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公开(公告)号：US08168155B2
公开(公告)日：2012-05-01
申请号：US12524968
申请日：2008-01-29
IPC分类号： C01G41/02
CPC分类号： C01G41/00 , C01P2002/60 , C01P2002/88 , C01P2004/54 , C01P2006/10 , C01P2006/11 , C01P2006/80
摘要： The invention is directed to a method for the production of ammonium paratungstate tetrahydrate by thermal treatment of ammonium paratungstate decahydrate in an aqueous suspension. The ammonium paratungstate tetrahydrate can be produced with high purity and high yield. The production method may furthermore be carried out in a simple and energy-efficient manner.
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2.发明申请公开(公告)号：US20100028250A1
公开(公告)日：2010-02-04
申请号：US12524968
申请日：2008-01-29
IPC分类号： C01G41/00
CPC分类号： C01G41/00 , C01P2002/60 , C01P2002/88 , C01P2004/54 , C01P2006/10 , C01P2006/11 , C01P2006/80
摘要： The invention is directed to a method for the production of ammonium paratungstate tetrahydrate by thermal treatment of ammonium paratungstate decahydrate in an aqueous suspension. The ammonium paratungstate tetrahydrate can be produced with high purity and high yield. The production method may furthermore be carried out in a simple and energy-efficient manner.
摘要翻译： 本发明涉及一种通过在水性悬浮液中热处理仲钨酸铵十水合物生产仲钨酸铵的方法。 仲钨酸铵四水合物可以纯度高，产率高。 此外，制造方法还可以以简单且节能的方式进行。
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公开(公告)号：US08440161B2
公开(公告)日：2013-05-14
申请号：US13482075
申请日：2012-05-29
申请人： Viktor Stoller , Michael Erb , Juliane Meese-Marktscheffel , Michael Lohse , Klaus-Jürgen Marschall , Frank Schrumpf
发明人： Viktor Stoller , Michael Erb , Juliane Meese-Marktscheffel , Michael Lohse , Klaus-Jürgen Marschall , Frank Schrumpf
IPC分类号： C01G41/02
CPC分类号： C01G41/00 , C01G41/003 , C01P2002/01 , C01P2002/60 , C01P2002/72 , C01P2004/03 , C01P2004/54 , C01P2006/10 , C01P2006/11 , C01P2006/80 , Y10T428/2982
摘要： The invention is directed to ammonium paratungstate decahydrate containing at least 75% of crystals having a length of at least 200 μm and having a ratio of length to width of less than 4.5:1.
摘要翻译： 本发明涉及含有至少75％长度至少为200μm的晶体并具有小于4.5:1的长宽比的仲仲钨酸铵。
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公开(公告)号：US08431107B2
公开(公告)日：2013-04-30
申请号：US12524976
申请日：2008-01-29
IPC分类号： C01G39/02
CPC分类号： C01G39/003 , C01G39/00
摘要： A method for preparing ammonium heptamolybdate with the steps of: i) adding a molybdenum-containing organic phase to a liquid-liquid reextraction apparatus or to a desorption apparatus, and ii) directly cold-crystallization ammonium heptamolybdate by cooling the resulting reextraction or desorption solution.
摘要翻译： 一种制备七钼酸铵的方法，其步骤为：i）向液 - 液再萃取装置或解吸装置中加入含钼有机相，和ii）通过冷却所得的再萃取或解吸溶液直接冷结晶七钼酸铵 。
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公开(公告)号：US20090255372A1
公开(公告)日：2009-10-15
申请号：US12306853
申请日：2007-06-29
申请人： Armin Olbrich , Juliane Meese-Marktscheffel , Matthias Jahn , Rüdiger Zertani , Viktor Stoller , Michael Erb , Karl-Heinz Heine , Uwe Kutzler
发明人： Armin Olbrich , Juliane Meese-Marktscheffel , Matthias Jahn , Rüdiger Zertani , Viktor Stoller , Michael Erb , Karl-Heinz Heine , Uwe Kutzler
CPC分类号： C22B34/36 , C01G41/00 , C01G47/00 , C22B1/06 , C22B7/001 , C22B23/026 , C22B61/00 , Y02P10/214 , Y02P10/218 , Y02P10/224 , Y02P10/23
摘要： The invention relates to a process for recovering valuable metals from a superalloy which has the steps of digesting the superalloy in a salt melt. The salt melt contains 60-95% by weight of NaOH and 5-40% by weight of Na2SO4.
