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公开(公告)号：US4140773A
公开(公告)日：1979-02-20
申请号：US880830
申请日：1978-02-24
CPC分类号： C01F7/36 , C01P2004/32 , C01P2006/12 , C01P2006/16
摘要： High macro-pore content spheres (>1000A) are produced by use of a rotating wheel, wherein dry alumina is dropped onto the wheel under a peptizing spray misted onto the wheel through an atomizing device. Compressive stresses normally encountered in procedures such as pelletizing are avoided, thereby preserving macro-pores. Size of spheres can be adjusted by altering, for example, the angle at which the wheel rotates.
摘要翻译： 通过使用旋转轮产生高的大孔含量球体（> 1000A），其中干燥氧化铝通过雾化装置在雾化喷雾下方落在轮上。 避免在诸如造粒的过程中通常遇到的压缩应力，从而保留大孔。 可以通过改变例如车轮旋转的角度来调节球体的尺寸。
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公开(公告)号：US4218413A
公开(公告)日：1980-08-19
申请号：US970282
申请日：1978-12-18
CPC分类号： B01J20/08 , C01F7/448 , C01P2006/14
摘要： A method for increasing the pore volume of alumina powder produced by spray drying alumina slurries by heating the slurry to a temperature near the boiling point of water and a pressure up to the critical point of water then introducing the slurry to a spray drying chamber through a small orifice, thereby creating a backpressure in excess of slurry vapor pressure and up to the critical point of water.
摘要翻译： 通过将浆料加热到接近水沸点的温度并将压力升至水的临界点，从而通过喷雾干燥氧化铝浆料产生的氧化铝粉末的孔体积增加的方法，然后将浆料通过 从而产生超过浆料蒸汽压力并高达临界点的背压。
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公开(公告)号：US4176171A
公开(公告)日：1979-11-27
申请号：US933310
申请日：1978-08-14
CPC分类号： C01F7/36 , C01P2006/10 , C01P2006/12 , C01P2006/14 , C01P2006/16
摘要： An improved method for increasing alumina pore volumes said alumina being produced by the hydrolysis of aluminum alkoxides, the improvement comprising diluting the aluminum alkoxide, prior to entering the hydrolysis reactor, with an alkanol containing from 2 to 8 carbon atoms and injecting the dilute solution into the reactor at high velocities.
摘要翻译： 一种用于增加氧化铝孔体积的改进方法，所述氧化铝是通过水解醇铝产生的，其改进包括在进入水解反应器之前用含有2-8个碳原子的链烷醇稀释醇铝，并将稀溶液注入 反应堆处于高速度。
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公开(公告)号：US4117106A
公开(公告)日：1978-09-26
申请号：US820527
申请日：1977-08-01
申请人： Larry L. Bendig , John F. Scamehorn
发明人： Larry L. Bendig , John F. Scamehorn
CPC分类号： C01F7/36 , C01P2002/60 , C01P2004/51 , C01P2004/61 , C01P2006/10 , C01P2006/12 , C01P2006/14 , C01P2006/16 , C01P2006/80
摘要： Aluminum alkoxides are hydrolyzed at low temperatures using high injection velocities and are then vacuum stripped at or below 80.degree. C to produce .beta.-alumina trihydrates in large proportion. The .beta.-alumina trihydrate can then be converted to eta alumina.
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公开(公告)号：US4133871A
公开(公告)日：1979-01-09
申请号：US820528
申请日：1977-08-01
CPC分类号： C01F7/36 , C01P2006/10 , C01P2006/12 , C01P2006/16
摘要： An improvement in the method of preparing alumina by water hydrolysis of aluminum alkoxides is disclosed. Briefly, the improvement comprising admixing the water and aluminum alkoxide under high velocity conditions prior to passing the resulting admixture to the reactor. The improved process results in a product having improved physical properties, particularly pore volume and bulk density.
