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    Alkyl esters of 1-alkanoyl cycloalkanols and organoleptic uses thereof
    1.
    发明授权
    Alkyl esters of 1-alkanoyl cycloalkanols and organoleptic uses thereof 失效
    1-烷酰基环烷醇的烷基酯及其感官用途

    公开(公告)号：US4374055A

    公开(公告)日：1983-02-15

    申请号：US314002

    申请日：1981-10-22

    申请人： Ronald P. Schreck ,  Kenneth K. Light ,  John B. Hall ,  Frederick L. Schmitt ,  Manfred H. Vock ,  William L. Schreiber ,  Joaquin F. Vinals ,  Jacob Kiwala

    发明人： Ronald P. Schreck ,  Kenneth K. Light ,  John B. Hall ,  Frederick L. Schmitt ,  Manfred H. Vock ,  William L. Schreiber ,  Joaquin F. Vinals ,  Jacob Kiwala

    IPC分类号： A24B15/34 ,  C11B9/00 ,  C11D3/50 ,  A61K7/46

    CPC分类号： A24B15/34 ,  C11B9/0026 ,  C11D3/50

    摘要： Described is a process for preparing several substituted or unsubstituted cycloalkyl acyl alkanoates defined according to the generic structure: ##STR1## wherein R.sub.1 and R.sub.2 taken together complete a cycloalkyl moiety or methyl, dimethyl or trimethyl substituted cycloalkyl moiety containing five or six carbon atoms in the ring and wherein R.sub.3 is C.sub.1 -C.sub.3 lower alkyl and R.sub.4 is methyl or hydrogen by reacting a compound having the generic structure: ##STR2## in an aqueous silver-ion containing solution having a weakly acidic pH at elevated temperatures. The compounds so produced are useful for their organoleptic properties in consumable materials, such as foodstuffs, foodstuff flavorants, chewing gums, chewing gum flavorants, toothpastes, toothpaste flavorants, medicinal products, medicinal product flavorants, chewing tobaccos, chewing tobacco flavorants, smoking tobaccos, smoking tobacco flavorants, perfume compositions, perfumed articles, such as cationic, anionic, nonionic and zwitterionic detergents, fabric softener compositions, drier-added fabric softener articles, textile sizing agents and optical brighteners for textiles as well as colognes.

    摘要翻译： 描述了根据通用结构定义的若干取代或未取代的环烷基酰基链烷酸酯的方法：其中R 1和R 2一起完成环烷基部分或含有5或6个碳原子的甲基，二甲基或三甲基取代的环烷基部分 环，其中R 3是C 1 -C 3低级烷基，R 4是甲基或氢，通过使具有通式结构的化合物：在高温下具有弱酸性pH的含水银离子溶液中。 如此生产的化合物可用于消费材料如食品，食品香料，口香糖，口香糖调味剂，牙膏，牙膏调味剂，药用产品，药用香料，咀嚼烟草，咀嚼烟草香料，烟草烟草， 吸烟烟草调味剂，香料组合物，香料制品，例如阳离子，阴离子，非离子和两性离子洗涤剂，织物柔软剂组合物，干燥剂添加的织物柔软剂制品，纺织品上浆剂和用于纺织品的荧光增白剂以及古龙水。

    Process for enhancing the organoleptic properties of perfumed articles using alkyl esters of 1-alkanolyl cycloalkanols
    4.
    发明授权
    Process for enhancing the organoleptic properties of perfumed articles using alkyl esters of 1-alkanolyl cycloalkanols 失效
    使用1-链烷酰基环烷醇的烷基酯增强香料制品的感官特性的方法

    公开(公告)号：US4359395A

    公开(公告)日：1982-11-16

    申请号：US314003

    申请日：1981-10-22

    申请人： Ronald P. Schreck ,  Kenneth K. Light ,  John B. Hall ,  Frederick L. Schmitt ,  Manfred H. Vock ,  William L. Schreiber ,  Joaquin F. Vinals ,  Jacob Kiwala

    发明人： Ronald P. Schreck ,  Kenneth K. Light ,  John B. Hall ,  Frederick L. Schmitt ,  Manfred H. Vock ,  William L. Schreiber ,  Joaquin F. Vinals ,  Jacob Kiwala

