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公开(公告)号：US20100209696A1
公开(公告)日：2010-08-19
申请号：US12370910
申请日：2009-02-13
申请人： Roland D. Seals , Paul A. Menchhofer , Jane Y. Howe , Wei Wang
发明人： Roland D. Seals , Paul A. Menchhofer , Jane Y. Howe , Wei Wang
CPC分类号： B01J2/006 , B01J21/08 , B01J23/745 , B01J31/0274 , B01J35/0013 , B01J35/006 , B01J37/0207 , B01J37/0209 , B01J37/033 , B01J37/18 , B22F1/025 , B82Y30/00 , B82Y40/00 , C01B32/15 , Y10T428/12181 , Y10T428/25 , Y10T428/2991 , Y10T428/2993
摘要： Anchored nanostructure materials and methods for their fabrication are described. The anchored nanostructure materials may utilize nano-catalysts that include powder-based or solid-based support materials. The support material may comprise metal, such as NiAl, ceramic, a cermet, or silicon or other metalloid. Typically, nanoparticles are disposed adjacent a surface of the support material. Nanostructures may be formed as anchored to nanoparticles that are adjacent the surface of the support material by heating the nano-catalysts and then exposing the nano-catalysts to an organic vapor. The nanostructures are typically single wall or multi-wall carbon nanotubes.
摘要翻译： 描述了锚定的纳米结构材料及其制造方法。 锚定的纳米结构材料可以使用包括基于粉末或固体的支撑材料的纳米催化剂。 载体材料可以包括金属，例如NiAl，陶瓷，金属陶瓷或硅或其它准金属。 通常，纳米颗粒邻近支撑材料的表面设置。 纳米结构可以通过加热纳米催化剂然后将纳米催化剂暴露于有机蒸气而形成为锚定到邻近载体材料表面的纳米颗粒。 纳米结构通常是单壁或多壁碳纳米管。
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公开(公告)号：US08052951B2
公开(公告)日：2011-11-08
申请号：US12417887
申请日：2009-04-03
IPC分类号： D01F9/12
CPC分类号： D01F9/1277 , B82Y30/00 , B82Y40/00 , C01B32/16 , C01B32/162 , Y10S977/742 , Y10S977/842 , Y10T428/30 , Y10T428/31678
摘要： Disclosed are structures formed as bulk support media having carbon nanotubes formed therewith. The bulk support media may comprise fibers or particles and the fibers or particles may be formed from such materials as quartz, carbon, or activated carbon. Metal catalyst species are formed adjacent the surfaces of the bulk support material, and carbon nanotubes are grown adjacent the surfaces of the metal catalyst species. Methods employ metal salt solutions that may comprise iron salts such as iron chloride, aluminum salts such as aluminum chloride, or nickel salts such as nickel chloride. Carbon nanotubes may be separated from the carbon-based bulk support media and the metal catalyst species by using concentrated acids to oxidize the carbon-based bulk support media and the metal catalyst species.
摘要翻译： 公开了形成为具有由其形成的碳纳米管的本体支撑介质的结构。 本体支撑介质可以包括纤维或颗粒，并且纤维或颗粒可以由诸如石英，碳或活性炭的材料形成。 在本体支撑材料的表面附近形成金属催化剂种类，并且在金属催化剂种类的表面附近生长碳纳米管。 方法采用金属盐溶液，其可以包括铁盐如氯化铁，铝盐如氯化铝，或镍盐如氯化镍。 碳纳米管可以通过使用浓缩酸来氧化碳基本体载体介质和金属催化剂种类而从碳基体积载体介质和金属催化剂种类中分离出来。
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公开(公告)号：US20130195708A1
公开(公告)日：2013-08-01
申请号：US13528929
申请日：2012-06-21
CPC分类号： C22C32/0084 , B22F3/14
摘要： A metal-bonded graphite foam composite includes a ductile metal continuous phase and a dispersed phase that includes graphite foam particles.
摘要翻译： 金属粘结石墨泡沫复合材料包括延性金属连续相和包括石墨泡沫颗粒的分散相。
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公开(公告)号：US20100254885A1
公开(公告)日：2010-10-07
申请号：US12417887
申请日：2009-04-03
CPC分类号： D01F9/1277 , B82Y30/00 , B82Y40/00 , C01B32/16 , C01B32/162 , Y10S977/742 , Y10S977/842 , Y10T428/30 , Y10T428/31678
摘要： Disclosed are structures formed as bulk support media having carbon nanotubes formed therewith. The bulk support media may comprise fibers or particles and the fibers or particles may be formed from such materials as quartz, carbon, or activated carbon. Metal catalyst species are formed adjacent the surfaces of the bulk support material, and carbon nanotubes are grown adjacent the surfaces of the metal catalyst species. Methods employ metal salt solutions that may comprise iron salts such as iron chloride, aluminum salts such as aluminum chloride, or nickel salts such as nickel chloride. Carbon nanotubes may be separated from the carbon-based bulk support media and the metal catalyst species by using concentrated acids to oxidize the carbon-based bulk support media and the metal catalyst species.
