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21.发明授权Process for separating acrylic acid present as a main constituent and glyoxal present as a by-product in a product gas mixture of a partial heterogeneously catalyzed gas phase oxidation of a C3 precursor compound of acrylic acid 有权用于分离作为主要成分存在的丙烯酸和乙二醛作为副产物存在于丙烯酸的C3前体化合物的部分非均相催化气相氧化的产物气体混合物中公开(公告)号：US08299299B2
公开(公告)日：2012-10-30
申请号：US12509078
申请日：2009-07-24
申请人： Till Blum , Peter Zurowski , Steffen Rissel , Sylke Haremza , Thorsten Friese , Ulrich Jaeger , Volker Schliephake , Klaus Joachim Mueller-Engel , Ulrich Hammon , Joerg Heilek , Imke Britta Mueller
发明人： Till Blum , Peter Zurowski , Steffen Rissel , Sylke Haremza , Thorsten Friese , Ulrich Jaeger , Volker Schliephake , Klaus Joachim Mueller-Engel , Ulrich Hammon , Joerg Heilek , Imke Britta Mueller
IPC分类号： C07C51/42
CPC分类号： C07C51/252 , C07C51/43 , C07C57/04
摘要： A process for separating acrylic acid present as a main product and glyoxal present as a by-product in a product gas mixture of a partial gas phase oxidation of a C3 precursor compound, in which a liquid phase P is obtained, which consists of acrylic acid to an extent of at least 70% of its weight and, based on the molar amount of acrylic acid present therein, comprises at least 200 molar ppm of glyoxal, in which the glyoxal is separated from the acrylic acid in the liquid phase P by crystallization.
摘要翻译： 将作为主要成分存在的丙烯酸和作为副产物存在的乙二醛的方法分离在得到液相P的C3前体化合物的部分气相氧化的产物气体混合物中，该混合物由丙烯酸 至少其重量的70％的程度，并且基于其中存在的丙烯酸的摩尔量，包含至少200摩尔ppm的乙二醛，其中通过结晶将乙二醛与液相P中的丙烯酸分离 。
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22.发明授权Process for operating a continuous removal of a target product X in the form of fine crystals 有权用于以细晶体的形式连续移除靶产物X的方法公开(公告)号：US07732624B2
公开(公告)日：2010-06-08
申请号：US12208737
申请日：2008-09-11
申请人： Joerg Heilek , Ulrich Hammon , Klaus Joachim Mueller-Engel , Volker Schliephake , Dieter Baumann
发明人： Joerg Heilek , Ulrich Hammon , Klaus Joachim Mueller-Engel , Volker Schliephake , Dieter Baumann
IPC分类号： C07D207/26 , C07C51/43 , C07C7/14
CPC分类号： B01D9/0013 , B01D9/004 , B01D9/005 , B01D9/0063 , C07C7/14 , C07C51/43 , C07C15/08 , C07C57/04
摘要： A process for continuously removing a target product X in the form of fine crystals from a liquid phase P comprising the target product X and constituents other than the target product X by cooling suspension crystallization in an indirect heat transferer, in which the crystal suspension formed is conducted out of the heat transferer first into a mixed buffer tank and, from there, fed to an apparatus for separating the crystal suspension into crystals and liquid phase, and wherein external measures dissipade the oversaturation of the crystal suspension fed to the buffer vessel with target product X.
摘要翻译： 通过在间接热转移体中冷却悬浮液结晶，从包含目标产物X和除了目标产物X的成分的液相P连续除去目标产物X的形式的方法，其中形成的晶体悬浮液为 首先从热转移器中导出到混合缓冲罐中，从那里进料到用于将晶体悬浮液分离成晶体和液相的装置，并且其中外部措施消除了用目标物供给缓冲容器的晶体悬浮液的过饱和 产品X.
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23.发明授权Method of charging catalyst tubes of a bundle of catalyst tubes in a structured fashion 有权以结构化方式对催化剂管束的催化剂管进行充电的方法公开(公告)号：US07731916B2
公开(公告)日：2010-06-08
申请号：US11118433
申请日：2005-05-02
IPC分类号： B65B1/04
CPC分类号： B01J8/0015 , B01J8/003 , B01J8/06 , B01J8/067 , B01J23/002 , B01J23/8885 , B01J35/0006 , B01J35/026 , B01J2208/00212 , B01J2208/00752 , B01J2208/00814 , B01J2208/025 , B01J2523/00 , B01J2523/13 , B01J2523/41 , B01J2523/54 , B01J2523/68 , B01J2523/69 , B01J2523/842 , B01J2523/845
摘要： A method of charging catalyst tubes of a bundle of catalyst tubes in a structured fashion, in which uniformly predispensed portions of formulations of shaped catalyst bodies are used for producing a section of charge.
