摘要:
A method for producing a colored resin particle dispersion liquid comprises: polycondensing a polyester-forming monomer in a nonaqueous solvent to produce an unsaturated polyester; graft-polymerizing an ethylenic unsaturated monomer to the unsaturated polyester in a nonaqueous solvent to produce a modified polyester resin; and dispersing a colorant and the modified polyester resin to produce a colored resin particle dispersion liquid, the polycondensing and the graft-polymerizing being carried out at a temperature of 150° C. or less.
摘要:
A toner for developing an electrostatic image comprises: a binder resin; and a releasing agent, wherein the binder resin comprises a polycondensation resin obtained by polycondensing a polycondensation monomer in the presence of a polycondensation catalyst, the releasing agent comprises a condensation compound obtained by condensing a condensation monomer in the presence of a condensation catalyst, the toner contains a metallic element derived from the polycondensation catalyst and the condensation catalyst in an amount of from 0 to 10 ppm, and the toner contains a sulfur component in an amount of from 100 to 20,000 ppm.
摘要:
A Brønsted acid is a compound represented by formula (I): wherein n represents an integer of from 1 to 4, RHL('s) each independently represents Cl or F, and R1 represents an alkyl group having from 8 to 20 carbon atoms.
摘要:
An image forming method, which comprises: forming an electrostatic latent image on a surface of a latent image supporting member; developing the electrostatic latent image formed on the surface of the latent image supporting member with a toner for developing an electrostatic latent image or an electrostatic latent image developer containing the toner and a carrier to form a toner image; transferring the toner image formed on the surface of the latent image supporting member onto a surface of a transfer receiving material; and fixing the toner image transferred onto the transfer receiving material under pressure, wherein the toner comprises a block copolymer having a crystalline polyester block and a non-crystalline polyester block, and wherein a maximum pressure applied when the image is fixed is 1 MPa or greater but not greater than 10 MPa.
摘要:
A binder resin for an electrostatic image developing toner is obtained by a polycondensation reaction of a polycarboxylic acid and a polyol, wherein the polycarboxylic acid includes a compound represented by at least one of formula (1) and formula (2) as defined in the specification in an amount of from about 50 to about 100 mol %; the polyol includes a compound represented by formula (3) as defined in the specification in an amount of from about 10 to about 100 mol %; and a content of a catalyst-originated metal element in the binder resin is about 100 ppm or less. R1OOCA1mB1nA1lCOOR1′ (1) R2OOCA2pB2qA2rCOOR2′ (2) HOXh—Ph—Y—Ph—XkOH (3)
摘要:
A method of producing a toner for developing electrostatic charge image, the method comprising: aggregating particles containing a crystalline polyester resin, particles containing a non-crystalline polyester resin and particles of a releasing agent in an aqueous medium, so as to form aggregated particles; and heating the aggregated particles to fuse into a coalescent body, wherein at least one of the crystalline polyester resin and the non-crystalline polyester resin is obtained by polymerization at temperatures not higher than 150° C. with a Bronsted acid containing a sulfur atom as a catalyst, and wherein a first onset temperature A(° C.) of the toner and a glass transition temperature B(° C.) of the non-crystalline polyester resin as measured by differential scanning calorimeter satisfy a relation (B−A)≦10, and wherein a weight average molecular weight of the crystalline polyester resin is ½ or lower of a weight average molecular weight of the non-crystalline polyester resin.
摘要:
A process for producing a resin particle liquid dispersion for an electrostatic image developing toner, the process comprising: polycondensing a polycondensable monomer by utilizing an acid having a surface activating effect as a polycondensation catalyst, so as to obtain a polycondensed resin; and dispersing the polycondensed resin in an aqueous medium to which a base is added, so as to obtain a resin particle liquid dispersion in which a median diameter of resin particles is from 0.05 to 2.0 μm, or the process comprising: polycondensing a polycondensable monomer by utilizing an acid having a surface activating effect as a polycondensation catalyst in a co-presence of a polycondensed resin, so as to obtain a polycondensed resin-containing material; and dispersing the polycondensed resin-containing material in an aqueous medium, so as to obtain a resin particle liquid dispersion in which a median diameter of resin particles is from 0.05 to 2.0 μm.
摘要:
Methods and compositions including a compound represented by formula (I): wherein n represents an integer of from 1 to 4, RHL('s) each independently represents Cl or F, and R1 represents an alkyl group having from 8 to 20 carbon atoms.
摘要:
A method for producing a binder resin comprises polycondensing a polycondensable monomer by using a polycondensation catalyst that comprises: at least one of compounds of formula (I) or (II); and at least one of compounds represented of formula (III) or (IV), wherein weight ratio of total amount of the compounds of formula (I) or (II) to total amount of the compounds of formula (III) or (IV) is from 5:95 to 95:5: wherein R1 represents a C8-C20 straight-chain alkyl group; R2 represents a monovalent organic group; and number n of substituents R2 represents an integer of from 0 to 4; R3—SO3H (II) wherein R3 represents a C8-C20 straight-chain alkyl group; wherein R4 represents a C8-C20 branched alkyl group; R5 represents a monovalent organic group; and number m of substituents R5 represents an integer of from 0 to 4; and R6—SO3H (IV) wherein R6 represents a C8-C20 branched alkyl group.
摘要:
A resin particle dispersion liquid comprises: resin particles comprising polyester having terminal carboxyl groups, the polyester being obtained by polycondensation of a polycondensable monomer, wherein the polyester has the terminal carboxyl groups that are partially neutralized to form carboxyl anions, the resin particles in the resin particle dispersion liquid having a value of (da/(da+dc)) of from approximately 0.30 to approximately 0.90, when in an absorption spectrum of the resin particles measured with an infrared spectrometer, dc represents a peak intensity of the terminal carboxyl group in a range of from 1,780 to 1,680 cm−1, and da represents a peak intensity of the neutralized carboxyl anion in a range of from 1,670 to 1,550 cm−1, the polyester has an acid value of approximately 1 mg·KOH/g or more and less than approximately 15 mg·KOH/g before neutralization, the resin particles dispersion liquid comprises a divalent or higher organic acid in an amount of from approximately 0.1 to approximately 20 parts by weight per 100 parts by weight of the resin particles, and the resin particles have a median diameter of from approximately 0.1 to approximately 2.0 μm.