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    Composition for forming electrode active material of lithium secondary battery, composition for forming separator and method of preparing lithium secondary battery using the compositions
    1.
    发明授权
    Composition for forming electrode active material of lithium secondary battery, composition for forming separator and method of preparing lithium secondary battery using the compositions 有权
    用于形成锂二次电池的电极活性材料的组合物，用于形成隔膜的组合物和使用该组合物制备锂二次电池的方法

    公开(公告)号：US06692873B1

    公开(公告)日：2004-02-17

    申请号：US09629951

    申请日：2000-08-01

    申请人： Chi-kyun Park ,  Archana Kakirde ,  Peikang Liu ,  Venkatesan Manivannan ,  Chul Chai ,  Dong-joon Ihm ,  Jon-ha Lee ,  Kwon-sun Roh

    发明人： Chi-kyun Park ,  Archana Kakirde ,  Peikang Liu ,  Venkatesan Manivannan ,  Chul Chai ,  Dong-joon Ihm ,  Jon-ha Lee ,  Kwon-sun Roh

    IPC分类号： H01M216

    CPC分类号： H01M2/145 ,  H01M2/1653 ,  H01M2/1673 ,  H01M10/04 ,  H01M10/052 ,  Y10T29/49115

    摘要： An electrode active material forming composition, a separator forming composition and a manufacturing method of a lithium secondary battery using the compositions are provided. The method for manufacturing a lithium secondary battery including the steps of (a) coating electrode active material compositions each comprising a electrode active material, a binder and a solvent on an electrode current collector to form a cathode and an anode, (b) forming a separator on both surfaces of the anode using a composition for forming a separator comprising a polymer resin, a plasticizer, a filler and a solvent; (c) disposing and fixedly adhering the cathode on the separator to form a battery structure, (d) drying the battery structure under a vacuum condition, and (e) impregnating an electrolytic solution into the resultant structure, wherein the plasticizer of the composition for forming the separator is at least one material selected from the group consisting of an ethylene glycol derivative, a cyclic carbonate, a non-cyclic carbonate and propylene glycol carbonate. Therefore, since a plasticizer can be removed under a vacuum condition, the time required for manufacturing a battery can be reduced and the manufacturing process becomes simplified, thereby improving the productivity. Also, since an organic solvent extraction process using an organic solvent is not necessary, unlike in the conventional art, the cost required for a recovery facility of an organic solvent can be reduced. Further, uniform pores are formed in electrodes and a separator, the porosity characteristics are excellent, and adhesion between the separator and the electrodes is excellent, thereby exhibiting excellent high-rate, lifetime, and low-temperature characteristics.

    摘要翻译： 提供电极活性物质形成组合物，隔膜形成用组合物和使用该组合物的锂二次电池的制造方法。 一种锂二次电池的制造方法，包括以下步骤：（a）在电极集电体上涂布均包含电极活性物质，粘合剂和溶剂的电极活性物质组合物，形成阴极和阳极，（b） 使用用于形成包含聚合物树脂，增塑剂，填料和溶剂的隔膜的组合物的阳极的两个表面上的隔板; （c）将阴极设置并固定在隔板上以形成电池结构，（d）在真空条件下干燥电池结构，和（e）将电解液浸渍到所得结构中，其中用于 形成隔膜的是至少一种选自乙二醇衍生物，环状碳酸酯，非环状碳酸酯和丙二醇碳酸酯的材料。 因此，由于可以在真空条件下去除增塑剂，所以可以减少制造电池所需的时间，并且制造过程变得简化，从而提高生产率。 此外，由于不需要使用有机溶剂的有机溶剂萃取方法，与常规技术不同，可以降低有机溶剂的回收设备所需的成本。 此外，在电极和隔膜中形成均匀的孔，孔隙率特性优异，隔板和电极之间的粘附性优异，因此表现出优异的高速率，寿命和低温特性。

    Lithium secondary battery
    4.
    发明授权
    Lithium secondary battery 有权
    锂二次电池

