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1.发明授权
公开(公告)号：US5510212A
公开(公告)日：1996-04-23
申请号：US350281
申请日：1994-12-02
申请人： Frank M. Delnick , Narayan Doddapaneni , Robert R. Lagasse , Ronald F. Simandl , D. Gerald Glasgow , Alan Sylwester
发明人： Frank M. Delnick , Narayan Doddapaneni , Robert R. Lagasse , Ronald F. Simandl , D. Gerald Glasgow , Alan Sylwester
摘要： A secondary battery having a rechargeable lithium-containing anode, a cathode, and a separator positioned between the cathode and anode with an organic electrolyte solution absorbed therein is provided. The anode comprises three-dimensional microporous carbon structures synthesized by the controlled pyrolysis of gel derived polymer foam precursors. The gradual heating process in the carbonization of pretreated foam precursors stabilizes the pore structures in the pretreated foam.
摘要翻译： 提供了具有可再充电的含锂阳极，阴极和位于阴极和阳极之间并且吸收有机电解质溶液的隔膜的二次电池。 阳极包括通过凝胶衍生的聚合物泡沫前体的受控热解合成的三维微孔碳结构。 预处理的泡沫前体的碳化中的逐渐加热过程稳定了预处理泡沫体中的孔结构。
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2.发明授权公开(公告)号：US06506355B1
公开(公告)日：2003-01-14
申请号：US09444877
申请日：1999-11-22
申请人： D. Gerald Glasgow , Max L. Lake
发明人： D. Gerald Glasgow , Max L. Lake
IPC分类号： D01F912
摘要： High surface energy vapor grown carbon fibers and methods of making such fibers. The high surface energy vapor grown carbon fibers of the present invention have a surface energy greater than about 75 mJ/m2 without post-manufacture treatment.
摘要翻译： 高表面能蒸汽生长碳纤维和制造这种纤维的方法。 本发明的高表面能蒸汽生长碳纤维的表面能大于约75mJ / m 2，而无需后处理。
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公开(公告)号：US06911169B2
公开(公告)日：2005-06-28
申请号：US10315500
申请日：2002-12-09
CPC分类号： B29C70/14
摘要： A method of making a composite article of a graphite-filled polymer mixture that is robust during high shear mixing and compounding, and that exhibits relatively low electrical resistivity after molding. The mixture is formed by shear mixing a liquid polymeric material, graphitized carbon fibers having diameters of less than one micrometer, and glass fibers longer than the carbon fibers. The carbon and glass fibers constitute up to about 25 volume percent and up to about 50 weight percent, respectively, of the mixture, though the addition of as little as about 1 weight percent of the glass fibers has been shown to dramatically reduce resistivity. The mixture is then introduced into a mold so that the glass fibers are substantially oriented parallel to the direction of flow. Due at least in part to the glass fibers being larger than the carbon fibers, the carbon fibers are substantially aligned with the glass fibers and preferentially segregate to regions of the polymeric matrix near interfaces between the polymeric matrix and the glass fibers.
摘要翻译： 一种制备石墨填充聚合物混合物的复合制品的方法，其在高剪切混合和配混期间是坚固的，并且在模制之后显示相对低的电阻率。 混合物通过剪切混合液体聚合物材料，直径小于1微米的石墨化碳纤维和长于碳纤维的玻璃纤维形成。 尽管添加少至约1重量百分比的玻璃纤维可显着降低电阻率，碳和玻璃纤维分别占混合物的高达约25体积％和最多约50重量％。 然后将混合物引入模具中，使得玻璃纤维基本上定向为平行于流动方向。 至少部分地由于玻璃纤维大于碳纤维，碳纤维基本上与玻璃纤维对准，并优先分离到聚合物基质与聚合物基质和玻璃纤维之间界面附近的区域。
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4.发明授权Process for preparation of cross-linked poly(tri-n-butyltin)methacrylate with simultaneous particle size reduction 失效制备交联聚（三正丁基锡）甲基丙烯酸酯同时粒度降低的方法
公开(公告)号：US4524190A
公开(公告)日：1985-06-18
申请号：US609940
申请日：1984-05-14
申请人： D. Gerald Glasgow , Joseph Satanek
发明人： D. Gerald Glasgow , Joseph Satanek
摘要： Poly(tri-n-butyltin) methacrylate, an anti-fouling compound, is prepared bysterifying a cross-linked polymethacrylic acid with tributyltin oxide in the presence of a poly solvent. The poly solvent, such as acetone, dioxane or methyl-ethyl ketone, causes particle size reduction due to hydraulic shattering. The in-reaction particle size reduction eliminates the need for mechanical post grinding in the current process.
摘要翻译： 聚（三正丁基锡）甲基丙烯酸酯，防污化合物是通过在多溶剂的存在下，用三丁基氧化锡酯化交联的聚甲基丙烯酸来制备的。 多溶剂如丙酮，二恶烷或甲基乙基酮由于水力破碎而引起粒度降低。 反应中的粒度减小消除了在当前工艺中机械后磨削的需要。
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