PROCESS FOR PRODUCTION OF PHOSPHORIC ACID BY CRYSTALLISATION OF PHOSPHORIC ACID HEMIHYDRATE
    1.
    发明授权
    PROCESS FOR PRODUCTION OF PHOSPHORIC ACID BY CRYSTALLISATION OF PHOSPHORIC ACID HEMIHYDRATE 有权
    用于生产PHOSPHORIC结晶PHOSPHORIC半水

    公开(公告)号:EP1171382B1

    公开(公告)日:2002-12-04

    申请号:EP00914207.6

    申请日:2000-03-23

    IPC分类号: C01B25/234

    CPC分类号: C01B25/234

    摘要: The invention relates to a process for producing simultaneously food-grade and fodder-grade phosphoric acid by crystallizing phosphoric acid hemihydrate, H3PO4 x 0.5 H2O, from a prepurified feed acid, which is purified and crystallized with the help of the following steps, a) after the step of froth-flotation of phosphate concentrate, the concentrate is directed to a strongly magnetic separation step in order to decrease the Mg ion amount, b) the phosphate concentrate is leached in a mixture of sulfuric acid and phosphoric acid according to the wet process, the precipitated SO4 and As ions are removed, and a silicon source is added in order to adjust the F/Si molar ratio to 58% P2O5, solids concentration of

    PROCESS FOR PRODUCTION OF PHOSPHORIC ACID BY CRYSTALLISATION OF PHOSPHORIC ACID HEMIHYDRATE
    2.
    发明公开
    PROCESS FOR PRODUCTION OF PHOSPHORIC ACID BY CRYSTALLISATION OF PHOSPHORIC ACID HEMIHYDRATE 有权
    用于生产PHOSPHORIC结晶PHOSPHORIC半水

    公开(公告)号:EP1171382A1

    公开(公告)日:2002-01-16

    申请号:EP00914207.6

    申请日:2000-03-23

    IPC分类号: C01B25/234

    CPC分类号: C01B25/234

    摘要: The invention relates to a process for producing simultaneously food-grade and fodder-grade phosphoric acid by crystallizing phosphoric acid hemihydrate, H3PO4 x 0.5 H2O, from a prepurified feed acid, which is purified and crystallized with the help of the following steps, a) after the step of froth-flotation of phosphate concentrate, the concentrate is directed to a strongly magnetic separation step in order to decrease the Mg ion amount, b) the phosphate concentrate is leached in a mixture of sulfuric acid and phosphoric acid according to the wet process, the precipitated SO4 and As ions are removed, and a silicon source is added in order to adjust the F/Si molar ratio to 58% P2O5, solids concentration of