公开(公告)号：US07208627B2

公开(公告)日：2007-04-24

申请号：US11013192

申请日：2004-12-15

申请人： Tetsuya Yamamoto ,  Yasutaka Nakatani ,  Takuya Kamiyama

发明人： Tetsuya Yamamoto ,  Yasutaka Nakatani ,  Takuya Kamiyama

IPC分类号： C07F5/02

CPC分类号： C07F5/022

摘要： In the process of synthesizing alkylborazine compound represented by the chemical formula 2, by a reaction of a halogenated borazine compound represented by the chemical formula 1 with a Grignard reagent, thus synthesized alkylborazine compound is washed with water, or subjected to sublimation purification or distillation purification at least three times, and/or subjected to distillation purification at least twice. In the formulas, R1 independently represents alkyl group; R2 independently represents alkyl group; and X represents halogen atom.

摘要翻译： 在合成由化学式2表示的烷基硼氮化合物的过程中，通过化学式1表示的卤代环硼氮烷化合物与格氏试剂的反应，合成的烷基硼氮化合物用水洗涤，或进行升华纯化或蒸馏纯化 至少三次，和/或经蒸馏纯化至少两次。 在式中，R 1独立地表示烷基; R 2独立地表示烷基; X表示卤素原子。