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公开(公告)号:US09926266B2
公开(公告)日:2018-03-27
申请号:US15292106
申请日:2016-10-12
Applicant: KOREA INSTITUTE OF SCIENCE AND TECHNOLOGY
Inventor: Hyoung-Juhn Kim , Eun Ki Kim , So Young Lee , Jong Hyun Jang , Jin Young Kim , Sung Jong Yoo , Dirk Henkensmeier , Dae Ki Choi , Jonghee Han , Suk Woo Nam
IPC: C07C303/44 , C07C303/32 , C07C309/24
CPC classification number: C07C303/44 , C07C303/32 , C07C309/24
Abstract: Disclosed are a method for preparing a pure isophthalaldehyde bisulfite adduct free from impurities through a specific purification process, and use thereof as a starting material for polymerizing polybenzimidazole under a mild condition. According to the present disclosure, it is possible to obtain a pure isophthalaldehyde bisulfite adduct free from impurities, such as unreacted materials or byproducts. In addition, it is possible to accomplish industrial mass production of a high-molecular weight polybenzimidazole by using the adduct as a starting material for polymerizing polybenzimidazole under a mild condition in an organic solvent.