Imide complex, method for producing the same, metal-containing thin film and method for producing the same
    3.
    发明授权
    Imide complex, method for producing the same, metal-containing thin film and method for producing the same 有权
    酰亚胺络合物,其制造方法,含金属薄膜及其制造方法

    公开(公告)号:US07906668B2

    公开(公告)日:2011-03-15

    申请号:US12439364

    申请日:2007-08-20

    IPC分类号: C07F9/00 C23C16/00

    摘要: Objects of the present invention are to provide a novel niobium or tantalum complex having good vapor pressure and becoming a raw material for producing a niobium- or tantalum-containing thin film by a method such as CVD method, ALD method or the like, a method for producing the same, a metal-containing thin film using the same, and a method for producing the same. The present invention relates to producing an imide complex represented by the general formula (1) by, for example, the reaction between M1(NR1)X3(L)r (2) and an alkali metal alkoxide (3): (wherein M1 represents niobium atom or tantalum atom, R1 represents an alkyl group having from 1 to 12 carbon atoms, R2 represents an alkyl group having from 2 to 13 carbon atoms, X represents halogen atom, r is 1 when L is 1,2-dimethoxyethane ligand, r is 2 when L is pyridine ligand, and M2 represents an alkali metal), and producing a niobium- or tantalum-containing thin film by using the imide complex (1) as a raw material.

    摘要翻译: 本发明的目的是提供一种具有良好蒸气压的新型铌或钽络合物,并且通过诸如CVD法,ALD法等的方法成为生产含铌或钽的薄膜的原料, 为了制造它们,使用该薄膜的含金属薄膜及其制造方法。 本发明涉及通过例如M1(NR1)X3(L)r(2)和碱金属醇盐(3)之间的反应来制备由通式(1)表示的酰亚胺络合物:(其中M1表示 铌原子或钽原子,R1表示碳原子数1〜12的烷基,R2表示碳原子数2〜13的烷基,X表示卤素原子,当L为1,2-二甲氧基乙烷配体时,r为1, 当L为吡啶配体时,r为2,M2表示碱金属,通过使用酰亚胺络合物(1)作为原料制造含有铌或钽的薄膜。

    Radio selective calling receiver
    4.
    发明授权
    Radio selective calling receiver 失效
    无线电选呼接收机

    公开(公告)号:US06218957B1

    公开(公告)日:2001-04-17

    申请号:US08911934

    申请日:1997-08-15

    申请人: Ken-ichi Tada

    发明人: Ken-ichi Tada

    IPC分类号: G08B522

    摘要: A radio selective calling receiver which allows anybody to read characters easily which disappear when a message is scrolled up on a screen by means of a simple display. A control circuit 2 is used to scroll the message displayed on the screen vertically in units of a dot and to switch characters on a line which gradually disappear due to the scrolling to a simple display which can be recognized as characters at the point when they cannot be recognized as characters, based on a switch operation of a switching circuit 5.

    摘要翻译: 一种无线选择呼叫接收机,其允许任何人容易地读取通过简单显示在屏幕上向上滚动消息时消失的字符。 控制电路2用于以点为单位垂直地滚动屏幕上显示的消息,并且在由于滚动而逐渐消失的线上切换字符,以便在不能被识别的点处被识别为字符的简单显示 基于开关电路5的开关动作被识别为字符。

    Display of timer for programming mode of a radio selective calling
receiver
    5.
    发明授权
    Display of timer for programming mode of a radio selective calling receiver 失效
    显示无线电选呼接收机的编程模式的定时器

    公开(公告)号:US5963143A

    公开(公告)日:1999-10-05

    申请号:US747649

    申请日:1996-11-13

    申请人: Ken-ichi Tada

    发明人: Ken-ichi Tada

    IPC分类号: H04Q7/14 G08B5/22 H04Q1/00

    CPC分类号: G08B5/229

    摘要: A radio selective calling receiver includes at least a loudspeaker, a function setting switch, a display unit, a timer, and a time-out display control section. The loudspeaker notifies an incoming call by generating a sound. The function setting switch is operated by a user to set various functions. The display unit displays a message accompanying the incoming call, and the set contents of a predetermined function of the various functions. The timer counts an elapsed time from the start of an operation of the function setting switch to the end of a time-out time. The time-out display control section causes the display unit to display a counted time, obtained by the timer, until the end of the time-out time.