    公开(公告)号：US06503661B1

    公开(公告)日：2003-01-07

    申请号：US09629950

    申请日：2000-08-01

    申请人： Chi-kyun Park ,  Archana Kakirde ,  Peikang Liu ,  Venkatesan Manivannan ,  Chul Chai ,  Dong-joon Ihm ,  Jon-ha Lee

    发明人： Chi-kyun Park ,  Archana Kakirde ,  Peikang Liu ,  Venkatesan Manivannan ,  Chul Chai ,  Dong-joon Ihm ,  Jon-ha Lee

    IPC分类号： H01M618

    CPC分类号： H01M10/0525 ,  H01M6/168 ,  H01M6/181 ,  H01M6/188 ,  H01M10/0565

    摘要： A composition for forming polymer electrolyte and a lithium secondary battery employing the polymer electrolyte prepared using the composition are provided. The composition for forming polymer solid electrolyte having a polymer resin, a plasticizer, a filler and a solvent, wherein the filler is synthetic zeolite having an affinity for an organic solvent or moisture. Therefore, the mechanical strength and ionic conductivity can be improved by adding synthetic zeolite as a filler when forming polymer electrolyte. Also, use of such polymer electrolyte makes it possible to prepare lithium secondary batteries having good high-current discharge characteristics and excellent discharge capacity characteristics even under repeated charge/discharge conditions.

    摘要翻译： 提供了一种用于形成聚合物电解质的组合物和使用该组合物制备的使用聚合物电解质的锂二次电池。 用于形成具有聚合物树脂，增塑剂，填料和溶剂的聚合物固体电解质的组合物，其中填料是对有机溶剂或水分具有亲和性的合成沸石。 因此，当形成聚合物电解质时，通过加入合成沸石作为填料可以改善机械强度和离子传导性。 此外，通过使用这样的高分子电解质，即使在重复的充放电条件下也能够制备具有良好的高电流放电特性和优异的放电容量特性的锂二次电池。

    Organic lithium salt electrolytes having enhanced safety for rechargeable batteries and methods of making the same
    5.
    发明授权
    Organic lithium salt electrolytes having enhanced safety for rechargeable batteries and methods of making the same 失效
    对可充电电池的安全性提高的有机锂盐电解质及其制造方法

    公开(公告)号：US07534527B2

    公开(公告)日：2009-05-19

    申请号：US10952481

    申请日：2004-09-29

    申请人： Zhiqiang Xu ,  Chi-Kyun Park ,  Zhiwei Zhang ,  Chai Chul

    发明人： Zhiqiang Xu ,  Chi-Kyun Park ,  Zhiwei Zhang ,  Chai Chul

    IPC分类号： H01M6/04 ,  H01M6/16

    CPC分类号： H01M10/0569 ,  H01M6/164 ,  H01M2300/0025 ,  H01M2300/0031 ,  H01M2300/0034

    摘要： Organic lithium salts suitable for use in electrolytes for primary or secondary rechargeable batteries include de-localized bulky anions over Lewis acid fragments, typically BF3, and organic moieties. The organic moieties may be, for example, anions derived from fused nitrogen heterocycles (e.g. benzeneimidate, benzitriazolate and the like); multi carboxylates (e.g. oxalate, 1,2,4,5-benzenetetracarboxylate and the like), and pyromellitic diimidate. The organic lithium salts of the invention have the general formula: Liq[Org(MXn)m], in which Org represents the organic moieties and MXn represents an organic or inorganic boron, aluminum or phosphorous containing Lewis acid. The organic lithium salts are conveniently prepared by reacting an organic compound having at least one de-protonation group selected from NH, OH, SH or COOH with an inorganic or organic lithium compound to generate an organic lithium processor salt, and thereafter bringing the organic lithium processor salt into contact with an inorganic or organic Lewis acid to obtain the organic lithium product salt.

