公开(公告)号：US09512127B2

公开(公告)日：2016-12-06

申请号：US14499280

申请日：2014-09-29

Applicant: U.S. Army Research Laboratory ATTN: RDRL-LOC-I

Inventor： William Matthew Sherrill ,  Joseph Erik Banning

IPC: C07D487/04 ,  C06B25/34 ,  C06B45/00

CPC classification number: C07D487/04 ,  C06B25/34 ,  C06B45/00

Abstract: A spherical morphology of the high explosive tetranitroglycoluril (TNGU) has been discovered. This new morphology exhibits approximately a twofold improvement in the response of the material to impact, more than a one and a half fold improvement in friction and the same high resistance to electrostatic discharge over non-spherical TNGU produced by other methods.

Abstract translation: 已经发现高爆炸四硝基甘油（TNGU）的球形形态。 这种新的形态在材料对冲击的响应方面表现出大约两倍的改善，摩擦力提高了大约一倍半，而且通过其它方法产生的非球形TNGU具有相同的抗静电放电性能。

公开(公告)号：US09695177B2

公开(公告)日：2017-07-04

申请号：US14499278

申请日：2014-09-29

Applicant: U.S. Army Research Laboratory ATTN: RDRL-LOC-I

Inventor： William Matthew Sherrill ,  Eric Christopher Johnson

IPC: C06B25/34 ,  C06B45/00 ,  C07D487/04

CPC classification number: C07D487/04 ,  C06B25/34 ,  C06B45/00

Abstract: An improved method of preparing tetranitroglycoluril (TNGU) via the in situ decomposition of a nitrimino group with elimination of nitrogen without the use of dinitrogen pentoxide. The compound is useful as a high energy, high density explosive or propellant oxidizer.

公开(公告)号：US20160176878A1

公开(公告)日：2016-06-23

申请号：US14499278

申请日：2014-09-29

Applicant: U.S. Army Research Laboratory ATTN: RDRL-LOC-I

Inventor： William Matthew Sherrill ,  Eric Christopher Johnson

IPC: C07D487/04

CPC classification number: C07D487/04 ,  C06B25/34 ,  C06B45/00

Abstract: An improved method of preparing tetranitroglycoluril (TNGU) via the in situ decomposition of a nitrimino group with elimination of nitrogen without the use of dinitrogen pentoxide. The compound is useful as a high energy, high density explosive or propellant oxidizer.

Abstract translation: 通过在不使用五氧化二氮的情况下消除氮而原位分解硝酸基团来制备四硝基甘油（TNGU）的改进方法。 该化合物可用作高能量，高密度炸药或推进剂氧化剂。

公开(公告)号：US20160090388A1

公开(公告)日：2016-03-31

申请号：US14499280

申请日：2014-09-29

Applicant: U.S. Army Research Laboratory ATTN: RDRL-LOC-I

Inventor： William Matthew Sherrill ,  Joseph Erik Banning

IPC: C07D487/04 ,  C06B25/34 ,  C06B45/00

CPC classification number: C07D487/04 ,  C06B25/34 ,  C06B45/00

Abstract: A spherical morphology of the high explosive tetranitroglycoluril (TNGU) has been discovered. This new morphology exhibits approximately a twofold improvement in the response of the material to impact, more than a one and a half fold improvement in friction and the same high resistance to electrostatic discharge over non-spherical TNGU produced by other methods.

Abstract translation: 已经发现高爆炸四硝基甘油（TNGU）的球形形态。 这种新的形态在材料对冲击的响应方面表现出大约两倍的改善，摩擦力提高了大约一倍半，而且通过其它方法产生的非球形TNGU具有相同的抗静电放电性能。