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    Metal-free, substituted phthalocyanines in the .chi.-modification
    3.
    发明授权
    Metal-free, substituted phthalocyanines in the .chi.-modification 失效
    在x-修饰中无金属的取代酞菁

    公开(公告)号：US5367069A

    公开(公告)日：1994-11-22

    申请号：US59481

    申请日：1993-05-10

    申请人： Gunther Beck ,  Bernd Kaletta

    发明人： Gunther Beck ,  Bernd Kaletta

    IPC分类号： C09B47/30 ,  C09B67/12 ,  C09B67/50 ,  C09D7/12 ,  C09D11/02 ,  D06P1/44

    CPC分类号： C09B67/0026 ,  C09B47/30 ,  C09B67/0016

    摘要： Metal-free phthalocyanines in the .chi.-modification substituted in up to four ortho positions can be prepared by tetramerisation of a reaction mixture consisting of phthalonitriles substituted in the 3-position with phthalonitrile in a molar ratio of 4:0 to 1:40 in the presence of a base and subsequent heat treatment at temperatures of between 100.degree. and 300.degree. C. They constitute excellent organic pigments.

    摘要翻译： 在最多四个邻位取代的氯化改性中的无金属酞菁可以通过将由3-位取代的酞腈与邻苯二甲腈组成的反应混合物以4:0至1:40的摩尔比四 在100℃至300℃之间的温度下存在碱和随后的热处理。它们构成优异的有机颜料。

    Substituted 4,5-diamino-1,2,4-triazol-3-(thi)ones
    4.
    发明授权
    Substituted 4,5-diamino-1,2,4-triazol-3-(thi)ones 失效
    取代的4,5-二氨基-1,2,4-三唑-3-（硫）

    公开(公告)号：US5276008A

    公开(公告)日：1994-01-04

    申请号：US831261

    申请日：1992-01-31

    申请人： Dietmar Kuhnt ,  Kurt Findeisen ,  Michael Haug ,  Joachim Kluth ,  Klaus-Helmut Muller ,  Klaus Konig ,  Thomas Himmler ,  Gunther Beck ,  Hans-Joachim Santel ,  Klaus Lurssen ,  Robert R. Schmidt ,  Birgit Krauskopf

    发明人： Dietmar Kuhnt ,  Kurt Findeisen ,  Michael Haug ,  Joachim Kluth ,  Klaus-Helmut Muller ,  Klaus Konig ,  Thomas Himmler ,  Gunther Beck ,  Hans-Joachim Santel ,  Klaus Lurssen ,  Robert R. Schmidt ,  Birgit Krauskopf

    IPC分类号： A01N47/38 ,  C07C265/08 ,  C07C323/32 ,  C07C331/24 ,  C07D249/14 ,  C07D319/20 ,  C07D403/12 ,  C07D405/12 ,  A01N43/653 ,  C07D249/12

    CPC分类号： C07D403/12 ,  A01N47/38 ,  C07C265/08 ,  C07C323/32 ,  C07C331/24 ,  C07D249/14 ,  C07D319/20 ,  C07D405/12 ,  C07C2101/14

    摘要： The invention relates to new substituted 4,5-diamino-1,2,4-triazol-3-(thi)ones of the general formula (I), ##STR1## in which R.sup.1 represents alkyl, alkenyl, alkinyl, halogenoalkyl, halogenoalkenyl, halogenoalkinyl, cyanoalkyl, hydroxyalkyl, alkoxyalkyl, aryloxyalkyl, arylthioalkyl, arylsulfinylalkyl, arylsulfonylalkyl, arylaminoalkyl, N-alkyl-arylaminoalkyl, alkoxycarbonylalkyl, alkoxycarbonylalkenyl, alkylaminoalkyl, dialkylaminoalkyl, in each case optionally substituted cycloalkyl, cycloalkylalkyl, cycloalkenyl or cycloalkenylalkyl, or optionally substituted heterocyclylalkyl, or in each case optionally substituted aralkyl, arylalkenyl, arylalkinyl, aroyl, aryl, aralkyloxy or aryloxy, for alkoxy, alkenyloxy or alkinyloxy,R.sup.2, R.sup.3, R.sup.4 and R.sup.5 are identical or different and independently of one another represent hydrogen, alkyl, alkenyl, alkinyl, halogenoalkyl, halogenoalkenyl, halogenoalkinyl, cyanoalkyl, alkoxyalkyl, alkylthioalkyl, in each case optionally substituted cycloalkyl, cycloalkylalkyl, aryl or aralkyl or in each case two of these radicals (R.sup.2 and R.sup.3 or R.sup.4 and R.sup.5) represent together alkanediyl and R.sup.5 can also represent alkoxy,X represents oxygen or sulphur andY represents oxygen or sulphur,a plurality of processes and new intermediates for their preparation, and their use as herbicides and plant growth regulators.