    摘要翻译： 适用于初级或次级可再充电电池的电解质的有机锂盐包括超过路易斯酸片段（通常为BF 3）和有机部分的脱定位的大阴离子。 有机部分可以是例如衍生自稠合氮杂环的阴离子（例如苯亚氨酸酯，苯并三唑酸酯等）; 多羧酸盐（例如草酸盐，1,2,4,5-苯四羧酸盐等）和均苯四酸二亚胺酯。 本发明的有机锂盐具有通式：Liq [Org（MXn）m]，其中Org表示有机部分，MXn表示有机或无机硼，含铝或含磷的路易斯酸。 通过使具有至少一个选自NH，OH，SH或COOH的脱质子基团的有机化合物与无机或有机锂化合物反应，生成有机锂处理剂盐，然后将有机锂盐 处理剂盐与无机或有机路易斯酸接触以获得有机锂产物盐。

    High ionic conductivity gel polymer electrolyte for rechargeable polymer batteries
    6.
    发明授权
    High ionic conductivity gel polymer electrolyte for rechargeable polymer batteries 失效
    用于可充电聚合物电池的高离子电导率凝胶聚合物电解质

    公开(公告)号：US06841303B2

    公开(公告)日：2005-01-11

    申请号：US09986459

    申请日：2001-11-08

    申请人： Chi-Kyun Park ,  Zhiwei Zhang ,  Lu Ying Sun ,  Chul Chai

    发明人： Chi-Kyun Park ,  Zhiwei Zhang ,  Lu Ying Sun ,  Chul Chai

    IPC分类号： H01M4/131 ,  H01M4/133 ,  H01M4/58 ,  H01M4/587 ,  H01M6/18 ,  H01M10/052 ,  H01M10/0525 ,  H01M10/0565 ,  H01M10/0587 ,  H01M10/36 ,  H01M6/16

    CPC分类号： H01M10/0565 ,  H01M4/131 ,  H01M4/133 ,  H01M4/587 ,  H01M6/181 ,  H01M10/052 ,  H01M10/0525 ,  H01M10/0587 ,  H01M2300/0085 ,  Y10T29/4911

    摘要： Ionic gel polymer electrolytes for rechargeable polymer batteries preferably are formed by dissolving a gelling agent into organic liquid electrolytes, and then gelling the precursor in situ at elevated temperature after pouring it into a battery case that contains a cathode, an anode and a separator. The gel polymer electrolytes exhibit excellent ionic conductivity of up to about 10−2 S/cm and voltage stability for lithium rechargeable batteries. Most preferably, the gel polymer electrolyte is the reaction product of (A) a heterocyclic amine-group containing material (preferably a vinvlpyridine), and (B) halide or epoxy-group containing polymers, copolymers, oligomers or monomers that are capable of reacting with nitrogen-containing compounds, such as polymers, copolymers, oligomers or monomers containing alkylene halides or halomethyl group substituted aromatic units or at least one epoxy unit.

    摘要翻译： 用于可再充电聚合物电池的离子凝胶聚合物电解质优选通过将胶凝剂溶解到有机液体电解质中，然后在将其倾入包含阴极，阳极和隔膜的电池壳中之后将其高温地将其高温胶凝而形成。 凝胶聚合物电解质表现出高达约10 -2 S / cm的离子电导率和锂可充电电池的电压稳定性。 最优选地，凝胶聚合物电解质是（A）含杂环胺基材料（优选乙烯吡啶）的反应产物和（B）能够反应的卤化物或含环氧基的聚合物，共聚物，低聚物或单体的反应产物 与含氮化合物，例如聚合物，共聚物，低聚物或含有亚烷基卤化物或卤代甲基取代的芳族单元或至少一个环氧单元的单体。

    Method of making an electrochemical cell by the application of polysiloxane onto at least one of the cell components
    7.
    发明授权
    Method of making an electrochemical cell by the application of polysiloxane onto at least one of the cell components 失效
    通过将聚硅氧烷应用于至少一种电池组分来制造电化学电池的方法

    公开(公告)号：US06547839B2

    公开(公告)日：2003-04-15

    申请号：US09766672

    申请日：2001-01-23

    申请人： Zhiwei Zhang ,  Chi-Kyun Park ,  Lu Ying Sun ,  Chul Chai

    发明人： Zhiwei Zhang ,  Chi-Kyun Park ,  Lu Ying Sun ,  Chul Chai

    IPC分类号： H01M600

    CPC分类号： H01M10/0525 ,  H01M2/1653 ,  H01M2/1673 ,  H01M2/168 ,  H01M10/0587 ,  Y10T29/49108 ,  Y10T29/49112 ,  Y10T29/49115

