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公开(公告)号：US08173806B2
公开(公告)日：2012-05-08
申请号：US12282381
申请日：2007-03-14
申请人： Kazuo Tanaka , Yoshifumi Sato , Takafumi Yoshimura
发明人： Kazuo Tanaka , Yoshifumi Sato , Takafumi Yoshimura
IPC分类号： C07D239/72
CPC分类号： C07D239/88
摘要： In reacting an anthranilic acid derivative represented by the general formula (1), especially the anthranilic acid derivative selected from anthranilic acid, anthranilamide and anthranilate, with formamide, the reaction is attained under the condition of coexistence of acetic acid and a base as a catalyst in the reaction liquid, and it has made it possible to produce a quinazolin-4-one derivative represented by the general formula (2) and useful as a material for medicine intermediates, at high yield with no side production.
摘要翻译： 在使通式（1）表示的邻氨基苯甲酸衍生物，特别是选自邻氨基苯甲酸，邻氨基苯甲酰胺和邻氨基苯甲酸酯的邻氨基苯甲酸衍生物与甲酰胺反应时，在乙酸和碱作为催化剂共存的条件下反应 在反应液中，可以以高产率生产无副产物的由通式（2）表示的喹唑啉-4-酮衍生物作为医药中间体的材料。
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2.发明授权Process for production of iodine compounds and process for production of high-purity 5-iodo-2-methylbenzoic acid 失效生产碘化合物的方法和生产高纯度5-碘-2-甲基苯甲酸的方法公开(公告)号：US07750182B2
公开(公告)日：2010-07-06
申请号：US10545005
申请日：2004-02-10
CPC分类号： C07C253/30 , C07B39/00 , C07C17/12 , C07C17/156 , C07C17/158 , C07C51/363 , C07C51/43 , C07C25/02 , C07C25/13 , C07C25/18 , C07C25/125 , C07C63/70 , C07C255/50
摘要： Provided is a production method for an iodine compound in which iodine is reacted with a substrate in the presence of a porous material having a pore diameter of 500 nm or less or in the presence of the above porous material and an oxidizing agent and a production process for high purity 5-iodo-2-methylbenzoic acid comprising an iodination reaction step carried out by the above-mentioned, a crystal precipitation and separation step in which a product is precipitated by adding water or cooling and then separated and a purification step in which crystal separated is recrystallized using an organic solvent. According to the production method for an iodine compound described above, iodine can be introduced into various substrates at a high selectivity. Since expensive metals and specific reagents do not have to be used, it can readily be carried out in an industrially scale, and the product having a high purity can be obtained. Further, the process comprising the iodination reaction, separation and purification steps described above makes it possible to readily obtain at a high yield, 5-iodo-2-methylbenzoic acid having a high purity which is useful in uses for functional chemical products such as medicines. The process of the present invention comprising iodination reaction, separation and purification steps is characterized by that it is simple in terms of a procedure and that the purification load is smaller, and it is very advantageous in industrially carrying out.
摘要翻译： 提供一种碘化合物的制造方法，其中碘在孔径为500nm以下的多孔质材料的存在下，或者在上述多孔质材料和氧化剂的存在下，与基材反应，制造方法 包括通过上述进行的碘化反应步骤的高纯度5-碘-2-甲基苯甲酸，其中通过加入水或冷却然后分离产物而沉淀产物的晶体沉淀和分离步骤和纯化步骤，其中 使用有机溶剂重结晶晶体分离。 根据上述碘化合物的制造方法，能够以高选择性将碘引入各种基材中。 由于不需要使用昂贵的金属和特定试剂，因此可以容易地以工业规模进行，可以获得高纯度的产物。 此外，包括上述碘化反应，分离和纯化步骤的方法使得可以容易地以高产率获得具有高纯度的5-碘-2-甲基苯甲酸，其可用于诸如药物的功能性化学产品的用途 。 包括碘化反应，分离和纯化步骤的本发明方法的特征在于它在程序方面简单，净化负荷较小，在工业上非常有利。
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公开(公告)号：US20090160624A1
公开(公告)日：2009-06-25
申请号：US12359458
申请日：2009-01-26
IPC分类号： H04Q5/22
CPC分类号： G06Q10/00
摘要： An individual article management arrangements for managing an individual article distributed through a plurality of sites with a form thereof changed at least one of said plurality of sites, including: information processing apparatuses installed at said plurality of sites; and a data center apparatus connected to each of said information processing apparatuses through a network. The data center apparatus and the information processing apparatuses are configured to effect predetermined operations.
摘要翻译： 用于管理通过多个站点分发的单个文章的单独文章管理装置改变了所述多个站点中的至少一个，包括：安装在所述多个站点处的信息处理设备; 以及通过网络连接到每个所述信息处理设备的数据中心设备。 数据中心装置和信息处理装置被配置为实现预定的操作。
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公开(公告)号：US20080231427A1
公开(公告)日：2008-09-25
申请号：US12123171
申请日：2008-05-19
IPC分类号： H04Q5/22
CPC分类号： G06Q10/00
摘要： An individual article management system for managing an individual article distributed through a plurality of sites with a form thereof changed at least one of the plurality of sites. Each of the information processing apparatuses transmits read identification information and formed index data to a data center apparatus through a network, and the data center apparatus, receives the transmitted identification information and the transmitted index data, and stores each of the received index data into a storing apparatus so as to be associated with each other on the basis of the identification information for identifying the individual article.
