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公开(公告)号：US06586115B2
公开(公告)日：2003-07-01
申请号：US09833446
申请日：2001-04-12
IPC分类号： B32B1504
CPC分类号： F01D5/288 , C04B35/486 , C04B2235/3206 , C04B2235/3208 , C04B2235/3213 , C04B2235/3215 , C04B2235/3224 , C04B2235/3225 , C04B2235/3227 , C04B2235/3229 , C04B2235/3272 , C04B2235/3275 , C04B2235/3279 , C04B2235/787 , C04B2235/80 , C04B2235/85 , C23C28/00 , C23C30/00 , F05D2300/134 , F05D2300/5024 , Y10T29/49922 , Y10T428/12611 , Y10T428/12618 , Y10T428/249956
摘要： A thermal barrier coating (TBC) for a component intended for use in a hostile environment, such as the superalloy turbine, combustor and augmentor components of a gas turbine engine. The TBC is formed of zirconia that is partially stabilized with yttria (YSZ), preferably not more than 3 weight percent yttria, and to which one or more additional metal oxides are alloyed to increase crystallographic defects and lattice strains in the TBC grains and/or form precipitates of zirconia and/or compound(s) of zirconia and/or yttria and the additional metal oxide(s), the inclusion of which reduces the thermal conductivity of the YSZ to levels lower than conventional 6-8% YSZ. Improvements are particularly contemplated for TBC having a columnar grain structure, such as those deposited by EBPVD and other PVD techniques.
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12.发明授权公开(公告)号：US06533875B1
公开(公告)日：2003-03-18
申请号：US09693077
申请日：2000-10-20
IPC分类号： B05D722
CPC分类号： C23C28/321 , C23C10/18 , C23C10/26 , C23C10/30 , C23C10/48 , C23C10/52 , C23C10/56 , C23C28/3215 , C23C28/325 , C23C28/345 , C23C28/3455 , Y02T50/67
摘要： A surface of a nickel-base article such as an internal surface of a gas turbine airfoil is protected with a donor layer of aluminum and at least one other element. To form the protective layer, a donor alloy is contacted to the protected surface of the article, and simultaneously the article and the donor alloy are heated to a coating temperature that is greater than about 0.7 of the absolute solidus temperature of the donor alloy but is such that the donor alloy remains in the form of a condensed phase contacting the protected surface of the article. The donor alloy is thereafter interdiffused into the protected surface of the article.
摘要翻译： 诸如燃气轮机翼型件的内表面的镍基制品的表面由铝的供体层和至少一个其它元件保护。 为了形成保护层，供体合金与制品的被保护表面接触，并且同时将制品和供体合金加热至比供体合金的绝对固相线温度大约0.7的涂层温度，但是 使得供体合金保持为与受保护的表面接触的凝聚相的形式。 然后，供体合金相互扩散到制品的受保护表面。
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公开(公告)号：US06869508B2
公开(公告)日：2005-03-22
申请号：US10063808
申请日：2002-05-15
申请人： Ramgopal Darolia , Reed Roeder Corderman , Joseph David Rigney , Richard Arthur Nardi, Jr. , Michael James Weimer
发明人： Ramgopal Darolia , Reed Roeder Corderman , Joseph David Rigney , Richard Arthur Nardi, Jr. , Michael James Weimer
CPC分类号： B82Y10/00 , C23C14/16 , C23C14/246 , C23C14/30
摘要： A PVD process and apparatus (120) for depositing a coating (132) from multiple sources (110, 111) of different materials. The process and apparatus (120) are particulaity intended to deposit a beta-nickel aluminide coating (132) containing one or more elements whose vapor pressures are lower than NiAl. The PVD process and apparatus (120) entail feeding at least two materials (110, 111) into a coating chamber (122) and evaporating the materials (110, 111) at different rates from separate molten pools (114, 115) thereof. Articles (130) to be coated are suspended within the coating chamber (122), and transported with a support apparatus (118) relative to the two molten pools (114, 115) so as to deposit a coating (132) with a controlled composition that is a mixture of the first and second materials (110, 111).