    摘要： Lithium-ion electrochemical cells include an anode, a cathode and a separator between the anode and cathode, wherein at least one of the anode, cathode and separator includes a polysiloxane coating thereon. Most preferably, the polysiloxane coating is the polymerized reaction product of dimethyl siloxane and tetra(trimethylsiloxy) silane), and is present on the surface in an amount between about 0.05 to about 0.17 mg/cm2. After being coated with the polysiloxane adhesive, the electrodes and separator can easily be attached one to another at ambient temperature by application of pressure using a hand roller or with a laminator, and then subsequently formed into a spiral or stacked structure for placement in a battery cell case.

    摘要翻译： 锂离子电化学电池包括阳极，阴极和在阳极和阴极之间的隔板，其中阳极，阴极和隔板中的至少一个在其上包括聚硅氧烷涂层。 最优选地，聚硅氧烷涂层是二甲基硅氧烷和四（三甲基甲硅烷氧基）硅烷）的聚合反应产物，并且在表面上以约0.05至约0.17mg / cm 2的量存在。 在涂覆聚硅氧烷粘合剂之后，通过使用手动辊或层压机施加压力，电极和隔膜可以容易地在环境温度下彼此连接，然后形成螺旋或堆叠结构以放置在电池中 电池盒。

    Organic lithium salt electrolytes having enhanced safety for rechargeable batteries and methods of making the same
    9.
    发明申请
    Organic lithium salt electrolytes having enhanced safety for rechargeable batteries and methods of making the same 失效
    对可充电电池的安全性提高的有机锂盐电解质及其制造方法

    公开(公告)号：US20060068295A1

    公开(公告)日：2006-03-30

    申请号：US10952481

    申请日：2004-09-29

    申请人： Zhiqiang Xu ,  Chi-Kyun Park ,  Zhiwei Zhang ,  Chai Chul

    发明人： Zhiqiang Xu ,  Chi-Kyun Park ,  Zhiwei Zhang ,  Chai Chul

    IPC分类号： H01M6/18

    CPC分类号： H01M10/0569 ,  H01M6/164 ,  H01M2300/0025 ,  H01M2300/0031 ,  H01M2300/0034

    摘要： Organic lithium salts suitable for use in electrolytes for primary or secondary rechargeable batteries include de-localized bulky anions over Lewis acid fragments, typically BF3, and organic moieties. The organic moieties may be, for example, anions derived from fused nitrogen heterocycles (e.g. benzeneimidate, benzitriazolate and the like); multi carboxylates (e.g. oxalate, 1,2,4,5-benzenetetracarboxylate and the like), and pyromellitic diimidate. The organic lithium salts of the invention have the general formula: Liq[Org(MXn)m], in which Org represents the organic moieties and MXn represents an organic or inorganic boron, aluminum or phosphorous containing Lewis acid. The organic lithium salts are conveniently prepared by reacting an organic compound having at least one de-protonation group selected from NH, OH, SH or COOH with an inorganic or organic lithium compound to generate an organic lithium processor salt, and thereafter bringing the organic lithium processor salt into contact with an inorganic or organic Lewis acid to obtain the organic lithium product salt.

    摘要翻译： 适用于初级或次级可再充电电池的电解质的有机锂盐包括路易斯酸片段（通常为BF 3）和有机部分的脱定位的大阴离子。 有机部分可以是例如衍生自稠合氮杂环的阴离子（例如苯亚氨酸酯，苯并三唑酸酯等）; 多羧酸盐（例如草酸盐，1,2,4,5-苯四羧酸盐等）和均苯四酸二亚胺酯。 本发明的有机锂盐具有以下通式：其中Org表示有机物，其中，Org（= 部分和MX n表示含有有机或无机硼，铝或磷的路易斯酸。 通过使具有至少一个选自NH，OH，SH或COOH的脱质子基团的有机化合物与无机或有机锂化合物反应，生成有机锂处理剂盐，然后将有机锂盐 处理剂盐与无机或有机路易斯酸接触以获得有机锂产物盐。