摘要:
A process for preparing organosilicon compounds comprising polycarbosilane which comprises pyrolyzing polysilane such as polydimethylsilane as the starting material and simultaneously polycondensing the products produced by the pyrolysis, characterized by, while maintaining the pressure at 2-10 Kg/cm² in the system, separating gases produced by the pyrolysis and polycondensation into non-condensed gases and a liquid by the use of a partial condenser and then continuously removing the separated gases from the system simultaneously with returning the separated liquid to the reaction system, thereby to obtain organosilicon compounds suitable as material for silicon carbide fibers.
摘要翻译:一种制备包含聚碳硅烷的有机硅化合物的方法,其包括热聚聚硅烷如聚二甲基硅烷作为起始原料,同时使由热解产生的产物缩聚,其特征在于在体系中保持2-10Kg / cm 2的压力, 将通过热解和缩聚产生的气体通过使用部分冷凝器分离成液体,然后在将分离的液体返回到反应体系中同时连续地从系统中除去分离的气体,从而获得适合的有机硅化合物 作为碳化硅纤维的材料。