摘要翻译： 公开了形成为具有由其形成的碳纳米管的本体支撑介质的结构。 本体支撑介质可以包括纤维或颗粒，并且纤维或颗粒可以由诸如石英，碳或活性炭的材料形成。 在本体支撑材料的表面附近形成金属催化剂种类，并且在金属催化剂种类的表面附近生长碳纳米管。 方法采用金属盐溶液，其可以包括铁盐如氯化铁，铝盐如氯化铝，或镍盐如氯化镍。 碳纳米管可以通过使用浓缩酸来氧化碳基本体载体介质和金属催化剂种类而从碳基本体载体介质和金属催化剂种类分离。
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公开(公告)号：US06375877B2
公开(公告)日：2002-04-23
申请号：US09842375
申请日：2001-04-24
IPC分类号： B29C6500
CPC分类号： B28B1/008 , B22F7/06 , B22F2999/00 , B28B1/00 , C04B35/117 , B22F2207/01 , B22F3/22
摘要： A gelcasting method of making an internally graded article alternatively includes the steps of: preparing a slurry including a least two different phases suspended in a gelcasting solution, the phases characterized by having different settling characteristics; casting the slurry into a mold having a selected shape; allowing the slurry to stand for a sufficient period of time to permit desired gravitational fractionation in order to achieve a vertical compositional gradient in the molded slurry; gelling the slurry to form a solid gel while preserving the vertical compositional gradient in the molded slurry; drying the gel to form a dried green body; and sintering the dry green body to form a solid object, at least one property thereof varying along the vertical direction because of the compositional gradient in the molded slurry.
摘要翻译： 制备内部分级制品的凝胶浇铸方法交替包括以下步骤：制备包含悬浮在凝胶浇注溶液中的至少两个不同相的浆料，其特征在于具有不同的沉降特性; 将浆料浇注到具有选定形状的模具中; 允许浆料静置足够的时间以允许所需的重力分馏，以便在模制浆料中达到垂直组分梯度; 将浆料胶凝以形成固体凝胶，同时保持模制浆料中的垂直组分梯度; 干燥凝胶以形成干燥的生坯; 并且将干燥的生坯烧结以形成固体物体，由于模制浆料中的组成梯度，其至少一种特性沿垂直方向变化。
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公开(公告)号：US09017598B2
公开(公告)日：2015-04-28
申请号：US13528929
申请日：2012-06-21
申请人： Paul A. Menchhofer , James W. Klett
发明人： Paul A. Menchhofer , James W. Klett
CPC分类号： C22C32/0084 , B22F3/14
摘要： A metal-bonded graphite foam composite includes a ductile metal continuous phase and a dispersed phase that includes graphite foam particles.
摘要翻译： 金属粘结石墨泡沫复合材料包括延性金属连续相和包括石墨泡沫颗粒的分散相。
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公开(公告)号：US5476622A
公开(公告)日：1995-12-19
申请号：US898914
申请日：1992-06-12
IPC分类号： B28B3/20 , B29C47/88 , B30B11/22 , C04B35/622 , C04B35/64
CPC分类号： B29C47/8805 , B28B3/20 , B29C47/0016 , B29C47/0019 , B29C47/0023 , B29C47/0028 , B29C47/003 , B30B11/22 , C04B35/622 , B29K2101/10 , B29K2503/00
摘要： A method and apparatus for the production of articles made of a particle-based material; e.g., ceramics and sintered metals. In accordance with the invention, a thermally settable slurry containing a relatively high concentration of the particles is conveyed through an elongate flow area having a desired cross-sectional configuration. The slurry is heated as it is advanced through the flow area causing the slurry to set or harden in a shape which conforms to the cross-sectional configuration of the flow area. The material discharges from the flow area as a self-supporting solid of near net final dimensions. The article may then be sintered to consolidate the particles and provide a high density product.