摘要翻译： 一种用于从不同材料的多个源（110,111）沉积涂层（132）的PVD工艺和设备（120）。 该方法和装置（120）特别用于沉积含有一种或多种蒸气压低于NiAl的元素的β-镍铝化物涂层（132）。 PVD工艺和设备（120）需要将至少两种材料（110,111）进料到涂覆室（122）中并且以与其分离的熔池（114,115）不同的速率蒸发材料（110,111）。 待涂覆的制品（130）悬浮在涂覆室（122）内，并相对于两个熔池（114,115）用支撑装置（118）运输，以便沉积具有受控组合物的涂层（132） 即第一和第二材料（110,111）的混合物。
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14.发明授权Article protected by a diffusion aluminide coating applied by painting techniques 失效用喷涂技术涂覆的扩散铝化物涂层进行保护公开(公告)号：US06676992B2
公开(公告)日：2004-01-13
申请号：US09934752
申请日：2001-08-22
申请人： Jeffrey Allan Pfaendtner , Michael James Weimer , William Evan McCormack , Joseph David Rigney , Mark Lloyd Miller , John Lewis Lackman
发明人： Jeffrey Allan Pfaendtner , Michael James Weimer , William Evan McCormack , Joseph David Rigney , Mark Lloyd Miller , John Lewis Lackman
IPC分类号： B05D302
摘要： A method for coating an article includes preparing a coating precursor paint including aluminum-containing pigment particles, a temporary organic binder comprising an acrylic, and a solvent for the temporary organic binder. The coating precursor paint is applied to a surface of the article and thereafter heated to a temperature of from about 1200° F. to about 2100° F. in a non-oxidizing environment.
摘要翻译： 一种涂布物品的方法包括制备包括含铝颜料颗粒的涂料前体涂料，包含丙烯酸的临时有机粘合剂和用于临时有机粘合剂的溶剂。 将涂层前体涂料施加到制品的表面，然后在非氧化环境中加热至约1200°F至约2100°F的温度。
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公开(公告)号：US06544665B2
公开(公告)日：2003-04-08
申请号：US09765228
申请日：2001-01-18
IPC分类号： B32B1504
CPC分类号： C23C14/083 , C23C28/321 , C23C28/3215 , C23C28/323 , C23C28/325 , C23C28/345 , C23C28/3455 , C23C30/00 , Y10T428/12549 , Y10T428/1259 , Y10T428/12618 , Y10T428/249953 , Y10T428/26 , Y10T428/268
摘要： A thermal barrier coating (TBC) for a component intended for use in a hostile environment, such as the superalloy turbine, combustor and augmentor components of a gas turbine engine. The TBC is formed to contain small amounts of alumina precipitates dispersed throughout the grain boundaries and pores of the TBC to getter oxide impurities that would otherwise allow or promote grain sintering and coarsening and pore coarsening, the consequence of which would be densification of the TBC and therefore increased thermal conductivity. If sufficiently fine, the precipitates also serve to pin the grains and pore boundaries of the TBC, the effect of which is to reduce the tendency for the microstructure of the TBC to sinter, coarsen and undergo pore redistribution, which also increase thermal conductivity of the TBC 26.
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公开(公告)号：US06492038B1
公开(公告)日：2002-12-10
申请号：US09723273
申请日：2000-11-27
IPC分类号： B32B1504
CPC分类号： C23C14/0021 , C23C8/02 , C23C14/06 , C23C28/321 , C23C28/3215 , C23C28/324 , C23C28/325 , C23C28/345 , C23C28/3455 , F01D5/288 , F05D2230/90 , F05D2300/2118 , F05D2300/226 , F05D2300/228 , F05D2300/611 , Y10T428/12576 , Y10T428/12611 , Y10T428/249953 , Y10T428/249986
摘要： A thermal barrier coating (TBC) and method for forming the coating on a component intended for use in a hostile environment. The coating and method are particularly directed to inhibiting sintering, grain coarsening/growth and pore redistribution in the coating during high temperature excursions by providing limited amounts of extremely fine carbide-based and/or nitride-based precipitates preferably formed at defects and pores at and between the grain boundaries of the TBC microstructure. The precipitates pin the TBC grain boundaries and pores during high temperature excursions, with the effect that the TBC microstructure is thermally stabilized. A coating containing the carbides and/or nitrides can be formed using a physical vapor deposition technique in an atmosphere that contains carbon and/or nitride gases or compounds thereof, or by evaporating a source material that contains carbon, carbon-containing compounds, carbides and/or nitrides.
