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    Fluorine-containing acrylate monomers
    1.
    发明授权
    Fluorine-containing acrylate monomers 有权
    含氟丙烯酸酯单体

    公开(公告)号：US06784312B2

    公开(公告)日：2004-08-31

    申请号：US10198044

    申请日：2002-07-19

    申请人： Satoru Miyazawa ,  Kazuhiko Maeda ,  Kenji Tokuhisa ,  Shoji Arai

    发明人： Satoru Miyazawa ,  Kazuhiko Maeda ,  Kenji Tokuhisa ,  Shoji Arai

    IPC分类号： C07C6952

    CPC分类号： G03F7/0046 ,  C07C69/65 ,  C07C69/653 ,  C07C69/96 ,  C07C2601/14 ,  C07C2602/42 ,  C08F20/22 ,  C08F20/26 ,  C08F220/24 ,  G03F7/0392 ,  G03F7/0397

    摘要： The present invention relates to a polymerizable monomer represented by the general formula (1), wherein R1 is a hydrogen atom, a halogen atom, a hydrocarbon group or a fluorine-containing alkyl group; R2 is a straight-chain or branched alkyl group, a cyclic alkyl group, an aromatic group, or a substituent having at least two of these groups, the R2 being optionally partially fluorinated; R3 is a hydrogen atom, a hydrocarbon group that is optionally branched, a fluorine-containing alkyl group, or a cyclic group having an aromatic or alicyclic structure, the R3 optionally containing a bond of an oxygen atom or carbonyl group; and n is an integer of 1-2.

    摘要翻译： 本发明涉及由通式（1）表示的可聚合单体，其中R 1是氢原子，卤素原子，烃基或含氟烷基; R 2是直链或支链烷基，环状烷基，芳族基团或具有这些基团中至少两个的取代基，R 2任选地被部分氟化; R 3是氢原子，任选支链的烃基，含氟烷基或具有芳族或脂环结构的环状基团，R 3任选地含有氧原子或羰基的键 组; n为1-2的整数。

    Reaction reagent for trifluoromethylation
    2.
    发明授权
    Reaction reagent for trifluoromethylation 失效
    用于三氟甲基化的反应试剂

    公开(公告)号：US07981318B2

    公开(公告)日：2011-07-19

    申请号：US12225249

    申请日：2007-11-06

    申请人： Tetsu Yamakawa ,  Kyoko Yamamoto ,  Daisuke Uraguchi ,  Kenji Tokuhisa

    发明人： Tetsu Yamakawa ,  Kyoko Yamamoto ,  Daisuke Uraguchi ,  Kenji Tokuhisa

    IPC分类号： C09K3/00 ,  C01B15/00 ,  C01B15/01

    CPC分类号： C07C209/74 ,  C07C17/32 ,  C07D213/64 ,  C07D231/12 ,  C07D239/54 ,  C07D473/16 ,  C07D473/18 ,  C07C211/52

    摘要： Provided is a reaction reagent for trifluoromethylation with high general versatility and good efficiency.The reaction reagent for trifluoromethylation contains an iron compound, trifluoromethyl iodide, a sulfoxide and a peroxide, and may further contain an acid. The iron compound is, for example, iron(II) sulfate, ammonium iron(II) sulfate, iron(II) tetrafluoroborate, ferrocene, bis(η5-pentamethylcyclopentadienyl)iron or an iron powder; the sulfoxide is, for example, dimethyl sulfoxide; the peroxide is, for example, hydrogen peroxide or hydrogen peroxide-urea composite; and the acid is, for example, sulfuric acid, tetrafluoroboric acid or trifluoromethanesulfonic acid.