    摘要翻译: 无线电选呼接收机至少包括扬声器,功能设置开关,显示单元,定时器和超时显示控制部分。 扬声器通过产生声音通知来电。 功能设置开关由用户操作以设置各种功能。 显示单元显示与来电相关的消息,以及各种功能的预定功能的设定内容。 定时器计算从功能设置开关的操作开始到超时时间结束的经过时间。 超时显示控制部分使显示单元显示由定时器获得的计时时间,直到超时时间结束。

    Selective-calling radio receiver capable of vibration warning
    6.
    发明授权
    Selective-calling radio receiver capable of vibration warning 失效
    选择性呼叫无线电接收器能够进行振动警告

    公开(公告)号:US5955964A

    公开(公告)日:1999-09-21

    申请号:US679484

    申请日:1996-07-12

    申请人: Ken-ichi Tada

    发明人: Ken-ichi Tada

    CPC分类号: G08B6/00

    摘要: A radio selective calling receiver that enables to restrain the vibration strength change of a warning vibrator independent of the supply voltage change of a dc power supply. This receiver contains a warning controller for controlling a specified warning operation including a warning vibration to give a warning to a user on receipt of a calling signal, a vibrator for producing the warning vibration by an electric power supplied from a dc power supply, and a switching transistor for switching the electric power supplied to the vibrator to thereby produce the warning vibration intermittently. The transistor has a first state in which the electric power is supplied to the vibrator and a second state in which the electric power is not supplied to the vibrator. The both states are alternately effected by a control signal generated by the warning controller. The receiver further includes a power compensator for compensating change of the electric power supplied to the vibrator to thereby restrain change of a vibration strength of the warning vibration. The compensator adjusts the control signal so that a duration of the first state of the transistor is increased according to the decrease of the electric power supplied to the vibrator.

    摘要翻译: 一种无线电选呼接收机,其能够独立于直流电源的电源电压变化来抑制警告振动器的振动强度变化。 该接收器包括警报控制器,用于控制包括警告振动的指定警告操作,以在接收到呼叫信号时向用户发出警告,用于通过由直流电源提供的电力产生警告振动的振动器,以及 切换晶体管,用于切换提供给振动器的电力,从而间歇地产生警告振动。 晶体管具有向振动器提供电力的第一状态和不向振动器供电的第二状态。 这两个状态交替地由警告控制器产生的控制信号影响。 接收器还包括功率补偿器,用于补偿提供给振动器的电力的变化,从而抑制警告振动的振动强度的变化。 补偿器调整控制信号,使得晶体管的第一状态的持续时间根据提供给振动器的电力的减小而增加。

    Metal-containing compound, its production method, metal-containing thin film, and its formation method
    8.
    发明授权
    Metal-containing compound, its production method, metal-containing thin film, and its formation method 有权
    含金属化合物,其制备方法,含金属薄膜及其形成方法

    公开(公告)号:US07816549B2

    公开(公告)日:2010-10-19

    申请号:US11997819

    申请日:2006-07-28

    IPC分类号: C07F7/00 C07F5/06 C23C16/00

    摘要: A compound which has thermal stability and moderate vaporizability and is satisfactory as a material for the CVD or ALD method; a process for producing the compound; a thin film formed from the compound as a raw material; and a method of forming the thin film. A compound represented by the general formula (1) is produced by reacting a compound represented by the general formula (2) with a compound represented by the general formula (3). The compound produced is used as a raw material to form a metal-containing thin film. [Chemical formula 1] (1) [Chemical formula 2] (2) [Chemical formula 3] Mp(NR4R5)q(3) (In the formulae, M represents a Group 4 element, aluminum, gallium, etc.; n is 2 or 3 according to cases; R1 and R3 each represents C1-6 alkyl, etc.; R2 represents C1-6 alkyl, etc.; R4 and R5 each represents C1-4 alkyl, etc.; X represents hydrogen, lithium, or sodium; p is 1 or 2 according to cases; and q is 4 or 6 according to cases).

