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    Polyisocyanates containing allophanate and silane groups
    1.
    发明授权
    Polyisocyanates containing allophanate and silane groups 有权
    含有脲基甲酸酯和硅烷基团的聚异氰酸酯

    公开(公告)号：US07956209B2

    公开(公告)日：2011-06-07

    申请号：US12171737

    申请日：2008-07-11

    Applicant: Hans-Josef Laas ,  Reinhard Halpaap

    Inventor： Hans-Josef Laas ,  Reinhard Halpaap

    IPC: C07F7/18

    CPC classification number: C08G18/289 ,  C07F7/1804 ,  C08G18/7837 ,  C08G71/04

    Abstract: The invention relates to polyisocyanates containing allophanate groups and silane groups, to a process for preparing them and to their use as a starting component in the production of polyurethane polymers, more particularly as a crosslinker component in polyurethane paints and coatings.

    Abstract translation: 本发明涉及含有脲基甲酸酯基团和硅烷基团的多异氰酸酯，其制备方法以及它们在聚氨酯聚合物生产中作为起始成分的用途，更特别地涉及聚氨酯涂料和涂料中的交联剂组分。

    Self-crosslinking polyurethane dispersions and a process for their preparation
    5.
    发明申请
    Self-crosslinking polyurethane dispersions and a process for their preparation 审中-公开
    自交联聚氨酯分散体及其制备方法

    公开(公告)号：US20070004856A1

    公开(公告)日：2007-01-04

    申请号：US11475691

    申请日：2006-06-27

    Applicant: Jan Mazanek ,  Dorota Greszta-Franz ,  Sebastian Dorr ,  Jurgen Meixner ,  Reinhard Halpaap ,  Helmut Muller ,  Olaf Fleck ,  Heino Muller

    Inventor： Jan Mazanek ,  Dorota Greszta-Franz ,  Sebastian Dorr ,  Jurgen Meixner ,  Reinhard Halpaap ,  Helmut Muller ,  Olaf Fleck ,  Heino Muller

    IPC: C08G18/08

    CPC classification number: C08G18/8064 ,  C08G18/0823 ,  C08G18/4219 ,  C08G18/8048 ,  C08G18/807 ,  C08G18/8077 ,  C09D175/06

    Abstract: The present invention relates to a process for preparing self-crosslinking polyurethane dispersions by I) reacting a1) polyisocyanates with a2) at least one hydroxyl component having an average OH functionality of ≧2 and a number average molecular weight of 62 to 2500 g/mol, wherein the hydroxyl component contains at least one acid-functional compound containing at least one isocyanate-reactive group, to form an NCO-functional and optionally OH-functional prepolymer, II) then reacting the NCO-functional and optionally OH-functional prepolymer with a3) a hydroxyl component having an average OH functionality of >1 and a4) optionally another polyisocyanate component, which may be the same as or different from a1), to form an OH-functional and NCO-free polyurethane, III) adding a blocked polyisocyanate either before, during or after the reaction of steps I) and II), or forming a blocked polyisocyanate in situ from a polyisocyanate and a blocking agent after the reaction of step II) has taken place, IV) neutralizing the acid groups of the resulting composition by adding a5) a neutralizing agent, and V) dispersing the resulting composition in water. The present invention also relates to the dispersions prepared by the present invention and to their use in coating, adhesive and sealant compositions.

    Abstract translation: 本发明涉及一种制备自交联聚氨酯分散体的方法，其方法是使a1）多异氰酸酯与a2）至少一种平均OH官能度> = 2，数均分子量为62〜2500g / mol，其中所述羟基组分含有至少一种含有至少一个异氰酸酯反应性基团的酸官能化合物，以形成NCO-官能和任选的OH-官能预聚物，II）然后使所述NCO-官能和任选的OH-官能预聚物 其中a3）具有平均OH官能度> 1的羟基组分和a4）任选地可以与a1）相同或不同的另一种多异氰酸酯组分，以形成OH-官能和无NCO的聚氨酯，III）加入 在步骤I）和II）的反应之前，期间或之后封闭的多异氰酸酯，或在步骤II）的反应之后由多异氰酸酯和封闭剂原位形成封端多异氰酸酯具有ta 呃地方，IV）通过添加a）中和剂中和所得组合物的酸基，和V）将得到的组合物分散在水中。 本发明还涉及由本发明制备的分散体及其在涂料，粘合剂和密封剂组合物中的用途。

    Process for the production of light-colored uretdione polyisocyanates
    8.
    发明授权
    Process for the production of light-colored uretdione polyisocyanates 有权
    生产浅色脲二酮多异氰酸酯的方法

