Processes for the preparation of titanyl phthalocyanines
    31.
    发明授权
    Processes for the preparation of titanyl phthalocyanines 失效
    制备钛酞菁的方法

    公开(公告)号:US5350844A

    公开(公告)日:1994-09-27

    申请号:US24145

    申请日:1993-03-01

    CPC classification number: C09B67/0016 C09B67/0019 C09B67/0026

    Abstract: A process for the preparation of a more perfect crystalline form of the Type I polymorph of titanyl phthalocyanine which comprises dissolving a precursor titanyl phthalocyanine Type I in a solution of trihaloacetic acid and alkylene chloride; adding the resultant solution to a solvent thereby enabling precipitation of Type X titanyl phthalocyanine; separating the titanyl phthalocyanine Type X from the solution; followed by a first washing with an organic solvent and a second washing with water; slurrying the resulting Type X titanyl phthalocyanine in an organic solvent enabling conversion of said Type X to Type IV titanyl phthalocyanine; and thereafter, subjecting the Type IV titanyl phthalocyanine obtained to treatment with an organic solvent to enable said crystalline form of titanyl phthalocyanine Type I.

    Abstract translation: 制备氧化钛酞菁的I型多晶型物的更完美结晶形式的方法,其包括将前体氧钛酞菁I溶解在三卤代乙酸和亚烷基氯的溶液中; 将所得溶液加入到溶剂中,从而使X型氧钛酞菁沉淀; 从溶液中分离X型氧钛酞菁; 然后用有机溶剂进行第一次洗涤,并用水洗涤第二次; 将得到的X型氧钛酞菁在有机溶剂中制浆,使所述X型转化为IV型氧钛酞菁; 然后,将得到的IV型钛酞菁用有机溶剂进行处理,得到所述晶型的钛氧酞菁I型。

    Imaging members and processes for the preparation thereof
    32.
    发明授权
    Imaging members and processes for the preparation thereof 失效
    成像成员及其制备方法

    公开(公告)号:US5300393A

    公开(公告)日:1994-04-05

    申请号:US929227

    申请日:1992-08-14

    CPC classification number: G03G5/0564

    Abstract: A process for the preparation of photoconductive imaging members which comprises coating a supporting substrate with a photogenerator layer comprised of photogenerating pigments and a mixture of cyclic oligomers wherein said mixture is heated to obtain a polycarbonate resin binder, and subsequently applying to the photogenerating layer a layer of charge transport molecules.

    Abstract translation: 一种制备光导成像构件的方法,包括用由光生颜料和环状低聚物的混合物组成的光发生器层涂覆支撑基底,其中将所述混合物加热以获得聚碳酸酯树脂粘合剂,随后向光生代层施加层 的电荷转运分子。

    Encapsulated reactive ink and method for forming images using same
    33.
    发明授权
    Encapsulated reactive ink and method for forming images using same 有权
    封装反应性油墨及使用其形成图像的方法

    公开(公告)号:US08807697B2

    公开(公告)日:2014-08-19

    申请号:US12947041

    申请日:2010-11-16

    CPC classification number: C09D11/101

    Abstract: An ink including at least one first reactive component, at least one second component comprising a triggerable component, at least one third reactive component, and an optional colorant; wherein the at least one first reactive component and the at least one third reactive component are capable of reacting with one another to form a solid ink on a substrate; wherein the at least one first reactive component is encapsulated in a microcapsule; wherein the ink can be jetted onto a substrate and treated whereby the treatment causes the at least one triggerable component to trigger the rupture of the microcapsule thereby releasing the at least one first reactive component from the microcapsule so that the at least one first reactive component and the at least one third reactive component come into contact, react, and polymerize thereby curing the ink.

    Abstract translation: 包括至少一种第一反应性组分的油墨,至少一种包含可触发组分的第二组分,至少一种第三活性组分和任选的着色剂; 其中所述至少一种第一反应性组分和所述至少一种第三活性组分能够彼此反应以在基材上形成固体油墨; 其中所述至少一种第一反应性组分被包封在微胶囊中; 其中所述油墨可以被喷射到基底上并进行处理,由此所述处理使所述至少一个可触发组分触发所述微胶囊的破裂,从而从所述微胶囊释放所述至少一种第一反应性组分,使得所述至少一种第一反应性组分和 所述至少一个第三反应性组分接触,反应和聚合,从而固化所述油墨。

    Phase change inks and process for the preparation thereof
    36.
    发明授权
    Phase change inks and process for the preparation thereof 有权
    相变油墨及其制备方法

    公开(公告)号:US06878198B1

    公开(公告)日:2005-04-12

    申请号:US10722164

    申请日:2003-11-25

    CPC classification number: C09D11/34

    Abstract: Phase change ink compositions comprising (a) an ink carrier comprising a monoamide and a tetra-amide, and (b) pigment particles having oxygen-containing functional groups on the surfaces thereof. Also, processes for preparing a phase change ink which comprise (a) melting a tetra-amide which is solid at about 25° C.; (b) admixing with the molten tetra-amide pigment particles having oxygen-containing functional groups on the surfaces thereof; (c) maintaining the mixture of pigment and tetra-amide at a temperature of at least about 100° C. and at a temperature of no more than about 200° C. for a period sufficient to enable the molten tetra-amide to wet the pigment particle surfaces; (d) subsequent to wetting of the pigment particle surfaces with the molten tetra-amide, adding to the mixture a monoamide; (e) subsequent to addition of the monoamide, subjecting the resulting mixture to high shear mixing; and (f) subsequent to subjecting the mixture to high shear mixing, optionally adding to the mixture additional ink ingredients.