摘要翻译： 公开了通过水解铝醇盐制备氧化铝的方法的改进。 简而言之，改进包括在将所得混合物通入反应器之前，在高速条件下混合水和烷氧化铝。 改进的方法产生具有改善的物理性能，特别是孔体积和体积密度的产品。
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公开(公告)号：US4696726A
公开(公告)日：1987-09-29
申请号：US885519
申请日：1986-07-14
CPC分类号： C07C31/36 , B01D61/025 , C07C29/76
摘要： A continuous process for the production of dichlorohydrin by the reaction of allyl chloride, water and chlorine having substantially lower energy requirements than conventional processes, wherein the reaction mixture is subjected to reverse osmosis to concentrate the dichlorohydrin and to provide a permeate stream substantially free of dichlorohydrin, which permeate stream is recycled to the reaction.
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7.发明授权
公开(公告)号：US6119511A
公开(公告)日：2000-09-19
申请号：US299379
申请日：1999-04-27
申请人： Sherril D. Christian , Andrew R. Slagle , Edwin E. Tucker , John F. Scamehorn , Katsuhiko Fujio
发明人： Sherril D. Christian , Andrew R. Slagle , Edwin E. Tucker , John F. Scamehorn , Katsuhiko Fujio
IPC分类号： G01N13/02
CPC分类号： G01N13/02
摘要： A method and apparatus is presented for determining surface tension of a liquid or interfacial tension between two dissimilar liquids by using a rigidly suspended probe with small sample sizes and by measuring probe force using a top-loading balance used for supporting the container of liquids under test. When a small sample size in a small container is used, capillary action between a probe and the container walls enhances the measured force, and an adjustment factor for the capillary action must be applied. A probe rigidly suspended to overcome capillary action between the probe and walls permits such measurements. For any sized sample, in accordance with Isaac Newton's third law of equal and opposite forces acting between objects, the force required for lifting a probe vertically from a liquid is equivalent to the reduction in weight of the liquid and container. Force magnitude is thus determined using a top-loading balance for observing weight change, either in the liquid while a suitably configured probe is withdrawn from the liquid or in a probe suspended by a direction converter resting on a top-loading balance while the container and liquid are lowered.
摘要翻译： 提出了一种方法和装置，用于通过使用具有小样品尺寸的刚性悬挂的探针和通过使用用于支撑待测液体的容器的顶部负载平衡来测量探针力来确定液体的表面张力或两种不同液体之间的界面张力 。 当使用小容器中的小样品尺寸时，探头和容器壁之间的毛细作用增强了测量的力，并且必须应用毛细作用的调节因子。 刚性悬挂以克服探针和墙壁之间的毛细作用的探针允许这种测量。 对于任何尺寸的样品，根据Isaac Newton在物体之间作用的相等和相反力的第三定律，从液体垂直提起探头所需的力等于液体和容器重量的减少。 因此，使用用于观察重量变化的顶部载荷平衡来确定力的大小，无论是在液体中，而适当配置的探针从液体中取出，或者在由搁置在顶部装载平衡上的方向转换器悬挂的探针中，而容器和 液体降低。
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8.发明授权Method for selectively plugging the more permeable regions of an underground formation having non-uniform permeability 失效选择性地堵塞具有不均匀渗透性的地下地层的更可渗透区域的方法
公开(公告)号：US4745976A
公开(公告)日：1988-05-24
申请号：US908634
申请日：1986-09-18
IPC分类号： C09K8/50 , E21B43/22 , E21B33/138
CPC分类号： C09K8/501
摘要： A method for selectively plugging the more permeable regions of an underground formation having non-uniform permeability wherein a first surfactant solution is injected into the formation in an amount effective to contact a substantial portion of the surface area of the highly permeable regions of the formation, which first surfactant solution is characterized as having a selected chromatographic velocity and as being capable of reversibly adsorbing onto the surface of the pores of the formation.After injecting the first surfactant solution, a water-soluble spacer fluid is injected in an amount sufficient to place the first surfactant solution a selected distant into the formation, the spacer fluid being characterized as having a pre-injection viscosity about equal to the first surfactant solution.After injecting the space fluid, a second surfactant solution is injected in an amount about equal to the amount of the first surfactant solution, and characterized as having a pre-injection viscosity about equal to the first surfactant solution and the spacer fluid, and as having a selected chromatographic velocity which is higher than the chromatographic velocity of the first surfactant solution, and has having a composition such that it will be capable of interacting physically with the first surfactant solution to produce a phase change so that the product of such interaction is capable of at least partially plugging the pores of the formation in which such product is placed.