    公开(公告)号：US6043332A

    公开(公告)日：2000-03-28

    申请号：US129584

    申请日：1998-08-05

    Applicant: Hans-Josef Laas ,  Reinhard Halpaap ,  Hans-Ulrich Meier-Westhues ,  Ulrich Freudenberg

    Inventor： Hans-Josef Laas ,  Reinhard Halpaap ,  Hans-Ulrich Meier-Westhues ,  Ulrich Freudenberg

    IPC: C08G18/02 ,  C08G18/16 ,  C08G18/79 ,  C08K5/524 ,  C09D5/46 ,  C08G18/00 ,  C07D229/00 ,  C07D273/00 ,  C08G18/08 ,  C08G18/22

    CPC classification number: C08G18/798 ,  C08G18/027 ,  C08G18/168 ,  C08K5/524 ,  C08G2150/20

    Abstract: The present invention relates to a process for the production of polyisocyanates containing uretdione groups bya) oligomerizing a portion of the isocyanate groups of diisocyanates having aliphatically and/or cycloaliphatically bound isocyanate groups in the presence of catalysts or catalyst systems which accelerate the dimerization of isocyanate groups and in the presence of trisubstituted phosphite stabilizers corresponding to formula (I) ##STR1## b) optionally termination of the oligomerization reaction at a degree of oligomerization of 10 to 60% by adding a catalyst poison andc) optionally removing unreacted diisocyanate by extraction or thin-layer distillation.The present invention also relates to the use of the resulting uretdione polyisocyanates as a starting component for polyurethane plastics, particularly as an isocyanate component for the production of uretdione hardeners for powder coating compositions.

    Abstract translation: 本发明涉及一种通过以下方法生产含脲二酮基团的多异氰酸酯的方法：a）在催化剂或催化剂体系存在下使一部分具有脂族和/或环状结合的异氰酸酯基团的异氰酸酯基团的异氰酸酯基团低聚，这加快了异氰酸酯的二聚 并且在对应于式（I）的三取代的亚磷酸酯稳定剂的存在下，b）通过加入催化剂毒物以10至60％的低聚度任意地终止低聚反应，和c）任选地通过萃取或稀释除去未反应的二异氰酸酯， 层蒸馏。 本发明还涉及使用所得的脲二酮多异氰酸酯作为聚氨酯塑料的起始组分，特别是作为制备用于粉末涂料组合物的脲二酮硬化剂的异氰酸酯组分。

    Polyurethane powder coating compositions which have a low stoving temperature
    9.
    发明授权
    Polyurethane powder coating compositions which have a low stoving temperature 失效
    具有低烘烤温度的聚氨酯粉末涂料组合物

    公开(公告)号：US5847044A

    公开(公告)日：1998-12-08

    申请号：US834799

    申请日：1997-04-03

    Applicant: Hans-Josef Laas ,  Hans-Ulrich Meier-Westhues ,  Reinhard Halpaap ,  Ulrich Freudenberg ,  Hans-Peter Klee

    Inventor： Hans-Josef Laas ,  Hans-Ulrich Meier-Westhues ,  Reinhard Halpaap ,  Ulrich Freudenberg ,  Hans-Peter Klee

    IPC: C08G18/18 ,  C08G18/20 ,  C08G18/32 ,  C08G18/40 ,  C08G18/42 ,  C08G18/79 ,  C09D5/03 ,  C09D5/46 ,  C09D175/04 ,  C08J3/00 ,  C08K3/20 ,  C08L75/00

    CPC classification number: C08G18/798 ,  C08G18/1858 ,  C08G18/2063 ,  C08G18/4219 ,  C08G2150/20 ,  Y10T428/31551

    Abstract: The present invention relates to a polyurethane powder coating composition containing A) a binder component which is solid below 40.degree. C. and liquid above 130.degree. C. and has an OH number of 25 to 200 and a number average molecular weight of 400 to 10,000, B) a polyaddition compound which is solid below 40.degree. C. and liquid above 125.degree. C., contains uretdione groups and optionally free isocyanate groups and is prepared from aliphatic and/or cycloaliphatic diisocyanates and C) one or more catalysts containing N,N,N'-trisubstituted amidine groups which have an amidine group content (calculated as CN.sub.2 ; molecular weight=40) of 12.0 to 47.0 wt. %, provided that components A) and B) are present in amounts such that component B) has 0.6 to 1.4 isocyanate groups for each hydroxyl group present in component A) and the amount of component C) is 0.05 to 5 wt. %, based on the total weight of the coating composition. The present invention also relates to the use of this powder coating composition for coating heat resistant substrates.