    IPC分类号： A24B15/34 ,  C11D3/50 ,  D06M13/00

    CPC分类号： D06M13/005 ,  A24B15/34 ,  C11D3/50

    摘要： Described is a process for preparing several substituted or unsubstituted cycloalkyl acyl alkanolates defined according to the generic structure: ##STR1## wherein R.sub.1 and R.sub.2 taken together complete a cycloalkyl moiety or methyl, dimethyl or trimethyl substituted cycloalkyl moiety containing five or six carbon atoms in the ring and wherein R.sub.3 is C.sub.1 -C.sub.3 lower alkyl and R.sub.4 is methyl or hydrogen by reacting a compound having the generic structure: ##STR2## in an aqueous silver-ion containing solution having a weakly acidic pH at elevated temperatures. The compounds so produced are useful for their organoleptic properties in consumable materials, such as foodstuffs, foodstuff flavorants, chewing gums, chewing gum flavorants, toothpastes, toothpaste flavorants, medicinal products, medicinal product flavorants, chewing tobaccos, chewing tobacco flavorants, smoking tobaccos, smoking tobacco flavorants, perfume compositions, perfumed articles, such as cationic, anionic, nonionic and zwitterionic detergents, fabric softener compositions, drier-added fabric softener articles, textile sizing agents and optical brighteners for textiles as well as colognes.

    摘要翻译： 描述了根据以下通用结构定义的几种取代或未取代的环烷基酰基链烷醇酯的方法：其中R1和R2一起完成环烷基部分或含有5或6个碳原子的甲基，二甲基或三甲基取代的环烷基部分 环，其中R 3是C 1 -C 3低级烷基，R 4是甲基或氢，通过使具有通式结构的化合物：在高温下具有弱酸性pH的含水银离子溶液中。 如此生产的化合物可用于消费材料如食品，食品香料，口香糖，口香糖调味剂，牙膏，牙膏调味剂，药用产品，药用香料，咀嚼烟草，咀嚼烟草香料，烟草烟草， 吸烟烟草调味剂，香料组合物，香料制品，例如阳离子，阴离子，非离子和两性离子洗涤剂，织物柔软剂组合物，干燥剂添加的织物柔软剂制品，纺织品上浆剂和用于纺织品的荧光增白剂以及古龙水。

    Process for producing solanone, norsolanadione and intermediates therefor
    7.
    发明授权
    Process for producing solanone, norsolanadione and intermediates therefor 失效
    制备索罗酮，二酰甘油和其中间体的方法

    公开(公告)号：US4412083A

    公开(公告)日：1983-10-25

    申请号：US357158

    申请日：1982-03-11

    申请人： Kenneth K. Light ,  William L. Schreiber ,  Joseph A. McGhie ,  Ronald P. Schreck ,  Takao Yoshida ,  Loren B. Schreiber ,  Ranya Muralidhara

    发明人： Kenneth K. Light ,  William L. Schreiber ,  Joseph A. McGhie ,  Ronald P. Schreck ,  Takao Yoshida ,  Loren B. Schreiber ,  Ranya Muralidhara

    IPC分类号： A23L27/20 ,  A24B15/32 ,  C07C45/42 ,  C07C45/51 ,  C07C45/59 ,  C07C45/66 ,  C07D295/02 ,  C07D295/03 ,  C07D295/145 ,  C07D295/155 ,  C07D309/28 ,  C07D317/30 ,  C07C119/12

    CPC分类号： C07D295/03 ,  A23L27/2024 ,  A24B15/32 ,  C07C255/00 ,  C07C45/42 ,  C07C45/516 ,  C07C45/59 ,  C07C45/66 ,  C07D295/145 ,  C07D295/155 ,  C07D309/28 ,  C07D317/30

    摘要： Described is a process for preparing solanone and norsolanadione using chemical intermediates defined according to the generic structure: ##STR1## wherein X is one of the moieties: ##STR2## wherein R represents hydrogen or methyl; wherein Y represents one of the structures: ##STR3## wherein one of the dashed lines represents a carbon-carbon single bond and the other of the dashed lines represents a carbon-carbon double bond; with the provisos that:(i) when Y is the moiety having the structure: ##STR4## then X is the moiety having the structure: ##STR5## (ii) when X is the moiety having the structure: ##STR6## then Y is the moiety having the structure:--C.tbd.N]In preparing solanone, the compound having the structure: ##STR7## or a mixture of compounds defined according to the structure: ##STR8## is reacted with methyl lithium and the resulting intermediate is hydrolyzed and the resulting compound is dehydrated. In producing the norsolanadione, the compound having the structure: ##STR9## or a mixture of compounds according to the structure: ##STR10## is reacted with ethylene glycol or propylene glycol thereby forming a ketal and the resulting ketal is reacted with methyl lithium and the resulting intermediate is then hydrolyzed in the presence of acid.