    Abstract translation: 相变油墨组合物,其包含(a)包含单酰胺和四酰胺的油墨载体,和(b)在其表面上具有含氧官能团的颜料颗粒。 另外,制备相变油墨的方法包括(a)在约25℃熔化固体的四酰胺; (b)与表面具有含氧官能团的熔融四酰胺颜料颗粒混合; (c)将颜料和四酰胺的混合物在至少约100℃的温度和不超过约200℃的温度下保持足以使熔融的四酰胺湿润的时间 颜料颗粒表面; (d)在用四酰胺熔融物润湿颜料颗粒表面之后,向混合物中加入单酰胺; (e)在加入单酰胺后,将所得混合物进行高剪切混合; 和(f)在混合物进行高剪切混合之后,任选地向混合物中加入另外的油墨成分。

    Ink jet inks and printing processes
    39.
    发明授权
    Ink jet inks and printing processes 失效
    喷墨油墨和印刷工艺

    公开(公告)号:US5709737A

    公开(公告)日:1998-01-20

    申请号:US603516

    申请日:1996-02-20

    CPC classification number: C09D11/30

    Abstract: Disclosed is an ink composition which comprises an aqueous liquid vehicle, a colorant, and an additive material selected from the group consisting of (a) symmetric acetylenic bisester alcohols, (b) symmetric acetylenic bisalkyl alcohols and acetylenic bisalkoxy alcohols, (c) symmetric acetylenic bisamido alcohols, (d) symmetric bisamido alcohols, (e) mono amido alcohols, (f) trialkylhydroxy compounds, (g) derivatives of 1,2-diols and 1,3-diols, (h) thio diols, (i) aromatic diols, (j) heterocyclic diols, (k) imino alcohols, (l) salts of hydroxyl compounds, (m) saccharides and saccharide derivatives, and (n) mixtures thereof. Also disclosed is an ink jet process which comprises (1) incorporating into a thermal ink jet printing apparatus the aforementioned ink composition; and (2) causing droplets of the ink to be ejected from the printing apparatus in an imagewise pattern onto a substrate, thereby generating images on the substrate. Further disclosed is an ink jet printing process which comprises (1) incorporating into a thermal ink jet printing apparatus the aforementioned ink composition; (2) causing droplets of the ink to be ejected from the printing apparatus in an imagewise pattern onto a substrate, thereby generating images on the substrate; and (3) exposing the substrate to microwave radiation, thereby drying the images on the substrate.

    Abstract translation: 公开了一种油墨组合物,其包含水性液体载体,着色剂和选自(a)对称炔属双酯醇,(b)对称炔属双烷基醇和炔属双烷氧基醇的添加剂材料,(c)对称炔属 (d)对称双酰氨基醇,(e)单酰胺醇,(f)三烷基羟基化合物,(g)1,2-二醇和1,3-二醇的衍生物,(h)硫代二醇,(i)芳族 二醇,(j)杂环二醇,(k)亚氨基醇,(l)羟基化合物的盐,(m)糖和糖衍生物,和(n)它们的混合物。 还公开了一种喷墨方法,其包括(1)将上述油墨组合物结合到热喷墨印刷装置中; 和(2)使墨液滴以成像图案从印刷装置喷射到基板上,从而在基板上产生图像。 进一步公开了一种喷墨印刷方法,其包括(1)将上述油墨组合物结合到热喷墨印刷装置中; (2)使墨水的液滴以成像图案从打印装置喷射到基板上,从而在基板上产生图像; 和(3)将基板暴露于微波辐射,从而干燥基板上的图像。

    Titanium phthalocyanine imaging member
    40.
    发明授权
    Titanium phthalocyanine imaging member 失效
    钛酞菁成像构件

    公开(公告)号:US5371213A

    公开(公告)日:1994-12-06

    申请号:US111255

    申请日:1993-08-23

    Applicant: James D. Mayo

    Inventor: James D. Mayo

    CPC classification number: C09B67/0016 C09B67/0026

    Abstract: A process for the preparation of titanyl phthalocyanine Type 1a which comprises admixing Type I titanyl phthalocyanine with a component that enables dissolution thereof; adding the resulting dissolved titanyl phthalocyanine pigment to a solvent mixture thereby enabling reprecipitation of said pigment; and subsequently contacting the Type X titanyl phthalocyanine formed with hot halobenzene.

    Abstract translation: 制备1a型钛酞菁的方法,其包括将I型氧钛酞菁与能够溶解的组分混合; 将所得溶解的氧钛酞菁颜料加入到溶剂混合物中,从而使所述颜料再沉淀; 并随后使形成的X型氧钛酞菁与热卤代苯接触。

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