    Abstract translation: 本发明涉及一种聚氨酯粉末涂料组合物，其包含A）粘合剂组分，其固体低于40℃，液体高于130℃，OH值为25至200，数均分子量为400至10,000 B）固体低于40℃，液体高于125℃的加聚化合物含有脲二酮基团和任选的游离异氰酸酯基团，并由脂族和/或脂环族二异氰酸酯制备，和C）一种或多种含N， 具有脒基含量（以CN2计算;分子量= 40）为12.0〜47.0重量％的N，N'-三取代脒基。 ％，条件是组分A）和B）的存在量使得组分B）对于组分A）中存在的每个羟基具有0.6至1.4个异氰酸酯基团，并且组分C）的量为0.05至5重量％ ％，基于涂料组合物的总重量。 本发明还涉及这种粉末涂料组合物用于涂覆耐热基材的用途。

    Matt polyurethane powder coatings and their use for coating heat resistant substrates
    10.
    发明授权
    Matt polyurethane powder coatings and their use for coating heat resistant substrates 失效
    马特聚氨酯粉末涂料及其用于涂覆耐热基材的用途

    公开(公告)号：US5811190A

    公开(公告)日：1998-09-22

    申请号：US794256

    申请日：1997-01-31

    Applicant: Hans-Josef Laas ,  Hans-Ulrich Meier-Westhues ,  Reinhard Halpaap ,  Ulrich Freudenberg ,  Hans-Peter Klee

    Inventor： Hans-Josef Laas ,  Hans-Ulrich Meier-Westhues ,  Reinhard Halpaap ,  Ulrich Freudenberg ,  Hans-Peter Klee

    IPC: C08G18/38 ,  C08G18/42 ,  C08G18/58 ,  C08G18/65 ,  C08G18/79 ,  C08G18/80 ,  C09D5/00 ,  C09D5/03 ,  C09D5/46 ,  C09D175/00 ,  C09D175/04 ,  C09D175/06 ,  C08L33/06 ,  C08L67/02 ,  C08L75/04

    CPC classification number: C08G18/807 ,  C08G18/3825 ,  C08G18/4219 ,  C08G18/6541 ,  C08G18/792 ,  C08G18/8048 ,  C09D175/04 ,  C08G2150/20 ,  Y10S525/934 ,  Y10T428/31551

    Abstract: The present invention relates to a powder coating composition for the production of matt coatings containing as binder A) a component having hydroxyl groups, B) a polyisocyanate having blocked and optionally free isocyanate groups, C) a component having carboxyl groups and/or carboxylic anhydride groups and contains one or more of the following: C1) aliphatic and/or cycloaliphatic dicarboxylic acids having 4 to 20 carbon atoms, C2) monomeric and/or polymeric anhydrides of dicarboxylic acids C1) and C3) aliphatic hydroxycarboxylic acids having 4 to 18 carbon atoms, and D) a component which has groups that are reactive with carboxyl groups and/or carboxylic anhydride groups wherein components A), B), C) and D) are present in amounts such that 1) 0.6 to 1.4 isocyanate groups of component B) are present for each hydroxyl group of component A), 2) 0.3 to 1.5 groups of component D) that are reactive with carboxyl groups and/or carboxylic anhydride groups are present for each carboxyl equivalent of component C) and 3) components C) and D) are present in an amount of 10 to 40 wt. %, based on the total weight of components A), B), C) and D). The invention further relates to heat resistant substrates coated with this powder coating composition.

    Abstract translation: 本发明涉及一种用于生产含有粘合剂的无光泽涂料的粉末涂料组合物，A）具有羟基的组分，B）具有封端和任意游离的异氰酸酯基团的多异氰酸酯，C）具有羧基和/或羧酸酐的组分 基团并且包含以下一种或多种：C1）具有4至20个碳原子的脂族和/或脂环族二羧酸，C2）二羧酸的单体和/或聚合酸酐C1）和C3）具有4至18个碳原子的脂族羟基羧酸 原子和D）具有与羧基和/或羧酸酐基团反应的基团的组分，其中组分A），B），C）和D）的存在量使得1）组分的0.6-1.4个异氰酸酯基 B）对于组分A）的每个羟基存在，2）对于每个羧基等同物存在与羧基和/或羧酸酐基团反应的0.3至1.5组的组分D） 组分C）和3）组分C）和D）以10〜40重量％的量存在。 ％，基于组分A），B），C）和D）的总重量。 本发明还涉及涂覆有该粉末涂料组合物的耐热基材。

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