摘要翻译： 以结构方式装载一束催化剂管的催化剂管的方法，其中使用成形催化剂体的制剂的均匀预分配部分来产生一部分电荷。
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24.发明申请PROCESS FOR STORING A MONOMER PHASE WHICH IS LIQUID UNDER THE CONDITIONS OF STORAGE 有权存储根据存储条件液化的单体相的过程公开(公告)号：US20090221780A1
公开(公告)日：2009-09-03
申请号：US12053268
申请日：2008-03-21
CPC分类号： C07C67/48 , C07C45/79 , C07C51/42 , C07C51/47 , C07C51/50 , C07C67/56 , Y10T137/0391 , Y10T137/6579 , C07C57/04 , C07C69/54 , C07C47/22
摘要： A process for storing a monomer phase which is liquid under the conditions of storage and comprises methacrylic monomers to an extent of ≧95% by weight and has been obtained by condensation out of a gaseous phase or by melting a crystalline phase, in a storage vessel, in which polymer of the monomer present in dissolved form in the liquid monomer phase is removed therefrom on the route from its generation into the storage vessel, and also a process for withdrawing liquid monomer phase from the storage vessel in which polymer of the monomer present in dissolved form in the monomer phase is likewise removed.
摘要翻译： 一种在储存条件下储存液体的单体相的方法，其包含甲基丙烯酸单体至> 95重量％的程度，并且通过在气相中冷凝或熔融结晶相获得， 容器，其中以其溶解形式存在于液体单体相中的单体的聚合物在其从其产生进入储存容器的路线上被除去，以及从存储容器中抽出液体单体相的方法，其中单体的聚合物 在单体相中以溶解形式存在，同样地被除去。
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公开(公告)号：US07566804B2
公开(公告)日：2009-07-28
申请号：US12020264
申请日：2008-01-25
摘要： A process for preparing acrylic acid, in which an acrylic acid-comprising product gas mixture obtained by catalytic gas phase partial oxidation of a C3 precursor of acrylic acid is fractionally condensed in a condensation column provided with internals ascending into itself with side draw removal of crude acrylic acid and with liquid phase draw removal of acrylic acid-comprising acid water, and acrylic acid present in acid water is taken up into an extractant and then removed from the extractant and recycled into the condensation column, or taken up in aqueous metal hydroxide, or sent to further purification of the crude acrylic acid.
摘要翻译： 制备丙烯酸的方法，其中通过丙烯酸的C3前体的催化气相部分氧化获得的含丙烯酸的产物气体混合物在冷凝塔中分级冷凝，所述内部装有自身上升的侧向抽出粗品 丙烯酸和含丙烯酸的酸性水的液相萃取和酸性水中存在的丙烯酸被吸收到萃取剂中，然后从萃取剂中除去并循环到冷凝柱中，或者被吸收在金属氢氧化物水溶液中， 或者进一步纯化粗丙烯酸。
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26.发明授权Operation of a continuous heterogeneously catalyzed gas phase partial oxidation of at least one organic compound 有权操作至少一种有机化合物的连续不均匀催化气相部分氧化公开(公告)号：US07196217B2
公开(公告)日：2007-03-27
申请号：US10912075
申请日：2004-08-06
IPC分类号： C07C51/235 , C07C51/16
CPC分类号： C07C45/33 , C07C45/35 , C07C51/252 , C07C47/22 , C07C57/04
摘要： Process for operating a continuous heterogeneously catalyzed gas phase partial oxidation of at least one organic compound using compressed air as the oxygen source which is filtered before its compression.
