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    Carbonate polymer resins containing low volatility aromatic phosphate ester compounds
    1.
    发明授权
    Carbonate polymer resins containing low volatility aromatic phosphate ester compounds 失效
    含低挥发性芳族磷酸酯化合物的碳酸酯聚合物树脂

    公开(公告)号：US5663280A

    公开(公告)日：1997-09-02

    申请号：US636291

    申请日：1996-04-23

    申请人： Samuel A. Ogoe ,  Nancy J. Schrock ,  Jimmie D. Spoon

    发明人： Samuel A. Ogoe ,  Nancy J. Schrock ,  Jimmie D. Spoon

    IPC分类号： C08K5/43 ,  C08K5/521 ,  C08K5/523 ,  C08L27/18 ,  C08L69/00 ,  C08G64/00

    CPC分类号： C08K5/43 ,  C08K5/523

    摘要： Disclosed is a carbonate polymer composition comprising (a) a carbonate polymer having a weight average molecular weight of from about 20,000 to about 40,000 and (b) from greater than about 0.1 to less than about 1.0 weight percent (based on carbonate polymer composition weight) low volatility aromatic phosphate ester compound, and optionally (c) from about 0.001 to about 0.1 weight percent (based on carbonate polymer compositions weight) of an alkali metal salt having a pH of at least about 7. Preferably the low volatility aromatic phosphate ester is selected from the group of aromatic phosphate ester oligomer compounds or haloaryl phosphate compounds. It has been found to be preferable to use a low volatility aromatic phosphate ester which experiences a weight loss of no more than 5 weight percent at 250.degree. C. when heated to a temperature of 500.degree. C. in a thermogravimetric analysis (TGA) at a heating rate of 20.degree. C. per minute, more preferably no more than 40 percent at 300.degree. C. It has been found that these compositions surprisingly achieve the Underwriters Laboratory (UL-94) V-2 rating without significantly sacrificing the otherwise good combinations of properties of carbonate polymer resins.

    摘要翻译： 公开了一种碳酸酯聚合物组合物，其包含（a）重均分子量为约20,000至约40,000的碳酸酯聚合物和（b）大于约0.1至小于约1.0重量％（基于碳酸酯聚合物组合物重量） 低挥发性芳族磷酸酯化合物，以及任选地（c）约0.001至约0.1重量％（基于碳酸酯聚合物组合物重量）的pH为至少约7的碱金属盐。优选地，低挥发性芳族磷酸酯是 选自芳族磷酸酯低聚物化合物或卤代芳基磷酸酯化合物。 已经发现，优选使用低挥发性芳族磷酸酯，当在热重分析（TGA）中加热到500℃时，在250℃下经历重量损失不超过5重量％ 加热速度为每分钟20℃，更优选在300℃下更优选不超过40％。已经发现，这些组合物令人惊讶地实现了保险商实验室（UL-94）V-2等级，而没有显着牺牲其他良好 碳酸酯聚合物树脂的性能组合。

    Dispersing ignition resistant additives into carbonate polymers
    4.
    发明授权
    Dispersing ignition resistant additives into carbonate polymers 失效
    将耐燃添加剂分散在碳酸酯聚合物中

    公开(公告)号：US5041479A

    公开(公告)日：1991-08-20

    申请号：US398036

    申请日：1989-08-24

    申请人： Samuel A. Ogoe

    发明人： Samuel A. Ogoe

    IPC分类号： C08J3/22 ,  C08K3/30 ,  C08K5/00 ,  C08K5/03 ,  C08K5/136 ,  C08K5/36 ,  C08K5/43 ,  C08L69/00

    CPC分类号： C08J3/226 ,  C08K3/30 ,  C08K5/136 ,  C08K5/43 ,  C08J2369/00 ,  C08J2469/00

    摘要： A process for dispersing one or more powdered ignition resistant or flame retardant additives into carbonate polymers which comprises the steps of preparing a base concentrate having about 5 to about 50 weight per cent of said additives by blending said additives with a carbonate polymer having a melt flow rate from about 3 to about 20, pelletizing said base concentrate having said ignition resistant additive dispersed therein, dry blending said concentrate pellets with carbonate pellets having a melt flow rate from about 1 to about 80 whereby said polymer/concentrate blend has an amount of said additive dispersed therein effective to render said blend ignition resistant, and pelletizing or molding said carbonate polymer/concentrate blend. The use of this method gives ignition resistant carbonate polymers with improved impact properties as measured by Izod impact tests.

    Ultra violet light resistant carbonate polymers with improved processing stability
    9.
    发明授权
    Ultra violet light resistant carbonate polymers with improved processing stability 失效
    具有改善加工稳定性的紫外线耐光碳酸酯聚合物

    公开(公告)号：US4782103A

    公开(公告)日：1988-11-01

    申请号：US86994

    申请日：1987-08-19

    申请人： Samuel A. Ogoe

    发明人： Samuel A. Ogoe

    IPC分类号： C08L69/00 ,  C08K5/00 ,  C08K5/3475 ,  C08K5/36 ,  C08K5/42 ,  C08K5/43 ,  C08K5/47 ,  C08K5/44

    CPC分类号： C08K5/3475 ,  C08K5/43

    摘要： Ultra violet light resistant polycarbonates are produced having processing or heat stability by adding compatible UV absorbing compounds and aromatic sulfonimides. The UV absorbing compounds are used in amounts from about 0.01 to about 5.0% by weight and the sulfonimides are used in an amount from about 0.0001 to about 10.0%. The preferred UV absorber is 2-(2'-hydroxy-5'-t-octylphenyl)-benzotriazole. The preferred sulfonimide is N-(p-tolylsulfonyl)-p-toluenesulfonimide.

    摘要翻译： 通过添加兼容的UV吸收化合物和芳香族磺酰亚胺，生产具有加工或热稳定性的耐紫外线聚碳酸酯。 UV吸收化合物的用量为约0.01至约5.0重量％，磺酰亚胺的用量为约0.0001至约10.0重量％。 优选的UV吸收剂是2-（2'-羟基-5'-叔辛基苯基） - 苯并三唑。 优选的磺酰亚胺是N-（对甲苯磺酰基）对甲苯磺酰亚胺。

    Fire retardant carbonate polymer composition
    10.
    发明授权
    Fire retardant carbonate polymer composition 失效
    阻燃碳酸酯聚合物组合物

    公开(公告)号：US4626563A

    公开(公告)日：1986-12-02

    申请号：US726853

    申请日：1985-04-24

    申请人： Samuel A. Ogoe ,  Kevin F. Dick

    发明人： Samuel A. Ogoe ,  Kevin F. Dick

    IPC分类号： C08K3/30 ,  C08K5/43 ,  C08L69/00

    CPC分类号： C08K3/30 ,  C08K5/43 ,  C08L69/00

    摘要： Flame retardant carbonate polymers containing an aromatic sulfimide, a monomeric or polymeric halogenated organic compound, a metal sulfate having a pka from 1 to 5 and a fibril forming polytetrafluoroethylene as additives in effective amounts give carbonate polymers that are not only flame retardant but are melt stable i.e. show little loss in molecular weight during processing or melt shearing.

    摘要翻译： 含有芳族硫酰亚胺，单体或聚合卤化有机化合物的阻燃碳酸酯聚合物，具有1〜5的pka的金属硫酸盐和作为有效量的添加剂的原纤维形成聚四氟乙烯的碳酸酯聚合物不仅具有阻燃性，而且熔融稳定 即在加工或熔融剪切过程中分子量的损失很小。