摘要:
Methyl 2-(chloro- or bromomethyl)phenylacetate is prepared by treating 3-isochromanone with thionyl chloride or thionyl bromide in the presence of methanol.
摘要:
3-Isochromanome is prepared by reacting an o-xylene-&agr;,&agr;′-dihalide with carbon monoxide and water in the presence of a metal catalyst such that the pH of the reaction is maintained between about 7 and 11.
摘要:
3-Isochromanone is prepared by contacting an o-xylene-&agr;,&agr;′-dihalide with carbon monoxide in a two-phase liquid medium, in which one phase is aqueous and the other phase is water-immiscible, in the presence of a catalyst and a hindered amine base.