摘要翻译： 本发明涉及一种从超级合金中回收有价值金属的方法，该方法具有在盐熔体中消化超合金的步骤。 盐熔体含有60-95重量％的NaOH和5-40重量％的Na 2 SO 4。
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6.发明授权Method for producing ammonium paratungstate hydrates and ammonium paratungstate decahydrate 有权生产仲钨酸铵水合物和仲钨酸铵十水合物的方法公开(公告)号：US08216533B2
公开(公告)日：2012-07-10
申请号：US12524957
申请日：2008-01-29
申请人： Viktor Stoller , Michael Erb , Juliane Meese-Marktscheffel , Michael Lohse , Klaus-Jürgen Marschall , Frank Schrumpf
发明人： Viktor Stoller , Michael Erb , Juliane Meese-Marktscheffel , Michael Lohse , Klaus-Jürgen Marschall , Frank Schrumpf
CPC分类号： C01G41/00 , C01G41/003 , C01P2002/01 , C01P2002/60 , C01P2002/72 , C01P2004/03 , C01P2004/54 , C01P2006/10 , C01P2006/11 , C01P2006/80 , Y10T428/2982
摘要： The invention is directed to a process for the continuous preparation of ammonium paratungstate hydrate by back reextraction of a tungsten-laden organic phase with an ammonia-containing aqueous solution in a mixer-settler apparatus. The reextraction is carried out at an NH3:W molar ratio of from 0.83 to 1.30, and a volume feed ratio of the tungsten-laden organic phase to the ammonia-containing aqueous solution of from 5 to 25. The above crystalline is in high purity and in high yield. The production method can be carried out in a simple and energy-efficient manner.
摘要翻译： 本发明涉及一种连续制备仲钨酸铵水合物的方法，该方法是通过在混合器 - 沉降器装置中用含氨水溶液反萃取含钨载体的有机相。 再提取的NH 3 :W摩尔比为0.83〜1.30，载有钨的有机相与含氨水溶液的体积进料比为5〜25。上述结晶为高纯度 并以高产量。 生产方法可以简单，节能的方式进行。
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7.发明申请METHOD FOR PRODUCTION OF AMMONIUM PARATUNGSTATE TETRAHYDRATE AND HIGHLY PURE AMMONIUM PARATUNGSTATE TETRAHYDRATE 有权生产甲基四氢OF OF ATE ATE ATE ATE ATE ATE ATE ATE ATE ATE ATE ATE ATE ATE ATE ATE ATE公开(公告)号：US20110070148A1
公开(公告)日：2011-03-24
申请号：US12945038
申请日：2010-11-12
IPC分类号： C01G41/02
CPC分类号： C01G41/00 , C01P2002/60 , C01P2002/88 , C01P2004/54 , C01P2006/10 , C01P2006/11 , C01P2006/80
摘要： The invention is directed to a method for the production of ammonium paratungstate tetrahydrate by thermal treatment of ammonium paratungstate decahydrate in an aqueous suspension. The ammonium paratungstate tetrahydrate can be produced with high purity and high yield. The production method may furthermore be carried out in a simple and energy-efficient manner.
