Title translation:VERFAHREN ZUR ANALIESE VON STICKSTOFF METALPROBEN,VORRICHTUNG ZUR ANALYSE VON STICKSTOFF METALLPROBEN,VERFAHREN ZUR ANPASSUNG DER STICKOFOFKONZENZATION IN GESCHMOLZENEM STAHL UND VERFAHREN
Abstract:
Provided are a method for analyzing nitrogen in a metal sample with which nitrogen content in a metal sample is determined accurately and at low cost, an apparatus for analyzing nitrogen in a metal sample, a method for adjusting nitrogen concentration in molten steel, and a method for manufacturing steel. The method for analyzing nitrogen in a metal sample according to the present invention includes: a melting process in which a metal sample containing a nitrogen component is melted in an argon gas atmosphere by performing impulse heating to gasify the nitrogen component; and an analyzing process in which nitrogen content in the metal sample is determined by analyzing nitrogen gas generated in the melting process and the argon gas by using a gas discharge optical emission method. By analyzing the nitrogen concentration of a sample taken from molten steel by using the analysis method described above, and by determining treatment conditions for adjusting nitrogen concentration on the basis of the nitrogen analysis value derived by the analysis, nitrogen concentration in molten steel is adjusted.
Abstract:
A method for analyzing a metal specimen includes an electrolysis step of electrolyzing a metal specimen containing a reference element and a target element in an electrolytic solution, a sampling step of sampling a portion of the electrolytic solution, an analysis step of analyzing the sampled electrolytic solution, a concentration ratio-calculating step of calculating the concentration ratio of the target element to the reference element in the electrolytic solution on the basis of the analysis results, and a content-calculating step of calculating the content of the target element present in the form of a solid solution by multiplying the content of the reference element in the metal specimen by the obtained concentration ratio.
Abstract:
A method for analyzing a metallic material includes the steps of electrolyzing a metal sample in an electrolyte; removing the electrolyzed metal sample from the electrolyte; immersing the metal sample removed from the electrolyte into a dispersive solution that is different from the electrolyte to separate at least one selected from the group consisting of a precipitate and an inclusion deposited on the metal sample; and analyzing the at least one selected from the group consisting of a precipitate and an inclusion extracted into.the dispersive solution.
Abstract:
There are provided a method for desulfurizing molten steel, characterized in that a sample taken out from molten steel after the tapping from a converter or during the secondary refining is analyzed rapidly in a high accuracy by a method comprising a high frequency induction heating step wherein the sample is combusted and oxidized under the high frequency induction heating in a pure oxygen atmosphere to convert S in the sample into SO 2 and an analyzing step wherein SO 2 -containing gas produced in the high frequency induction heating step is analyzed through an ultraviolet fluorescence method to quantify S concentration of the sample, whereby S concentration of molten steel after the tapping from the converter can be controlled in a high accuracy to prevent failure of S concentration and also desulfurization time in the secondary refining can be shortened and the amount of the desulfurizer or the like used can be reduced, and a method of manufacturing molten steel by using such a method.