIDT, Helmut
- Current Assignee: INSTITUT FÜR NEUE MATERIALIEN GEM. GMBH,LESNIAK, Christoph,SCHIESTEL, Thomas,NASS, Rüdiger,SCHMIDT, Helmut
- Priority: DE196 19960410
- Main IPC: C09D17/00
- IPC: C09D17/00
Abstract:
The invention relates to a process for preparing an agglomerate-free suspension of nanoscalar iron oxide particles coated in a stable manner. Said process comprises the following stages in the given order: (1) preparation of an aqueous suspension of nanoscalar iron oxide particles which are partially or completely in the form of agglomerates; (2) addition (i) of a trialoxysilane which has a hydrocarbon group bonded directly to Si, to which group at least one amino group, carboxyl group, epoxy group, mercapto group, cyano group, hydroxy group and/or (meth)acryl group is bonded and (ii) addition of a polar organic solvent which can mixed with water and has a boiling point at least 10 DEG C higher than the boiling point of water; (3) treatment of the resulting suspension with ultrasound until at least 70 % of the particles present are in the range of +/- 20 % of the average particle diameter; (4) removal by distillation of the water by the action of ultrasound; and (5) separation of the non-disintegrated agglomerates.
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