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公开(公告)号：US20130296612A1
公开(公告)日：2013-11-07
申请号：US13464726
申请日：2012-05-04
Applicant: DANIEL B. POURREAU , ROGER A. GREY , ANDREW P. KAHN
Inventor： DANIEL B. POURREAU , ROGER A. GREY , ANDREW P. KAHN
IPC: C07C45/83 , C07C29/84 , C07C29/145
Abstract: The present invention relates to a method of treating a crude acetone stream. The method generally includes treating a crude acetone stream which has acetone and at least one low-boiling impurity with a catalyst to form a treated acetone stream that has acetone and at least one higher-boiling impurity and then distilling the treated acetone stream to remove at least a portion of the higher-boiling impurity to produce a purified acetone stream. This is particularly helpful in processes where a more pure acetone is desired, including a process for making purified isopropanol.
Abstract translation: 本发明涉及一种处理粗丙酮流的方法。 该方法通常包括用催化剂处理具有丙酮和至少一种低沸点杂质的粗丙酮流，以形成具有丙酮和至少一种较高沸点杂质的经处理的丙酮流，然后蒸馏经处理的丙酮流以在 至少一部分较高沸点的杂质以产生纯化的丙酮流。 这在需要更纯丙酮的方法中尤其有用，包括制备纯化异丙醇的方法。
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公开(公告)号：US08440846B2
公开(公告)日：2013-05-14
申请号：US12894626
申请日：2010-09-30
Applicant: Vu A. Dang , Roger A. Grey , Jay F. Miller , Beaven S. Mandimutsira
Inventor： Vu A. Dang , Roger A. Grey , Jay F. Miller , Beaven S. Mandimutsira
IPC: C07D301/06 , C07D301/12
CPC classification number: C07D301/06
Abstract: The invention is a process for epoxidizing an olefin with hydrogen and oxygen in a solvent comprising acetonitrile in the presence of an quinone-acid salt and a catalyst comprising a titanium zeolite and a noble metal. The process results in higher productivity and improved selectivity to propylene oxide from hydrogen and oxygen, as compared to processes that use only a quinone.
Abstract translation: 本发明是在包含乙酸的溶剂中，在醌 - 酸盐和包含钛沸石和贵金属的催化剂存在下，用氢和氧环氧化烯烃的方法。 与仅使用醌的方法相比，该方法导致更高的生产率和来自氢气和氧气的环氧丙烷的改进选择性。
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公开(公告)号：US07696367B2
公开(公告)日：2010-04-13
申请号：US11784911
申请日：2007-04-10
Applicant: Roger A. Grey , Steven M. Augustine
Inventor： Roger A. Grey , Steven M. Augustine
IPC: C07D301/06 , C07D301/12
CPC classification number: C07D301/06
Abstract: The invention is a process for epoxidizing an olefin with hydrogen and oxygen in the presence of a catalyst mixture containing a titanium or vanadium zeolite and a supported catalyst comprising palladium, gold, and an inorganic oxide carrier. Prior to its use in the epoxidation process, the supported catalyst is calcined in the presence of oxygen at a temperature from 450 to 800° C. and reduced in the presence of hydrogen at a temperature greater than 20° C. The process results in significantly reduced alkane byproduct formed by the hydrogenation of olefin.
Abstract translation: 本发明是在含有钛或钒沸石的催化剂混合物和包含钯，金和无机氧化物载体的载体催化剂存在下，用氢和氧环氧化烯烃的方法。 在其用于环氧化方法之前，将载体催化剂在氧气存在下在450-800℃的温度下煅烧，并在氢气存在下在大于20℃的温度下还原。 由烯烃氢化形成的还原烷烃副产物。
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公开(公告)号：US07671222B2
公开(公告)日：2010-03-02
申请号：US11484906
申请日：2006-07-12
Applicant: Mark P. Kaminsky , Roger A. Grey
Inventor： Mark P. Kaminsky , Roger A. Grey
IPC: C07D301/06 , C07D301/12
CPC classification number: C07D301/06 , B01J21/063 , B01J21/066 , B01J23/6567 , B01J29/89 , B01J35/0006 , B01J35/1014 , B01J37/0205
Abstract: The invention is a process for epoxidizing an olefin with hydrogen and oxygen in the presence of a catalyst mixture containing a titanium or vanadium zeolite and a supported catalyst comprising palladium, rhenium and a carrier. The process results in significantly reduced alkane byproduct formed by the hydrogenation of olefin.
Abstract translation: 本发明是在含有钛或钒沸石的催化剂混合物和包含钯，铼和载体的负载催化剂存在下，用氢和氧环氧化烯烃的方法。 该方法可显着减少由烯烃氢化形成的烷烃副产物。
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公开(公告)号：US07615654B2
公开(公告)日：2009-11-10
申请号：US11254829
申请日：2005-10-20
Applicant: Bi Le-Khac , Mark P. Kaminsky , Kun Qin , Roger A. Grey
Inventor： Bi Le-Khac , Mark P. Kaminsky , Kun Qin , Roger A. Grey
IPC: C07D301/10 , C07D303/00
CPC classification number: C07D301/06
Abstract: A process is disclosed for the epoxidation of an olefin with hydrogen and oxygen in the presence of an oxidation catalyst comprising a transition metal zeolite, and a noble metal catalyst comprising a noble metal and an ion-exchange resin. The process is highly productive and selective in making epoxides. A noble metal catalyst comprising a cation-exchanged resin further improves the productivity and/or the selectivity of the process.