    摘要翻译： 描述了使用根据以下通用结构定义的化学中间体制备索罗酮和尼考兰那酮的方法：其中X是部分之一：其中R表示氢或甲基; 其中Y表示以下结构之一：其中一条虚线表示碳 - 碳单键，另一条虚线表示碳 - 碳双键; 条件是：（i）当Y是具有以下结构的部分时：X是具有以下结构的部分：（ⅱ）当X是具有以下结构的部分时，则Y是 具有以下结构的部分：-C 3 N N]在制备solone的过程中，将具有以下结构的化合物：IMAGE或根据结构定义的化合物的混合物与甲基锂反应，并将所得中间体水解， 所得化合物脱水。 在制备硝酰甘油的过程中，将具有以下结构的化合物：IMAGE或根据以下结构的化合物的混合物与乙二醇或丙二醇反应，从而形成缩酮，得到的缩酮与甲基锂反应， 得到的中间体然后在酸的存在下水解。

    Vaginal moisture balanced tampon and process
    8.
    发明授权
    Vaginal moisture balanced tampon and process 失效
    阴道水分平衡卫生棉条和过程

    公开(公告)号：US06353147B1

    公开(公告)日：2002-03-05

    申请号：US08789747

    申请日：1997-01-27

    申请人： Theodore A. Foley ,  Linda M. Pierson ,  Harry L. Pine ,  Ronald P. Schreck ,  Richard A. Schroeder

    发明人： Theodore A. Foley ,  Linda M. Pierson ,  Harry L. Pine ,  Ronald P. Schreck ,  Richard A. Schroeder

    IPC分类号： A61F1315

    CPC分类号： A61F13/2051 ,  Y10S604/904

    摘要： Vaginal epithelium drying is substantially reduced or prevented by reducing the capillary suction pressure of a tampon in early use. This is accomplished by modifying the capillary suction pressure of the surface of the tampon by using hydrophobic components in the tampon, such as hydrophobic fibers and/or hydrophobic cover material. Other means of obtaining a lower capillary suction pressure include increasing the denier of the fibers in the tampon's absorbent core and/or decreasing the density of the tampon.

    摘要翻译： 阴道上皮干燥通过减少早期使用中棉塞的毛细吸入压力而大大降低或防止。 这通过使用棉塞中的疏水性成分（例如疏水性纤维和/或疏水性覆盖材料）来改变卫生棉条表面的毛细吸入压力来实现。 获得较低毛细管吸入压力的其它方法包括增加卫生棉条的吸收芯中纤维的旦数和/或降低棉条的密度。

    Vaginal moisure balance tampon and process
    9.
    发明授权
    Vaginal moisure balance tampon and process 失效
    阴道moisure平衡棉塞和过程

    公开(公告)号：US5817077A

    公开(公告)日：1998-10-06

    申请号：US814688

    申请日：1997-03-11

    申请人： Theodore A. Foley ,  Linda M. Pierson ,  Harry L. Pine ,  Ronald P. Schreck

    发明人： Theodore A. Foley ,  Linda M. Pierson ,  Harry L. Pine ,  Ronald P. Schreck

    IPC分类号： A61F13/20 ,  A61F13/15

    CPC分类号： A61F13/2051 ,  Y10S604/904

    摘要： Vaginal epithelium drying is substantially reduced or prevented by reducing the capillary suction pressure of a tampon in early use. This is accomplished by modifying the capillary suction pressure of the surface of the tampon by using hydrophobic components in the tampon, such as hydrophobic fibers and/or hydrophobic cover material. Other means of obtaining a lower capillary suction pressure include increasing the denier of the fibers in the tampon's absorbent core and/or decreasing the density of the tampon.

    摘要翻译： 阴道上皮干燥通过减少早期使用中棉塞的毛细吸入压力而大大降低或防止。 这通过使用棉塞中的疏水性成分（例如疏水性纤维和/或疏水性覆盖材料）来改变卫生棉条表面的毛细吸入压力来实现。 获得较低毛细管吸入压力的其它方法包括增加卫生棉条的吸收芯中纤维的旦数和/或降低棉条的密度。