Invention Application
- Patent Title: METHOD FOR PRODUCING CATALYST MONOLITHS
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Application No.: PCT/EP2017/080794Application Date: 2017-11-29
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Publication No.: WO2018099956A1Publication Date: 2018-06-07
- Inventor: GROENEVELD, Esther , BERBEN, Peter , REESINK, Bennie
- Applicant: BASF SE
- Applicant Address: Carl-Bosch-Str. 38 67056 Ludwigshafen am Rhein DE
- Assignee: BASF SE
- Current Assignee: BASF SE
- Current Assignee Address: Carl-Bosch-Str. 38 67056 Ludwigshafen am Rhein DE
- Agency: FÉAUX DE LACROIX, Stefan
- Priority: EP16201403.9 20161130
- Main IPC: B29C64/106
- IPC: B29C64/106 ; B29C64/165 ; B01J23/755 ; B01J21/08 ; B01J35/04
Abstract:
A method for producing a three-dimensional porous catalyst monolith of stacked catalyst fibers, comprising the following steps: a) Preparing a suspension paste in a liquid diluent of metal, metal alloy and/or metal oxide particles of catalytically active metal or metal alloy in which the metals, metal alloy and metal oxide particles can be supported on or mixed with inorganic oxide catalyst support particles, and which suspension can furthermore comprise a binder material, all particles in the suspension having an average particle size in the range of from 0.5 to 500 µm, b) extruding the paste of step a) through one or more nozzles preferably having a maximum diameter of less than 5 mm, more preferably less than 1 mm to form fibers, and depositing the extruded fibers to form a three-dimensional porous catalyst monolith precursor, c) drying the porous catalyst monolith precursor to remove the liquid diluent, d) if necessary, reducing the metal oxide(s) in the porous catalyst monolith precursor to form the catalytically active metal or metal alloy, wherein no temperature treatment of the porous catalyst monolith precursor or porous catalyst monolith at temperatures above 1000 °C is performed.
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