摘要翻译： 热障涂层（TBC）以及用于在敌对环境中使用的部件上形成涂层的方法。 涂层和方法特别涉及通过提供有限量的非常细小的碳化物基和/或氮化物基沉淀物，优选在缺陷和孔处形成，并且在高温偏移期间在缺陷和孔处形成，从而抑制涂层中的烧结，晶粒粗化/生长和孔再分布 在TBC微结构的晶界之间。 沉淀物在高温偏移期间将TBC晶粒边界和孔隙固定，从而使TBC微结构热稳定。 含有碳化物和/或氮化物的涂层可以使用物理气相沉积技术在含有碳和/或氮化物气体或其化合物的气氛中或通过蒸发含有碳，含碳化合物，碳化物的源材料和 /或氮化物。
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17.发明授权公开(公告)号：US08512874B2
公开(公告)日：2013-08-20
申请号：US11757521
申请日：2007-06-04
申请人： Ramgopal Darolia , Joseph David Rigney , Gillion Herman Marijnissen , Eric Richard Irma Carolus Vergeldt , Annejan Bernard Kloosterman
发明人： Ramgopal Darolia , Joseph David Rigney , Gillion Herman Marijnissen , Eric Richard Irma Carolus Vergeldt , Annejan Bernard Kloosterman
CPC分类号： F01D5/288 , C23C4/18 , C23C10/02 , C23C10/48 , C23C10/50 , C23C10/52 , C23C28/021 , C23C28/321 , C23C28/3455 , C23C30/00 , F05D2230/90 , F05D2300/611 , Y10T428/12611 , Y10T428/12618 , Y10T428/12736 , Y10T428/12937 , Y10T428/12944 , Y10T428/12951 , Y10T428/24967 , Y10T428/264 , Y10T428/265 , Y10T428/31678
摘要： A coating and process for depositing the coating on a substrate. The coating is a nickel aluminide overlay coating of predominantly the beta (NiAl) and gamma-prime (Ni3Al) intermetallic phases, and is suitable for use as an environmental coating and as a bond coat for a thermal barrier coating (TBC). The coating can be formed by depositing nickel and aluminum in appropriate amounts to yield the desired beta+gamma prime phase content. Alternatively, nickel and aluminum can be deposited so that the aluminum content of the coating exceeds the appropriate amount to yield the desired beta+gamma prime phase content, after which the coating is heat treated to diffuse the excess aluminum from the coating into the substrate to yield the desired beta+gamma prime phase content.
摘要翻译： 用于将涂层沉积在基材上的涂层和方法。 涂层是主要是β（NiAl）和γ-prime（Ni3Al）金属间相的镀镍铝覆盖涂层，适用于环境涂层和用作热障涂层（TBC）的粘合涂层。 可以通过以适当的量沉积镍和铝来形成所述涂层，以产生所需的β+γ初相相含量。 或者，可以沉积镍和铝，使得涂层的铝含量超过适当的量以产生所需的β+γ初相相含量，之后热处理涂层以将过量的铝从涂层扩散到基底中 产生期望的β+γ'相相含量。
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18.发明授权公开(公告)号：US07326441B2
公开(公告)日：2008-02-05
申请号：US10904844
申请日：2004-12-01
申请人： Ramgopal Darolia , Joseph David Rigney , Gillion Herman Marijnissen , Eric Richard Irma Carolus Vergeldt , Annejan Bernard Kloosterman
发明人： Ramgopal Darolia , Joseph David Rigney , Gillion Herman Marijnissen , Eric Richard Irma Carolus Vergeldt , Annejan Bernard Kloosterman
IPC分类号： B05D3/02
CPC分类号： F01D5/288 , C23C4/18 , C23C10/02 , C23C10/48 , C23C10/50 , C23C10/52 , C23C28/021 , C23C28/321 , C23C28/3455 , C23C30/00 , F05D2230/90 , F05D2300/611 , Y10T428/12611 , Y10T428/12618 , Y10T428/12736 , Y10T428/12937 , Y10T428/12944 , Y10T428/12951 , Y10T428/24967 , Y10T428/264 , Y10T428/265 , Y10T428/31678
摘要： A coating and process for depositing the coating on a substrate. The coating is a nickel aluminide overlay coating of predominantly the beta (NiAl) and gamma-prime (Ni3Al) intermetallic phases, and is suitable for use as an environmental coating and as a bond coat for a thermal barrier coating (TBC). The coating can be formed by depositing nickel and aluminum in appropriate amounts to yield the desired beta+gamma prime phase content. Alternatively, nickel and aluminum can be deposited so that the aluminum content of the coating exceeds the appropriate amount to yield the desired beta+gamma prime phase content, after which the coating is heat treated to diffuse the excess aluminum from the coating into the substrate to yield the desired beta+gamma prime phase content.