    摘要翻译： 提供具有高通用性和高效率的三氟甲基化反应试剂。 用于三氟甲基化的反应试剂含有铁化合物，三氟甲基碘化物，亚砜和过氧化物，并且还可以含有酸。 铁化合物是例如硫酸铁（II），硫酸铁（II），四氟硼酸铁（II），二茂铁，双（5-五甲基环戊二烯基）铁或铁粉; 亚砜是例如二甲基亚砜; 过氧化物是例如过氧化氢或过氧化氢 - 尿素复合物; 酸是例如硫酸，四氟硼酸或三氟甲磺酸。

    Reaction Reagent for Trifluoromethylation
    3.
    发明申请
    Reaction Reagent for Trifluoromethylation 失效
    三氟甲基化反应试剂

    公开(公告)号：US20100230633A1

    公开(公告)日：2010-09-16

    申请号：US12225249

    申请日：2007-11-06

    申请人： Tetsu Yamakawa ,  Kyoko Yamamoto ,  Daisuke Uraguchi ,  Kenji Tokuhisa

    发明人： Tetsu Yamakawa ,  Kyoko Yamamoto ,  Daisuke Uraguchi ,  Kenji Tokuhisa

    IPC分类号： C09K3/00

    CPC分类号： C07C209/74 ,  C07C17/32 ,  C07D213/64 ,  C07D231/12 ,  C07D239/54 ,  C07D473/16 ,  C07D473/18 ,  C07C211/52

    摘要： Provided is a reaction reagent for trifluoromethylation with high general versatility and good efficiency.The reaction reagent for trifluoromethylation contains an iron compound, trifluoromethyl iodide, a sulfoxide and a peroxide, and may further contain an acid. The iron compound is, for example, iron(II) sulfate, ammonium iron(II) sulfate, iron(II) tetrafluoroborate, ferrocene, bis(η5-pentamethylcyclopentadienyl)iron or an iron powder; the sulfoxide is, for example, dimethyl sulfoxide; the peroxide is, for example, hydrogen peroxide or hydrogen peroxide-urea composite; and the acid is, for example, sulfuric acid, tetrafluoroboric acid or trifluoromethanesulfonic acid.

    摘要翻译： 提供具有高通用性和高效率的三氟甲基化反应试剂。 用于三氟甲基化的反应试剂含有铁化合物，三氟甲基碘化物，亚砜和过氧化物，并且还可以含有酸。 铁化合物是例如硫酸铁（II），硫酸铁（II），四氟硼酸铁（II），二茂铁，双（5-五甲基环戊二烯基）铁或铁粉; 亚砜是例如二甲基亚砜; 过氧化物是例如过氧化氢或过氧化氢 - 尿素复合物; 酸是例如硫酸，四氟硼酸或三氟甲磺酸。

    Fluorine-containing polymerisable monomer and polymer prepared by using same
    5.
    发明申请
    Fluorine-containing polymerisable monomer and polymer prepared by using same 有权
    含氟可聚合单体和使用它制备的聚合物

    公开(公告)号：US20060252897A1

    公开(公告)日：2006-11-09

    申请号：US11485422

    申请日：2006-07-13

    申请人： Satoru Miyazawa ,  Kazuhiko Maeda ,  Kenji Tokuhisa ,  Shoji Arai

    发明人： Satoru Miyazawa ,  Kazuhiko Maeda ,  Kenji Tokuhisa ,  Shoji Arai

    IPC分类号： C08F220/22

    CPC分类号： G03F7/0046 ,  C07C69/65 ,  C07C69/653 ,  C07C69/96 ,  C07C2601/14 ,  C07C2602/42 ,  C08F20/22 ,  C08F20/26 ,  C08F220/24 ,  G03F7/0392 ,  G03F7/0397

    摘要： The present invention relates to a polymerizable monomer represented by the general formula (1), wherein R1 is a hydrogen atom, a halogen atom, a hydrocarbon group or a fluorine-containing alkyl group; R2 is a straight-chain or branched alkyl group, a cyclic alkyl group, an aromatic group, or a substituent having at least two of these groups, the R2 being optionally partially fluorinated; R3 is a hydrogen atom, a hydrocarbon group that is optionally branched, a fluorine-containing alkyl group, or a cyclic group having an aromatic or alicyclic structure, the R3 optionally containing a bond of an oxygen atom or carbonyl group; and n is an integer of 1-2.