摘要翻译： 本发明涉及一种通过在水性悬浮液中热处理仲钨酸铵十水合物生产仲钨酸铵的方法。 仲钨酸铵四水合物可以纯度高，产率高。 此外，制造方法还可以以简单且节能的方式进行。
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8.发明申请公开(公告)号：US20100098619A1
公开(公告)日：2010-04-22
申请号：US12524957
申请日：2008-01-29
申请人： Viktor Stoller , Michael Erb , Juliane Meese-Marktscheffel , Michael Lohse , Klaus-Jürgen Marschall , Frank Schrumpf
发明人： Viktor Stoller , Michael Erb , Juliane Meese-Marktscheffel , Michael Lohse , Klaus-Jürgen Marschall , Frank Schrumpf
IPC分类号： C01G41/02
CPC分类号： C01G41/00 , C01G41/003 , C01P2002/01 , C01P2002/60 , C01P2002/72 , C01P2004/03 , C01P2004/54 , C01P2006/10 , C01P2006/11 , C01P2006/80 , Y10T428/2982
摘要： The invention is directed to a process for the continuous preparation of ammonium paratungstate hydrate by back reextraction of a tungsten-laden organic phase with an ammonia-containing aqueous solution in a mixer-settler apparatus. The reextraction is carried out at an NH3:W molar ratio of from 0.83 to 1.30, and a volume feed ratio of the tungsten-laden organic phase to the ammonia-containing aqueous solution of from 5 to 25. The above crystalline is in high purity and in high yield. The production method can be carried out in a simple and energy-efficient manner.
摘要翻译： 本发明涉及一种连续制备仲钨酸铵水合物的方法，该方法是通过在混合器 - 沉降器装置中用含氨水溶液反萃取含钨载体的有机相。 再提取的NH 3 :W摩尔比为0.83〜1.30，载有钨的有机相与含氨水溶液的体积进料比为5〜25。上述结晶为高纯度 并以高产量。 生产方法可以简单，节能的方式进行。
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公开(公告)号：US20100008846A1
公开(公告)日：2010-01-14
申请号：US12524976
申请日：2008-01-29
IPC分类号： C01G39/00
CPC分类号： C01G39/003 , C01G39/00
摘要： A method for preparing ammonium heptamolybdate with the steps of: i) adding a molybdenum-containing organic phase to a liquid-liquid reextraction apparatus or to a desorption apparatus and adding an ammonia-containing aqueous solution to this reextraction or desorption apparatus, and ii) directly cold-crystallizing ammonium heptamolybdate by cooling the resulting reextraction or desorption solution.
摘要翻译： 一种制备七钼酸铵的方法，其步骤为：i）向液 - 液再萃取装置或解吸装置中加入含钼有机相，并向该再提取或解吸装置中加入含氨水溶液，和ii） 通过冷却所得的再提取或解吸溶液直接冷结晶七钼酸铵。
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公开(公告)号：US07217366B2
公开(公告)日：2007-05-15
申请号：US10935563
申请日：2004-09-07
CPC分类号： C01G39/00 , C22B3/42 , C22B34/34 , Y02P10/234
摘要： A process for reducing the content of alkali metal impurities (e.g., potassium) in ammonium metallate solutions is described. The process involves subjecting a feed solution containing ammonium metallate and alkali metal impurities to membrane filtration. The membrane filtration results in the formation of a retentate having a reduced level alkali metal relative to the feed solution, and a permeate containing substantially the balance of alkali metal. The permeate may also be further treated, to remove alkali metal there from, by passage through a cation exchange column, thereby forming a cation exchange treated permeate that may be combined with the retentate of the membrane filtration step.
摘要翻译： 描述了一种降低金属铵盐溶液中碱金属杂质（例如钾）含量的方法。 该方法包括使含有金属铵盐和碱金属杂质的进料溶液进行膜过滤。 膜过滤导致相对于进料溶液形成具有降低的碱金属含量的渗余物，和形成基本上余量的碱金属的渗透物。 也可以进一步处理渗透物，以通过阳离子交换柱除去碱金属，从而形成阳离子交换处理的渗透物，其可与膜过滤步骤的渗余物组合。
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