摘要翻译： 用于将涂层沉积在基材上的涂层和方法。 涂层是主要是β（NiAl）和γ-prime（Ni 3 Al 3 Al）金属间相的镍铝化物覆盖涂层，并且适合用作环境涂层和作为粘合涂层 隔热涂层（TBC）。 可以通过以适当的量沉积镍和铝来形成所述涂层，以产生所需的β+γ初相相含量。 或者，可以沉积镍和铝，使得涂层的铝含量超过适当的量以产生所需的β+γ初相相含量，之后热处理涂层以将过量的铝从涂层扩散到基底中 产生期望的β+γ'相相含量。
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公开(公告)号：US07244467B2
公开(公告)日：2007-07-17
申请号：US10604368
申请日：2003-07-15
IPC分类号： C23C16/00
CPC分类号： C23C14/5886 , C23C4/18 , C23C14/16 , C23C26/00 , C23C28/3215 , C23C28/345 , C23C28/3455
摘要： A process for forming a beta-phase nickel aluminide (NiAl) overlay coating that is suitable for use as a bond coat for a thermal barrier coating (TBC). The overlay coating is deposited by a method that produces a generally columnar grain structure in which grains extend through the coating such that at least some grain boundaries are open at the coating surface. The coating is then peened with a particulate media, followed by heating the overlay coating to a temperature sufficient to cause the overlay coating to recrystallize and form new grain boundaries that are not open to the outer surface of the coating and significantly less susceptible to accelerated oxidation than the original grain boundaries. The particulate media is formed of a composition containing nickel and aluminum, such that an oxide scale that forms on the surface of the coating after the peening operation is substantially free of deleterious oxide compounds, notably iron-containing spinels.
摘要翻译： 用于形成适合用作热障涂层（TBC）的粘合涂层的β-相镍铝化物（NiAl）覆盖涂层的方法。 覆盖涂层通过产生大致柱状晶粒结构的方法沉积，其中晶粒延伸穿过涂层，使得至少一些晶界在涂层表面开口。 然后用颗粒介质对涂层进行喷丸处理，然后将覆盖涂层加热至足以使覆盖涂层再结晶并形成不对涂层外表面开放的新晶粒边界，并显着降低易受加速氧化影响的温度 比原来的晶界。 颗粒介质由包含镍和铝的组合物形成，使得在喷丸操作之后在涂层表面上形成的氧化皮基本上不含有害氧化物化合物，特别是含铁尖晶石。
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公开(公告)号：US07163718B2
公开(公告)日：2007-01-16
申请号：US10685637
申请日：2003-10-15
IPC分类号： C23C16/00
CPC分类号： C23C10/06 , C23C10/02 , C23C10/14 , Y02T50/67 , Y10T428/12736
摘要： A process for forming diffusion aluminide coatings on an uncoated surface of a substrate, without interdiffusing a sufficient amount of aluminum into a coating layer to adversely affect the coating growth potential and mechanical properties of said coating layer. A metal substrate is provided comprising an external surface and an internal passage therein defined by an internal surface, at least a portion of the external surface of the substrate being coated with a coating layer selected from the group consisting of β-NiAl-base, MCrAlX, a line-of-sight diffusion aluminide, a non-line-of-sight diffusion aluminide, a pack diffusion aluminide, and a slurry diffusion aluminide on said substrate. The metal substrate is subjected to an aluminum vapor phase deposition process.
摘要翻译： 在基底的未涂覆表面上形成扩散铝化物涂层的方法，而不会将足够量的铝相互扩散到涂层中，从而不利地影响涂层生长电位和所述涂层的机械性能。 提供了一种金属基底，其包括由内表面限定的外表面和内部通道，所述基底的外表面的至少一部分被涂覆有选自β-NiAl基，MCrAlX ，视线扩散铝化物，非视线扩散铝化物，包层扩散铝化物和在所述衬底上的浆料扩散铝化物。 金属基板经受铝气相沉积工艺。
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