Abstract translation: 公开了在含有过渡金属沸石的氧化催化剂和包含贵金属和离子交换树脂的贵金属催化剂存在下，用氢和氧环氧化烯烃的方法。 该方法在制备环氧化物方面具有高生产率和选择性。 包含阳离子交换树脂的贵金属催化剂进一步提高了工艺的生产率和/或选择性。
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Patent Agency Ranking
公开(公告)号：US07595410B2
公开(公告)日：2009-09-29
申请号：US11489086
申请日：2006-07-18
Applicant: Kun Qin , Roger A. Grey , Peter J. Whitman
Inventor： Kun Qin , Roger A. Grey , Peter J. Whitman
IPC: C07D301/06 , C07D301/12
CPC classification number: C07D301/08 , C07D301/10
Abstract: A process for producing an epoxide comprising reacting an olefin, hydrogen and oxygen in the presence of a catalyst comprising a titanium or vanadium zeolite, palladium, and lead. The process results in significantly reduced alkane by-product formed by the hydrogenation of olefin.
Abstract translation: 一种制备环氧化物的方法，包括在包含钛或钒沸石，钯和铅的催化剂的存在下使烯烃，氢和氧反应。 该方法导致烯烃氢化形成的烷烃副产物显着减少。
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公开(公告)号：US07528269B2
公开(公告)日：2009-05-05
申请号：US11312036
申请日：2005-12-20
Applicant: Bi Le-Khac , Roger A. Grey
Inventor： Bi Le-Khac , Roger A. Grey
IPC: C07D301/12
CPC classification number: C07D301/12
Abstract: This invention is a process for oxidizing an organic compound with a hydrogen peroxide solution produced by reacting hydrogen and oxygen in the presence of an oxidation catalyst. The hydrogen peroxide is produced by reacting hydrogen and oxygen in a solvent in the presence of a H2O2-producing catalyst comprising a polymer-encapsulated combination of a noble metal and an ion-exchange resin. Polymer encapsulation of the H2O2-producing catalyst improves its productivity in making hydrogen peroxide and is expected to reduce metal loss.
Abstract translation: 本发明是一种通过在氧化催化剂存在下使氢和氧反应生成的过氧化氢溶液来氧化有机化合物的方法。 过氧化氢是通过在溶剂中在含有贵金属和离子交换树脂的聚合物封装的组合的H 2 O 2生成催化剂存在下使氢和氧反应来制备的。 产生H2O2的催化剂的聚合物包封提高了其在制备过氧化氢中的生产率，并预期减少金属损失。
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公开(公告)号：US07432384B2
公开(公告)日：2008-10-07
申请号：US11257955
申请日：2005-10-25
Applicant: Bi Le-Khac , Roger A. Grey
Inventor： Bi Le-Khac , Roger A. Grey
IPC: C07D301/10 , C07D301/12
CPC classification number: C07D301/06
Abstract: A process is disclosed for the epoxidation of an olefin with hydrogen and oxygen in the presence of an oxidation catalyst comprising a transition metal zeolite and a polymer-encapsulated noble metal catalyst. The noble metal catalyst comprises a noble metal and an ion-exchange resin. The process using the polymer-encapsulated noble metal catalyst gives higher epoxide productivity than a process that uses a noble metal catalyst which is not encapsulated by a polymer.
Abstract translation: 公开了一种在含有过渡金属沸石和聚合物包封的贵金属催化剂的氧化催化剂存在下，用氢和氧环氧化烯烃的方法。 贵金属催化剂包含贵金属和离子交换树脂。 使用聚合物包封的贵金属催化剂的方法比使用不被聚合物包封的贵金属催化剂的方法提供更高的环氧化物生产率。
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公开(公告)号：US20080021230A1
公开(公告)日：2008-01-24
申请号：US11489086
申请日：2006-07-18
Applicant: Kun Qin , Roger A. Grey , Peter J. Whitman
Inventor： Kun Qin , Roger A. Grey , Peter J. Whitman
IPC: C07D301/06
CPC classification number: C07D301/08 , C07D301/10
Abstract: A process for producing an epoxide comprising reacting an olefin, hydrogen and oxygen in the presence of a catalyst comprising a titanium or vanadium zeolite, palladium, and lead. The process results in significantly reduced alkane by-product formed by the hydrogenation of olefin.
Abstract translation: 一种制备环氧化物的方法，包括在包含钛或钒沸石，钯和铅的催化剂存在下使烯烃，氢和氧反应。 该方法导致烯烃氢化形成的烷烃副产物显着减少。
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公开(公告)号：US20080015372A1
公开(公告)日：2008-01-17
申请号：US11484906
申请日：2006-07-12
Applicant: Mark P. Kaminsky , Roger A. Grey
Inventor： Mark P. Kaminsky , Roger A. Grey
IPC: C07D301/06
CPC classification number: C07D301/06 , B01J21/063 , B01J21/066 , B01J23/6567 , B01J29/89 , B01J35/0006 , B01J35/1014 , B01J37/0205
Abstract: The invention is a process for epoxidizing an olefin with hydrogen and oxygen in the presence of a catalyst mixture containing a titanium or vanadium zeolite and a supported catalyst comprising palladium, rhenium and a carrier. The process results in significantly reduced alkane byproduct formed by the hydrogenation of olefin.
Abstract translation: 本发明是在含有钛或钒沸石的催化剂混合物和包含钯，铼和载体的负载催化剂存在下，用氢和氧环氧化烯烃的方法。 该方法可显着减少由烯烃氢化形成的烷烃副产物。
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