摘要翻译： 一种用于选择性地堵塞具有不均匀渗透性的地下地层的更可渗透区域的方法，其中第一表面活性剂溶液以有效接触地层的高可渗透区域的大部分表面积的量注入到地层中， 该第一表面活性剂溶液的特征在于具有选定的色谱速度并且能够可逆地吸附在地层的孔的表面上。 在注入第一表面活性剂溶液之后，以足以将第一表面活性剂溶液置于地层中的量使其注入水溶性间隔液，间隔液的特征在于预注射粘度大约等于第一表面活性剂 解。 在注入空间流体之后，以与第一表面活性剂溶液的量相等的量注入第二表面活性剂溶液，其特征在于具有等于第一表面活性剂溶液和间隔液的预注射粘度，并且具有 所选择的色谱速度高于第一表面活性剂溶液的色谱速度，并且具有使其能够与第一表面活性剂溶液物理相互作用以产生相变的组成，使得这种相互作用的产物具有能力 至少部分地堵塞放置这种产品的地层的孔隙。
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9.发明授权Incomplete drying of activated carbon in a process for VCM reduction in vapors 失效在蒸气中VCM还原过程中活性炭不完全干燥
公开(公告)号：US4128405A
公开(公告)日：1978-12-05
申请号：US769361
申请日：1977-02-16
CPC分类号： B01D53/02
摘要： A method for adsorbing VCM from vapors through the use of incompletely dried activated carbon under essentially adiabatic conditions allowing most of the VCM to adsorb on carbon having water previously adsorbed, the heat of adsorption of VCM desorbing the water instead of heating the carbon bed. The VCM adsorption is greater than that found on a dry bed when an adiabatic temperature rise is allowed to occur on the dry bed. A portion of the carbon bed can be kept dry if necessary to reach desired VCM levels. The advantage of the invention resides in adsorbing greater amounts of VCM per pound of carbon used, less drying necessary after regeneration, and less likelihood of high temperature deleterious reactions occurring.
摘要翻译： 一种通过在绝对条件下使用不完全干燥的活性炭从蒸气中吸附VCM的方法，允许大部分VCM吸附在先前被吸附的水的碳上，VCM吸附热而不是加热碳床。 当干燥床上允许绝热温度升高时，VCM吸附大于在干燥床上发现的吸附。 如果需要，碳床的一部分可以保持干燥以达到所需的VCM水平。 本发明的优点在于吸附更多量的VCM每磅碳，再生后需要较少的干燥，并且发生高温有害反应的可能性较小。
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公开(公告)号：US4126750A
公开(公告)日：1978-11-21
申请号：US857052
申请日：1977-12-05
IPC分类号： B01J8/06 , B01J21/00 , C07B61/00 , C07C27/00 , C07C37/16 , C07C39/07 , C07C67/00 , C07C37/12
CPC分类号： B01J8/067 , C07C37/16 , B01J2208/0007 , B01J2208/00212 , B01J2208/0053
摘要： High pressure methylation of 2,6-xylenol to produce 2,3,6-trimethylphenol is accomplished by maintaining the methanol/2,6-xylenol feed at temperature and pressures sufficient to keep the feed liquid in a reactor head then forcing the feed through orifices, expanding the feed into a mixed vapor liquid phase, the feed after expansion being in the range of reaction conditions of pressure and temperature while in the presence of the catalyst where the reaction takes place. The process avoids the current problems of uneven feed mixtures and catalyst tube plugging.
摘要翻译： 2,6-二甲苯酚的高压甲基化制备2,3,6-三甲基苯酚是通过将甲醇/ 2,6-二甲苯酚进料保持在足够的温度和压力下将进料液体保持在反应器头中，然后强制进料通过 孔，将进料膨胀成混合汽相液相，膨胀后的进料在反应发生的催化剂存在下在压力和温度的反应条件的范围内。 该过程避免了当前不均匀的进料混合物和催化剂管堵塞的问题。
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