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1.发明授权A highly purified 1-aminopropanediol-2,3 and a method for the purification thereof 无效高纯度的1-氨基丙二醇-2,3-和用于该化合物的纯化方法。
公开(公告)号：EP0470004B1
公开(公告)日：1995-01-25
申请号：EP91402167.0
申请日：1991-08-01
发明人： Koyama, Hiroshi , Takemoto, Etsuo
IPC分类号： C07C213/10 , C07C215/10
CPC分类号： C07C215/10 , C07C213/10 , Y10S159/16
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公开(公告)号：EP1201644A2
公开(公告)日：2002-05-02
申请号：EP02002839.5
申请日：1997-10-22
IPC分类号： C07C213/10
CPC分类号： C07C213/04 , C07C213/10 , C07C215/10
摘要： Disclosed are a process for the preparation of a dihydroxyamino compound in which water and discoloring ingredients are removed while preventing decomposition of a dihydroxyamino compound by distilling a crude reaction liquid containing an epoxy compound and an amino compound at a specified temperature and pressure, a process for improving a yield of a dihydroxyamino compound having high purity by recirculating an aqueous solution of an amino compound recollected from a crude reaction liquid into a reaction step, and a process in which there are prevented discoloration and a yield decline of a dihydroxyamino compound.
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公开(公告)号：EP0839802A3
公开(公告)日：1998-07-29
申请号：EP97402495.2
申请日：1997-10-22
IPC分类号： C07C253/34
CPC分类号： C07C213/04 , C07C213/10 , C07C215/10
摘要： Disclosed are a process for the preparation of a dihydroxyamino compound in which water and discoloring ingredients are removed while preventing decomposition of a dihydroxyamino compound by distilling a crude reaction liquid containing an epoxy compound and an amino compound at a specified temperature and pressure, a process for improving a yield of a dihydroxyamino compound having high purity by recirculating an aqueous solution of an amino compound recollected from a crude reaction liquid into a reaction step, and a process in which there are prevented discoloration and a yield decline of a dihydroxyamino compound.
摘要翻译： 本发明公开了一种制备二羟基氨基化合物的方法，其中通过在特定的温度和压力下蒸馏含有环氧化合物和氨基化合物的粗制反应液来防止二羟基氨基化合物分解，同时除去水和脱色成分， 通过将从粗反应液中回收的氨基化合物的水溶液再循环到反应步骤中来提高高纯度的二羟基氨基化合物的收率，以及防止二羟基氨基化合物的变色和收率降低的方法。
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公开(公告)号：EP1201644B1
公开(公告)日：2011-08-24
申请号：EP02002839.5
申请日：1997-10-22
IPC分类号： C07C213/10
CPC分类号： C07C213/04 , C07C213/10 , C07C215/10
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公开(公告)号：EP1201644A3
公开(公告)日：2004-01-02
申请号：EP02002839.5
申请日：1997-10-22
IPC分类号： C07C213/10
CPC分类号： C07C213/04 , C07C213/10 , C07C215/10
摘要： Disclosed are a process for the preparation of a dihydroxyamino compound in which water and discoloring ingredients are removed while preventing decomposition of a dihydroxyamino compound by distilling a crude reaction liquid containing an epoxy compound and an amino compound at a specified temperature and pressure, a process for improving a yield of a dihydroxyamino compound having high purity by recirculating an aqueous solution of an amino compound recollected from a crude reaction liquid into a reaction step, and a process in which there are prevented discoloration and a yield decline of a dihydroxyamino compound.
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6.发明公开A process for the preparation of a dihydroxyamino compound 失效Verfahren zur Herstellung einer Dihydroxyamino-Verbindung
公开(公告)号：EP0839802A2
公开(公告)日：1998-05-06
申请号：EP97402495.2
申请日：1997-10-22
IPC分类号： C07C253/34
CPC分类号： C07C213/04 , C07C213/10 , C07C215/10
摘要： Disclosed are a process for the preparation of a dihydroxyamino compound in which water and discoloring ingredients are removed while preventing decomposition of a dihydroxyamino compound by distilling a crude reaction liquid containing an epoxy compound and an amino compound at a specified temperature and pressure, a process for improving a yield of a dihydroxyamino compound having high purity by recirculating an aqueous solution of an amino compound recollected from a crude reaction liquid into a reaction step, and a process in which there are prevented discoloration and a yield decline of a dihydroxyamino compound.
摘要翻译： 公开了一种制备二羟基氨基化合物的方法，其中除去水和变色成分，同时通过在特定温度和压力下蒸馏含有环氧化合物和氨基化合物的粗反应液体来防止二羟基氨基化合物的分解， 通过将从粗反应液体回收的氨基化合物的水溶液再循环到反应步骤中，提高具有高纯度的二羟基氨基化合物的产率，以及防止二羟基氨基化合物的变色和产率下降的方法。
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7.发明公开A highly purified 1-aminopropanediol-2,3 and a method for the purification thereof 无效Hochreines 1-Aminopropandiol-2,3 und Verfahren zur Reinigung dieser Verbindung。
公开(公告)号：EP0470004A1
公开(公告)日：1992-02-05
申请号：EP91402167.0
申请日：1991-08-01
发明人： Koyama, Hiroshi , Takemoto, Etsuo
IPC分类号： C07C213/10 , C07C215/10
CPC分类号： C07C215/10 , C07C213/10 , Y10S159/16
摘要： 1-aminopropanediol-2,3 containing 2-aminopropanediol-1,3 of less than 0.30 % by weight can be prepared by the present purification process, which comprises distilling a 1-aminopropanediol-2,3 containing at least 0.3 % of 2-aminopropanediol-1,3 based on the weight of 1-aminopropanediol-2,3 with a distillation column, said distillation column having low pressure loss.
摘要翻译： 可以通过本纯化方法制备含有小于0.30重量％的2-氨基丙二醇-1,3-的1-氨基丙二醇-2,3，其包括将含有至少0.3％的2-氨基丙二醇-2,3-二 氨基丙二醇-1,3-基于1-氨基丙二醇-2,3的重量与蒸馏塔，所述蒸馏塔具有低压力损失。
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