    摘要翻译: 具有热稳定性和适度可燃性并且作为CVD或ALD方法的材料令人满意的化合物; 一种制备该化合物的方法; 由作为原料的化合物形成的薄膜; 以及形成薄膜的方法。 由通式(1)表示的化合物通过使由通式(2)表示的化合物与通式(3)表示的化合物反应来制备。 所制备的化合物用作原料以形成含金属的薄膜。 [化学式1](1)[化学式2](2)[化学式3] Mp(NR4R5)q(3)(式中,M表示4族元素,铝,镓等; n为 2或3; R1和R3各自表示C1-6烷基等; R2表示C1-6烷基等; R4和R5各自表示C1-4烷基等; X表示氢,锂或 钠;根据情况,p为1或2;根据情况,q为4或6)。

    METAL-CONTAINING COMPOUND, ITS PRODUCTION METHOD, METAL-CONTAINING THIN FILM, AND ITS FORMATION METHOD
    9.
    发明申请
    METAL-CONTAINING COMPOUND, ITS PRODUCTION METHOD, METAL-CONTAINING THIN FILM, AND ITS FORMATION METHOD 有权
    含金属化合物,其生产方法,含金属薄膜及其形成方法

    公开(公告)号:US20100105936A1

    公开(公告)日:2010-04-29

    申请号:US11997819

    申请日:2006-07-28

    IPC分类号: C07F7/28 C07F5/06 C07F7/00

    摘要: A compound which has thermal stability and moderate vaporizability and is satisfactory as a material for the CVD or ALD method; a process for producing the compound; a thin film formed from the compound as a raw material; and a method of forming the thin film. A compound represented by the general formula (1) is produced by reacting a compound represented by the general formula (2) with a compound represented by the general formula (3). The compound produced is used as a raw material to form a metal-containing thin film. [Chemical formula 1] (1) [Chemical formula 2] (2) [Chemical formula 3] Mp(NR4R5)q(3) (In the formulae, M represents a Group 4 element, aluminum, gallium, etc.; n is 2 or 3 according to cases; R1 and R3 each represents C1-6 alkyl, etc.; R2 represents C1-6 alkyl, etc.; R4 and R5 each represents C1-4 alkyl, etc.; X represents hydrogen, lithium, or sodium; p is 1 or 2 according to cases; and q is 4 or 6 according to cases.)

    摘要翻译: 具有热稳定性和适度可燃性并且作为CVD或ALD方法的材料令人满意的化合物; 一种制备该化合物的方法; 由作为原料的化合物形成的薄膜; 以及形成薄膜的方法。 由通式(1)表示的化合物通过使由通式(2)表示的化合物与通式(3)表示的化合物反应来制备。 所制备的化合物用作原料以形成含金属的薄膜。 [化学式1](1)[化学式2](2)[化学式3] Mp(NR4R5)q(3)(式中,M表示4族元素,铝,镓等; n为 2或3; R1和R3各自表示C1-6烷基等; R2表示C1-6烷基等; R4和R5各自表示C1-4烷基等; X表示氢,锂或 钠;根据情况,p为1或2;根据情况,q为4或6)

    Titanium complexes, their production methods, titanium-containing thin films, and their formation methods
    10.
    发明授权
    Titanium complexes, their production methods, titanium-containing thin films, and their formation methods 失效
    钛络合物,其制备方法,含钛薄膜及其形成方法

    公开(公告)号:US07632958B2

    公开(公告)日:2009-12-15

    申请号:US12093389

    申请日:2006-11-01

    IPC分类号: C07F7/28 C23C16/00

    摘要: Objects of the present invention are to provide a novel titanium complex that has good vaporization characteristics and an excellent thermal stability, and becomes a raw material for forming a titanium-containing thin film by methods such as CVD method or ALD method, its production method, a titanium-containing thin film formed using the same, and its formation method. In the invention, a titanium complex represented by the general formula (1) is produced by reacting a diimine represented by the general formula (2) and metallic lithium, and then reacting a tetrakisamide complex represented by the general formula (3). (In the formulae, R1 and R4 represent an alkyl group having from 1 to 6 carbon atoms. R2 and R3 each independently represents a hydrogen atom or an alkyl group having from 1 to 3 carbon atoms. R5 and R6 each independently represents an alkyl group having from 1 to 4 carbon atoms.).

    摘要翻译: 本发明的目的是提供具有良好的蒸发特性和优异的热稳定性的新颖的钛络合物,并且成为通过CVD法或ALD法等方法形成含钛薄膜的原料,其制造方法, 使用其形成的含钛薄膜及其形成方法。 在本发明中,由通式(1)表示的钛络合物通过使由通式(2)表示的二亚氨基与金属锂反应,然后使由通式(3)表示的四酰胺配合物反应来制备。 (式中,R 1和R 4表示碳原子数1〜6的烷基,R 2和R 3各自独立地表示氢原子或碳原子数1〜3的烷基,R 5和R 6各自独立地表示烷基 具有1至4个碳原子)。