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公开(公告)号:US07605297B2
公开(公告)日:2009-10-20
申请号:US10565187
申请日:2004-07-03
申请人: Matthias Maase , Manuel Budich , Georg Groβmann , Laszlo Szarvas
发明人: Matthias Maase , Manuel Budich , Georg Groβmann , Laszlo Szarvas
IPC分类号: A62D3/36
CPC分类号: C07B63/00 , Y02P20/542
摘要: The invention relates to a process for the extractive removal of phenols, alcohols, amines, phoshines, hydroxylamines, hydrazines, oximes, imines, water, carboxylic acids, amino acids, hydroxamic acids, sulfinic acids, sulfonic acids, peroxycarboxylic acids, phosphonous acids, phosphinous acids, phosphonic acids, phosphinic acids or phosphoric acids from aprotic solvents by means of ionic liquids of the formula [K]n+[A]n−, where n, [K]+ and An− are defined as in the description.
摘要翻译: 本发明涉及一种用于萃取去除酚,醇,胺,磷,羟胺,肼,肟,亚胺,水,羧酸,氨基酸,异羟肟酸,亚磺酸,磺酸,过氧羧酸,膦酸, 通过式[K] n + [A] n-,其中n,[K] +和An-的离子液体由非质子传递溶剂中的膦酸,次膦酸或次膦酸或磷酸定义如说明书中所定义。
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公开(公告)号:US20070254822A1
公开(公告)日:2007-11-01
申请号:US11597106
申请日:2005-05-27
IPC分类号: C07C209/68
CPC分类号: C07C209/22 , C07C213/08 , C07D295/023 , C07D295/037 , C07C211/63 , C07C215/40
摘要: The present invention relates to a process for preparing quaternary ammonium compounds, which comprises reacting compounds comprising an sp3-hybridized nitrogen atom with a dialkyl sulfate or trialkyl phosphate and subjecting the resulting ammonium compound to an anion exchange.
摘要翻译: 本发明涉及一种制备季铵化合物的方法,该方法包括使包含sp 3+杂化氮原子的化合物与硫酸二烷基酯或磷酸三烷基酯反应并使所得铵化合物进行阴离子交换。
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公开(公告)号:US20070142646A1
公开(公告)日:2007-06-21
申请号:US10587248
申请日:2005-01-26
申请人: Matthias Maase , Klemens Massone , Laszlo Szarvas
发明人: Matthias Maase , Klemens Massone , Laszlo Szarvas
IPC分类号: C07D233/02 , C07D213/06
CPC分类号: C07D233/56
摘要: In the process for preparing ionic liquids, an ionic liquid is firstly reacted with an alkoxide or with barium hydroxide and is subsequently neutralized with an acid. The ionic liquid contains a phosphonium and/or ammonium cation and an anion selected from the group consisting of halides, arylsulfonates, alkylsulfonates, sulfate, hydroxysulfate, alkylsulfates, hydrogencarbonate, carbonate. triflate and carboxylates. In this process, virtually any anions can be introduced into the ionic liquids.
摘要翻译: 在制备离子液体的过程中,首先使离子液体与醇盐或氢氧化钡反应,随后用酸中和。 离子液体含有鏻和/或铵阳离子和选自卤化物,芳基磺酸盐,烷基磺酸盐,硫酸盐,羟基硫酸盐,烷基硫酸盐,碳酸氢盐,碳酸盐的阴离子。 三氟甲磺酸酯和羧酸盐。 在这个过程中,几乎可以将任何阴离子引入到离子液体中。
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公开(公告)号:US07084298B2
公开(公告)日:2006-08-01
申请号:US10451740
申请日:2002-01-11
CPC分类号: C07F9/3808
摘要: The present invention relates to a process for the preparation of N-phosphonomethyliminodiacetic acid by reacting an alkali metal salt of iminodiacetic acid with phosphorus trichloride in aqueous solution with formation of the hydrochloride of iminodiacetic acid, phosphorous acid and of the corresponding alkali metal chloride, followed by reaction with a formaldehyde source and, if desired, recovery of the N-phosphonomethyliminodiacetic acid from the reaction mixture, in which water, which may comprise HCl, is removed from the reaction mixture during and/or after reacting the alkali metal salt of iminodiacetic acid with phosphorus trichloride until the concentration of iminodiacetic acid hydrochloride is at least 40% by weight, based on the weight of the reaction mixture minus the weight of alkali metal chloride.The process makes possible the preparation of N-phosphonomethyliminodiacetic acid in a simple fashion and in high yield.
摘要翻译: 本发明涉及一种通过将亚氨基二乙酸的碱金属盐与三氯化磷在水溶液中反应制备N-膦酰甲基亚氨基二乙酸的方法,形成亚氨基二乙酸,亚磷酸和相应的碱金属氯化物的盐酸盐,随后 通过与甲醛源反应,并且如果需要,从反应混合物中回收N-膦酰甲基亚氨基二乙酸,其中可以包含HCl的水在反应混合物中和/或之后反应亚氨基二乙酸的碱金属盐 酸与三氯化磷直到亚氨基二乙酸盐酸盐的浓度为至少40重量%,基于反应混合物的重量减去碱金属氯化物的重量。 该方法可以以简单的方式以高产率制备N-膦酰基甲基亚氨基二乙酸。
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公开(公告)号:US08193297B2
公开(公告)日:2012-06-05
申请号:US12602724
申请日:2008-06-06
申请人: Lars Wittenbecher , Matthias Maase , Georg Degen , Michael Henningsen , Manfred Doering , Ulrich Arnold
发明人: Lars Wittenbecher , Matthias Maase , Georg Degen , Michael Henningsen , Manfred Doering , Ulrich Arnold
CPC分类号: C08G59/686
摘要: The use of 1,3-substituted imidazolium salts of the formula I in which R1 and R3 independently of one another are an organic radical having 1 to 20 C atoms, R2, R4, and R5 independently of one another are an H atom or an organic radical having 1 to 20 C atoms, it also being possible for R4 and R5 together to form an aliphatic or aromatic ring, and X is a thiocyanate anion as latent catalysts for curing compositions comprising epoxy compounds.