    摘要翻译： 本发明涉及通式（I）的新的取代的4,5-二氨基-1,2,4-三唑-3-（thi），（*化学结构*）（I），其中R 1表示烷基，烯基 烷氧基烷基，芳基氨基烷基，芳基氨基烷基，烷基氨基烷基，烷氧基羰基烷基，烷氧基羰基烯基，烷基氨基烷基，二烷基氨基烷基，在各种情况下均为任选取代的环烷基，环烷基烷基，环烯基或 环烷基烷基或任选取代的杂环基烷基，或在每种情况下任选取代的芳烷基，芳基烯基，芳基炔基，芳酰基，芳基，芳烷氧基或芳氧基，对于烷氧基，烯氧基或烷氧基，R2，R3，R4和R5相同或不同， 代表氢，烷基，烯基，炔基，卤代烷基，卤代烯基，卤代烯基，氰基烷基，烷氧基烷基，烷硫基烷基， 环烷基，环烷基烷基，芳基或芳烷基，或者在每种情况下，这些基团中的两个（R2和R3或R4和R5）一起表示烷二基，R5也可以表示烷氧基，X表示氧或硫，Y表示氧或硫， 和新的中间体用于其制备，并用作除草剂和植物生长调节剂。

    N-sulphenylated 2-amino-4-chloro-thiazole-sulphonamides, their use, process for their preparation, and the intermediates 2,4-dichlorothiazole-sulphonyl chloride and 2-amino-4-chloro-thiazole-sulphonamides
    6.
    发明授权
    N-sulphenylated 2-amino-4-chloro-thiazole-sulphonamides, their use, process for their preparation, and the intermediates 2,4-dichlorothiazole-sulphonyl chloride and 2-amino-4-chloro-thiazole-sulphonamides 失效
    N-磺基化的2-氨基-4-氯 - 噻唑磺酰胺，它们的用途及其制备方法，和中间体2,4-二氯噻唑 - 磺酰氯和2-氨基-4-氯 - 噻唑 - 磺酰胺

    公开(公告)号：US4906650A

    公开(公告)日：1990-03-06

    申请号：US308180

    申请日：1989-02-08

    申请人： Gunther Beck ,  Bernd Baasner ,  Michael Schwamborn ,  Wilhelm Brandes

    发明人： Gunther Beck ,  Bernd Baasner ,  Michael Schwamborn ,  Wilhelm Brandes

    IPC分类号： C07D277/20 ,  A01N47/04 ,  C07D277/36 ,  C07D277/42 ,  C07D277/52 ,  C07D277/54 ,  C07D417/12

    CPC分类号： C07D417/12 ,  A01N47/04 ,  C07D277/36 ,  C07D277/42 ,  C07D277/52

    摘要： The fungicidally active N-sulphenylated 2-amino-4-chloro-thiazole-sulphonamides of the formula ##STR1## wherein R.sup.1 and R.sup.2 independently of one another denote hydrogen, alkyl, alkenyl, alkinyl, cycloalkyl, aryl, aralkyl or an aromatic or a non-aromatic heterocyclic radical andR.sup.3 and R.sup.4 independently of one another stand for hydrogen, alkyl, cycloalkyl, aryl or aralkyl or for the dichlorohalogenomethyl-sulphenyl radical --S--CCl.sub.2 X, in which X denotes fluorine, chlorine or bromine, and where furthermore one of the pairs of substituents R.sup.1 and R.sup.3 or R.sup.2 andR.sup.4 together with the nitrogen atom which they substitute can denote morpholino or thiomorpholino, with at least one of the radicals R.sup.3 and R.sup.4 standing for the radical --S--CCl.sub.2 X,can be prepared in a process in which, in a first step, 2,4-dichloro-thiazole is reacted with chlorosulphonic acid to give 2,4-dichloro-thiazole-sulphonyl chloride, in which, in a second step, the 2,4-dichloro-thiazole-sulphonyl chloride is reacted with primary amines or with a primary and a secondary amine to give 2-amino-4-chloro-thiazole-sulphonamides, and in which, in a third step, the sulphonamides mentioned are reacted with dichlorohalogenomethylsulphenyl chlorides to give the substances of the formula (I).

    摘要翻译： 式（I）的杀真菌活性N-磺基化2-氨基-4-氯 - 噻唑 - 磺酰胺其中R 1和R 2彼此独立地表示氢，烷基，烯基，炔基，环烷基，芳基，芳烷基或 芳族或非芳香族杂环基，R 3和R 4彼此独立地代表氢，烷基，环烷基，芳基或芳烷基或二氯卤代甲基 - 磺酰基-S-CCl 2 X，其中X表示氟，氯或溴，以及 此外，取代基R 1和R 3或R 2和R 4中的一个与它们所取代的氮原子一起可以表示吗啉代或硫代吗啉基，其中R3和R4中至少一个代表基团-S-CCl 2，可以是 其中在第一步中将2,4-二氯 - 噻唑与氯磺酸反应，得到2,4-二氯 - 噻唑 - 磺酰氯，其中在第二步中，2,4-二氯 - 二氯 - 噻唑 - 磺酰氯与伯胺反应 胺或与伯胺和仲胺反应，得到2-氨基-4-氯 - 噻唑 - 磺酰胺，其中在第三步中，所述磺酰胺与二氯卤代甲基亚磺酰氯反应，得到式（I）的物质， 。

    Dimeric ketene of 1,2,4-triazole-3-carboxylic acid
    8.
    发明授权
    Dimeric ketene of 1,2,4-triazole-3-carboxylic acid 失效
    1,2,4-三唑-3-羧酸二聚乙烯酮

    公开(公告)号：US4312987A

    公开(公告)日：1982-01-26

    申请号：US188427

    申请日：1980-09-18

    申请人： Gunther Beck

    发明人： Gunther Beck

    IPC分类号： C07D249/10 ,  C07D487/14

    CPC分类号： C07D487/14 ,  C07D249/10

    摘要： Dimeric ketene of 1,2,4-triazole-3-carboxylic acid, of the formula ##STR1## and a process for its preparation by contacting 1,2,4-triazole-3-carboxylic acid with at least an equal molar amount of an acid halide in the presence of the small amount of N,N-disubstituted carboxylic acid amide.

    摘要翻译： 具有式“IMAGE”的1,2,4-三唑-3-羧酸二聚烯酮及其制备方法，其通过使1,2,4-三唑-3-羧酸与至少相等摩尔量的 在少量的N，N-二取代的羧酸酰胺的存在下加入酰卤。