公开(公告)号：US20090152504A1

公开(公告)日：2009-06-18

申请号：US12223869

申请日：2007-12-27

申请人： Katsuhiko Komuro ,  Masahiko Ito ,  Daisuke Masuko

发明人： Katsuhiko Komuro ,  Masahiko Ito ,  Daisuke Masuko

IPC分类号： C07F5/06 ,  C08L71/02 ,  H01B1/12

CPC分类号： C08L71/00 ,  C07F7/21 ,  C08G59/70 ,  C08G2650/56 ,  C08J3/241 ,  H05K3/323

摘要： An aluminum chelate-based latent curing agent is provided which can cure a thermosetting epoxy resin at a relatively low temperature in a short period of time. A method for producing such an aluminum chelate-based latent curing agent, whose curing conditions can be relatively easily controlled, is also provided. The aluminum chelate-based latent curing agent is made latent by reacting a silsesquioxane-type oxetane derivative with an aluminum chelating agent in the presence of an alicyclic epoxy compound.

摘要翻译： 提供了一种铝螯合物潜固​​化剂，其可在短时间内以相对较低的温度固化热固性环氧树脂。 还提供了一种可以相对容易地控制其固化条件的这种基于铝螯合物的潜在性固化剂的制造方法。 通过在脂环族环氧化合物的存在下使倍半硅氧烷型氧杂环丁烷衍生物与铝螯合剂反应，使铝螯合物系潜在性固化剂成为潜在的。

公开(公告)号：US20080249257A1

公开(公告)日：2008-10-09

申请号：US12078156

申请日：2008-03-27

申请人： Daisuke Masuko ,  Katsuhiko Komuro ,  Masahiko Ito ,  Tadasu Kawashima

发明人： Daisuke Masuko ,  Katsuhiko Komuro ,  Masahiko Ito ,  Tadasu Kawashima

IPC分类号： C08G18/58

CPC分类号： C08G18/6484 ,  C08G18/7664 ,  C08G18/7671 ,  H05K3/323

摘要： A latent epoxy resin curing agent is provided which can be manufactured without using an amphiphilic polymer compound requiring a painful trial and error selection process, exhibits excellent solvent resistance and low-temperature fast-curing ability, and contains an imidazole-based compound as a main component. In the latent epoxy resin curing agent containing the imidazole-based compound as a main component, adduct particles formed through adduct reaction of an epoxy-based compound with the particulate imidazole-based compound are coated with an ethyl cellulose film. Furthermore, the surfaces of the adduct particles may be crosslinked with a polyfunctional isocyanate compound. A mixture of the epoxy-based compound, the particulate imidazole-based compound, and ethyl cellulose in a predetermined saturated hydrocarbon-based solvent is heated under stirring. Then, the epoxy-based compound and the particulate imidazole-based compound are subjected to adduct reaction to give a slurry of the adduct. After the slurry is cooled, the latent epoxy resin curing agent is filtrated. If necessary, the ethyl cellulose film is crosslinked with a polyfunctional isocyanate compound.

摘要翻译： 提供一种潜在的环氧树脂固化剂，其可以在不需要使用痛苦的试错误选择方法的两亲性聚合物化合物的情况下制造，显示出优异的耐溶剂性和低温快速固化能力，并且含有咪唑类化合物作为主要 零件。 在含有咪唑类化合物作为主要成分的潜在环氧树脂固化剂中，通过环氧类化合物与微粒状咪唑类化合物的加成反应而形成的加合物粒子被乙基纤维素膜包覆。 此外，加合物颗粒的表面可以与多官能异氰酸酯化合物交联。 在预定的饱和烃类溶剂中将环氧类化合物，微粒状咪唑类化合物和乙基纤维素的混合物在搅拌下加热。 然后，将环氧类化合物和微粒状咪唑类化合物进行加合反应，得到加合物的淤浆。 在浆液冷却后，过氧化潜在的环氧树脂固化剂。 如果需要，乙基纤维素膜与多官能异氰酸酯化合物交联。