摘要翻译: 其中R 1和R 3彼此独立地是具有1至20个C原子的有机基团,R 2,R 4和R 5彼此独立的式I的1,3-取代咪唑盐是H原子或 具有1至20个C原子的有机基团,R4和R5一起形成脂族或芳族环,X是硫氰酸根阴离子作为用于固化包含环氧化合物的组合物的潜在催化剂。
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公开(公告)号:US20100267596A1
公开(公告)日:2010-10-21
申请号:US12747372
申请日:2008-12-12
申请人: Georg Degen , Veit Stegmann , Klaus Ebel , Klemens Massonne , Laszlo Szarvas , Uwe Vagt , Matthias Maase
发明人: Georg Degen , Veit Stegmann , Klaus Ebel , Klemens Massonne , Laszlo Szarvas , Uwe Vagt , Matthias Maase
IPC分类号: C07D207/24 , C02F5/10 , C09K3/00 , B01F1/00 , B01J31/02 , H01M4/88 , C09K5/04 , G01N33/00 , C07K1/26
CPC分类号: C07D233/58 , C07D233/56
摘要: The present invention relates to a method for improving the hydrolysis stability of an ionic liquid (IL), in which at least one tertiary amine or one quaternary ammonium compound different from the ionic liquid (IL) is added to an ionic liquid (IL).
摘要翻译: 本发明涉及一种提高离子液体(IL)的水解稳定性的方法,其中将至少一种不同于离子液体的叔胺或一种季铵化合物(IL)加入到离子液体(IL)中。
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公开(公告)号:US20100209708A1
公开(公告)日:2010-08-19
申请号:US12676488
申请日:2008-09-09
申请人: Markus Braun , Rainer Dyllick-Brenzinger , Matthias Maase , Frank Stein , Megan Turner , Eric Uerdingen
发明人: Markus Braun , Rainer Dyllick-Brenzinger , Matthias Maase , Frank Stein , Megan Turner , Eric Uerdingen
CPC分类号: C08J3/24 , C08H8/00 , C08J2301/02 , C08J2397/02 , Y10T428/2982
摘要: Crosslinked cellulose beads or lignocellulose beads (referred to as beads for short), wherein at least 50% by weight of the beads have a particle diameter greater than 800 μm (21° C., 1 bar, determined by sieve analysis).
摘要翻译: 交联的纤维素珠或木质纤维素珠(简称为珠),其中至少50重量%的珠具有大于800μm的粒径(21℃,1巴,通过筛分分析确定)。
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公开(公告)号:US20100179299A1
公开(公告)日:2010-07-15
申请号:US12602724
申请日:2008-06-06
申请人: Lars Wittenbecher , Matthias Maase , Georg Degen , Michael Henningsen , Manfred Doering , Ulrich Arnold
发明人: Lars Wittenbecher , Matthias Maase , Georg Degen , Michael Henningsen , Manfred Doering , Ulrich Arnold
IPC分类号: C08G59/68
CPC分类号: C08G59/686
摘要: The use of 1,3-substituted imidazolium salts of the formula I in which R1 and R3 independently of one another are an organic radical having 1 to 20 C atoms, R2, R4, and R5 independently of one another are an H atom or an organic radical having 1 to 20 C atoms, it also being possible for R4 and R5 together to form an aliphatic or aromatic ring, and X is a thiocyanate anion as latent catalysts for curing compositions comprising epoxy compounds.
摘要翻译: 其中R 1和R 3彼此独立地是具有1至20个C原子的有机基团,R 2,R 4和R 5彼此独立的式I的1,3-取代咪唑盐是H原子或 具有1至20个C原子的有机基团,R4和R5一起形成脂族或芳族环,X是硫氰酸根阴离子作为用于固化包含环氧化合物的组合物的潜在催化剂。
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公开(公告)号:US20080287684A1
公开(公告)日:2008-11-20
申请号:US12094411
申请日:2006-11-15
IPC分类号: C07D233/54
CPC分类号: C07D233/56 , C07D295/03
摘要: The present invention describes a process for preparing ionic liquids (I) by reacting ionic liquids (II) whose anion is a halide with an acid (III), with the resulting hydrogen halide being scavenged by means of an amine and the resulting ammonium halide being able to be separated off.
摘要翻译: 本发明描述了通过使阴离子是卤化物的离子液体(II)与酸(III)反应制备离子液体(I)的方法,所得到的卤化氢通过胺被清除,所得的卤化铵是 能分开。
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10.
公开(公告)号:US20080164440A1
公开(公告)日:2008-07-10
申请号:US11911586
申请日:2006-04-12
申请人: Matthias Maase , Veit Stegmann
发明人: Matthias Maase , Veit Stegmann
IPC分类号: C09K3/00
CPC分类号: C08J3/096 , C08B1/003 , C08J2301/02 , Y02P20/542
摘要: The present invention relates to a solution comprising cellulose, an ionic liquid comprising anions and cations as solvent and 6-30% by weight of a nitrogen-comprising base, based on the total weight of the solution, its preparation and also its use for the physical or chemical treatment of cellulose.
摘要翻译: 本发明涉及包含纤维素,包含阴离子和阳离子作为溶剂的离子液体和基于溶液的总重量的6-30重量%的含氮基质的溶液,其制备方法及其用于 纤维素的物理或化学处理。
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