摘要翻译： 使用压缩空气作为在其压缩之前被过滤的氧源来操作至少一种有机化合物的连续非均相催化气相部分氧化的方法。
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27.发明授权Safe operation of a continuous heterogeneously catalyzed gas-phase partial oxidation of at least one organic compound 有权至少一种有机化合物的连续不均匀催化气相部分氧化的安全操作公开(公告)号：US07074955B2
公开(公告)日：2006-07-11
申请号：US10459782
申请日：2003-06-12
申请人： Ulrich Hammon , Jochen Meschke , Ulrich Rauh , Klaus Joachim Müller-Engel , Peter Schlemmer , Volker Schliephake
发明人： Ulrich Hammon , Jochen Meschke , Ulrich Rauh , Klaus Joachim Müller-Engel , Peter Schlemmer , Volker Schliephake
IPC分类号： C07C51/16
CPC分类号： C07C51/215 , C07C45/33 , C07C45/34 , C07C45/35 , C07C51/252 , C07C47/22 , C07C57/04
摘要： A continuously operated heterogeneously catalyzed gas-phase partial oxidation of at least one organic compound in an oxidation reactor is operated safely by a process in which an explosion diagram for the feed gas mixture is deposited as the basis of a cut-out mechanism in a computer.
摘要翻译： 在氧化反应器中连续操作的至少一种有机化合物的气相部分氧化被安全地通过其中沉积原料气体混合物的爆炸图作为计算机中的切断机构的基础的方法来操作 。
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公开(公告)号：US20060131766A1
公开(公告)日：2006-06-22
申请号：US11302206
申请日：2005-12-14
申请人： Armin Diefenbacher , Ulrich Hammon , Thomas Walter , Bruno Seider , Wolfgang Schneider , Bernd Gerber , Volker Schliephake , Michael Blechschmitt
发明人： Armin Diefenbacher , Ulrich Hammon , Thomas Walter , Bruno Seider , Wolfgang Schneider , Bernd Gerber , Volker Schliephake , Michael Blechschmitt
IPC分类号： B01F3/04
CPC分类号： B01D3/326
摘要： A tray column is proposed which comprises column trays, two or more supports which are arranged on the underside of the column trays and support them and a bearing ring for the column trays on the inner wall of the tray column, wherein three-way joints of inner column wall, bearing ring and support are prevented by cutouts in the bearing ring.
摘要翻译： 提出了一种托盘塔，其包括柱托盘，两个或更多个支撑件，其布置在塔托盘的下侧并支撑它们，并且托盘托架的内壁上的托盘的轴承环，其中三通关节 内柱壁，轴承圈和支撑件通过轴承圈中的切口防止。
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29.发明授权Preparation of at least one organic compound by heterogeneously catalyzed partial gas-phase oxidation 有权通过非均相催化的部分气相氧化制备至少一种有机化合物公开(公告)号：US06958414B2
公开(公告)日：2005-10-25
申请号：US10667782
申请日：2003-09-23
申请人： Volker Schliephake , Ulrich Hammon , Ernst Lang , Carl-Ludwig Krüger , Jürgen Schröder , Klaus Joachim Müller-Engel
发明人： Volker Schliephake , Ulrich Hammon , Ernst Lang , Carl-Ludwig Krüger , Jürgen Schröder , Klaus Joachim Müller-Engel
IPC分类号： C07C51/25 , C07C253/26 , C07C255/08 , C07C51/16
CPC分类号： C07C253/26 , C07C51/252 , C07C57/04 , C07C255/08
摘要： Organic compounds are prepared by heterogeneously catalyzed partial gas-phase oxidation of precursor compounds by a process in which a portion of the reaction gas starting mixture is brought from a low initial pressure to a higher final pressure by means of a radial compressor.
摘要翻译： 通过使反应气体起始混合物的一部分通过径向压缩机从低初始压力升至较高的最终压力的方法，通过异构催化的前体化合物的部分气相氧化来制备有机化合物。
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30.发明申请Method for the rectifying separation of fluids containing (meth)acryl monomers 有权含有（甲基）丙烯酸单体的流体的精馏分离方法公开(公告)号：US20050211542A1
公开(公告)日：2005-09-29
申请号：US10515639
申请日：2003-07-02
CPC分类号： B01D3/22 , B01D3/225 , C07C51/44 , Y10S203/11 , Y10S203/22 , C07C57/04
摘要： In a process for rectificatively separating (meth)acrylic monomer-containing fluids, a rectification column is employed which has at least one sieve tray without runoff segment in which the passages are arranged regularly.
摘要翻译： 在用于精馏（甲基）丙烯酸单体的流体的方法中，使用具有至少一个没有径流段的筛塔的精馏塔，其中通道排列规则。
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