    摘要翻译： 本发明涉及由通式（1）表示的可聚合单体，其中R 1是氢原子，卤素原子，烃基或含氟烷基; R 2是直链或支链烷基，环状烷基，芳族基团或具有这些基团中的至少两个的取代基，R 2是 任选部分氟化; R 3是氢原子，任选支链的烃基，含氟烷基或具有芳族或脂环结构的环状基团，R 3， 任选地含有氧原子或羰基的键; n为1-2的整数。

    Method for producing fluorine-containing acrylate
    7.
    发明申请
    Method for producing fluorine-containing acrylate 有权
    含氟丙烯酸酯的制造方法

    公开(公告)号：US20060122423A1

    公开(公告)日：2006-06-08

    申请号：US10550387

    申请日：2004-03-24

    申请人： Takamasa Fuchikami ,  Noriko Wakasa ,  Kenji Tokuhisa ,  Hideyuki Mimura ,  Shoji Arai

    发明人： Takamasa Fuchikami ,  Noriko Wakasa ,  Kenji Tokuhisa ,  Hideyuki Mimura ,  Shoji Arai

    IPC分类号： C07C51/14

    CPC分类号： C07C67/36 ,  C07C2601/14 ,  C07C2601/18 ,  C07C2603/74 ,  C07C69/653

    摘要： A process for producing a fluorine-containing acrylic acid ester represented by CH2═C(Rf)(COOR) characterized in that 1-bromo-1-perfluoroalkylethene represented by CH2═CBr—Rf, or 1,2-dibromo-1-perfluoroalkylethane represented by CH2CBr—CHBr—Rf is allowed to react with an alcohol represented by ROH in the presence of a palladium catalyst, carbon monoxide, and two or more kinds of bases. The fluorine-containing acrylic acid ester is a useful compound having wide applications in materials for pharmaceuticals and functional polymers.

    摘要翻译： 一种由CH 2 -C（Rf）（COOR）表示的含氟丙烯酸酯的制备方法，其特征在于由CH 2表示的1-溴-1-全氟烷基乙烯基 将由CH 2 CO 2 CBr-CHBr-Rf表示的-CBr-Rf或1,2-二溴-1-全氟烷基乙烷与由ROH表示的醇在钯催化剂存在下反应， 一氧化碳和两种或更多种碱。 含氟丙烯酸酯是广泛用于药物和功能聚合物的材料的有用化合物。

    Fluorine-containing polymerisable monomer and polymer prepared by using same
    9.
    发明授权
    Fluorine-containing polymerisable monomer and polymer prepared by using same 有权
    含氟可聚合单体和使用它制备的聚合物

    公开(公告)号：US07759440B2

    公开(公告)日：2010-07-20

    申请号：US11485422

    申请日：2006-07-13

    申请人： Satoru Miyazawa ,  Kazuhiko Maeda ,  Kenji Tokuhisa ,  Shoji Arai

    发明人： Satoru Miyazawa ,  Kazuhiko Maeda ,  Kenji Tokuhisa ,  Shoji Arai

    IPC分类号： C08F120/22

    CPC分类号： G03F7/0046 ,  C07C69/65 ,  C07C69/653 ,  C07C69/96 ,  C07C2601/14 ,  C07C2602/42 ,  C08F20/22 ,  C08F20/26 ,  C08F220/24 ,  G03F7/0392 ,  G03F7/0397

    摘要： The present invention relates to a polymerizable monomer represented by the general formula (1), wherein R1 is a hydrogen atom, a halogen atom, a hydrocarbon group or a fluorine-containing alkyl group; R2 is a straight-chain or branched alkyl group, a cyclic alkyl group, an aromatic group, or a substituent having at least two of these groups, the R2 being optionally partially fluorinated; R3 is a hydrogen atom, a hydrocarbon group that is optionally branched, a fluorine-containing alkyl group, or a cyclic group having an aromatic or alicyclic structure, the R3 optionally containing a bond of an oxygen atom or carbonyl group; and n is an integer of 1-2.

    摘要翻译： 本发明涉及由通式（1）表示的可聚合单体，其中R1是氢原子，卤素原子，烃基或含氟烷基; R2是直链或支链烷基，环状烷基，芳族基团或具有这些基团中至少两个的取代基，R2任选地部分氟化; R3是氢原子，任选支化的烃基，含氟烷基或具有芳族或脂环结构的环状基团，R3任选地含有氧原子或羰基的键; n为1-2的整数。