摘要翻译： 一种用于生产由颗粒基材料制成的制品的方法和装置; 例如陶瓷和烧结金属。 根据本发明，含有相对高浓度颗粒的热固性浆料通过具有所需横截面构型的细长流动区域输送。 浆料在其通过流动区域前进时被加热，使得浆料固化或硬化成符合流动区域的横截面构造的形状。 材料从流动区域排放为近净最终尺寸的自支撑固体。 然后可以将制品烧结以固结颗粒并提供高密度产品。
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18.发明申请CARBON NANOTUBE (CNT)-ENHANCED PRECURSOR FOR CARBON FIBER PRODUCTION AND METHOD OF MAKING A CNT-ENHANCED CONTINUOUS LIGNIN FIBER 审中-公开用于碳纤维生产的碳纳米管（CNT） - 增强前体和制备CNT增强的连续纤维的方法公开(公告)号：US20110285049A1
公开(公告)日：2011-11-24
申请号：US12783288
申请日：2010-05-19
CPC分类号： H01B1/24 , B29C48/05 , B29C48/30 , B29C48/345 , B29C48/387 , B29C48/395 , B29C2791/005 , B29L2031/731 , D01F1/09 , D01F9/17
摘要： A precursor for carbon fiber production comprises a continuous lignin fiber including carbon nanotubes dispersed therein at a concentration of about 10 wt. % or less. A method of melt-spinning a continuous lignin fiber includes preparing a melt comprising molten lignin and a plurality of carbon nanotubes, and extruding the melt through a spinneret to form a continuous lignin fiber having the carbon nanotubes dispersed therein.
摘要翻译： 用于碳纤维生产的前体包括以约10重量％的浓度分散在其中的包含碳纳米管的连续木质素纤维。 ％ 或更少。 熔融纺丝连续木质素纤维的方法包括制备包含熔融木质素和多个碳纳米管的熔体，并通过喷丝头挤出熔体以形成其中分散有碳纳米管的连续的木质素纤维。
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公开(公告)号：US06248286B1
公开(公告)日：2001-06-19
申请号：US09453774
申请日：1999-12-03
IPC分类号： B28B114
CPC分类号： B28B1/008 , B22F7/06 , B22F2999/00 , B28B1/00 , C04B35/117 , B22F2207/01 , B22F3/22
摘要： A gelcasting method of making an internally graded article includes the steps of: preparing at least two slurries, each of the slurries including a different gelcastable powder suspended in a gelcasting solution, the slurries characterized by having comparable shrinkage upon drying and sintering thereof; casting the slurries into a mold having a selected shape, wherein relative proportions of the slurries is varied in at least one direction within the selected shape; gelling the slurries to form a solid gel while preserving the variation in relative proportions of the slurries; drying the gel to form a dried green body; and sintering the dry green body to form a solid object, at least one property thereof varying because of the variation in relative proportions of the starting slurries. A gelcasting method of making an internally graded article alternatively includes the steps of: preparing a slurry including a least two different phases suspended in a gelcasting solution, the phases characterized by having different settling characteristics; casting the slurry into a mold having a selected shape; allowing the slurry to stand for a sufficient period of time to permit desired gravitational fractionation in order to achieve a vertical compositional gradient in the molded slurry; gelling the slurry to form a solid gel while preserving the vertical compositional gradient in the molded slurry; drying the gel to form a dried green body; and sintering the dry green body to form a solid object, at least one property thereof varying along the vertical direction because of the compositional gradient in the molded slurry.
摘要翻译： 制备内部分级制品的凝胶浇铸方法包括以下步骤：制备至少两种浆料，每种浆料包括悬浮在凝胶浇注溶液中的不同的可凝胶涂覆粉末，其特征在于其干燥和烧结时具有相当的收缩率; 将浆料浇铸到具有选定形状的模具中，其中浆料的相对比例在所选形状内的至少一个方向上变化; 胶凝形成固体凝胶，同时保持浆料相对比例的变化; 干燥凝胶以形成干燥的生坯; 并且将干燥的生坯烧结以形成固体物体，由于起始浆料的相对比例的变化，其至少一种性质变化。 制备内部分级制品的凝胶浇铸方法交替包括以下步骤：制备包含悬浮在凝胶浇注溶液中的至少两个不同相的浆料，其特征在于具有不同的沉降特性; 将浆料浇注到具有选定形状的模具中; 允许浆料静置足够的时间以允许所需的重力分馏，以便在模制浆料中达到垂直组分梯度; 将浆料胶凝以形成固体凝胶，同时保持模制浆料中的垂直组分梯度; 干燥凝胶以形成干燥的生坯; 并且将干燥的生坯烧结以形成固体物体，由于模制浆料中的组成梯度，其至少一种特性沿垂直方向变化。
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