摘要翻译： 用于管理通过具有其形式的多个站点分发的单个物品的单独的物品管理系统改变了多个站点中的至少一个站点。 每个信息处理设备通过网络将读取的标识信息和形成的索引数据发送到数据中心设备，并且数据中心设备接收所发送的标识信息和发送的索引数据，并将接收的每个索引数据存储到 存储装置，以便基于用于识别单个物品的识别信息彼此相关联。
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公开(公告)号：US07294594B2
公开(公告)日：2007-11-13
申请号：US10781326
申请日：2004-02-17
申请人： Toru Kawamoto , Yoshifumi Sato , Toshifumi Matsuda
发明人： Toru Kawamoto , Yoshifumi Sato , Toshifumi Matsuda
摘要： A glass composition of the present invention relates to a multicomponent oxide glass composition manufactured by melting glass raw materials, which contains: 10 ppm or more of at least one type of a polyvalent element; minimum valence cations of the polyvalent element in a ratio of the minimum valence cation content to the total polyvalent element content of 5 to 98% in mass ratio; and 0.01 to 2 μl/g (0° C., 1 atm) of helium.
摘要翻译： 本发明的玻璃组合物涉及通过熔化玻璃原料制造的多组分氧化物玻璃组合物，其包含：10ppm以上的至少一种多价元素; 最低价阳离子含量与总多价元素含量的比例为5〜98％质量比的多价元素的最低价阳离子; 和0.01至2mul / g（0℃，1atm）的氦。
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6.发明申请Process for production of iodine compounds and process for production of high-purity 5-iodo-2-methylbenzoic acid 失效生产碘化合物的方法和生产高纯度5-碘-2-甲基苯甲酸的方法公开(公告)号：US20060161028A1
公开(公告)日：2006-07-20
申请号：US10545005
申请日：2004-02-10
IPC分类号： C07C17/00
CPC分类号： C07C253/30 , C07B39/00 , C07C17/12 , C07C17/156 , C07C17/158 , C07C51/363 , C07C51/43 , C07C25/02 , C07C25/13 , C07C25/18 , C07C25/125 , C07C63/70 , C07C255/50
摘要： Provided is a production method for an iodine compound in which iodine is reacted with a substrate in the presence of a porous material having a pore diameter of 500 nm or less or in the presence of the above porous material and an oxidizing agent and a production process for high purity 5-iodo-2-methylbenzoic acid comprising an iodination reaction step carried out by the above-mentioned, a crystal precipitation and separation step in which a product is precipitated by adding water or cooling and then separated and a purification step in which crystal separated is recrystallized using an organic solvent. According to the production method for an iodine compound described above, iodine can be introduced into various substrates at a high selectivity. Since expensive metals and specific reagents do not have to be used, it can readily be carried out in an industrially scale, and the product having a high purity can be obtained. Further, the process comprising the iodination reaction, separation and purification steps described above makes it possible to readily obtain at a high yield, 5-iodo-2-methylbenzoic acid having a high purity which is useful in uses for functional chemical products such as medicines. The process of the present invention comprising iodination reaction, separation and purification steps is characterized by that it is simple in terms of a procedure and that the purification load is smaller, and it is very advantageous in industrially carrying out.
摘要翻译： 提供一种碘化合物的制造方法，其中碘在孔径为500nm以下的多孔质材料的存在下，或者在上述多孔质材料和氧化剂的存在下，与基材反应，制造方法 包括通过上述进行的碘化反应步骤的高纯度5-碘-2-甲基苯甲酸，其中通过加入水或冷却然后分离产物而沉淀产物的晶体沉淀和分离步骤和纯化步骤，其中 使用有机溶剂重结晶晶体分离。 根据上述碘化合物的制造方法，能够以高选择性将碘引入各种基材中。 由于不需要使用昂贵的金属和特定试剂，因此可以容易地以工业规模进行，可以获得高纯度的产物。 此外，包括上述碘化反应，分离和纯化步骤的方法使得可以容易地以高产率获得具有高纯度的5-碘-2-甲基苯甲酸，其可用于诸如药物的功能性化学产品的用途 。 包括碘化反应，分离和纯化步骤的本发明方法的特征在于它在程序方面简单，净化负荷较小，在工业上非常有利。
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公开(公告)号：US5793826A
公开(公告)日：1998-08-11
申请号：US722765
申请日：1996-09-27
申请人： Yoshifumi Sato , Nobuyuki Tanaka , Yukio Watanabe
发明人： Yoshifumi Sato , Nobuyuki Tanaka , Yukio Watanabe
CPC分类号： H02K49/106 , G21C7/12 , G21Y2002/10 , G21Y2002/302 , G21Y2002/303 , G21Y2002/40 , G21Y2004/30 , G21Y2004/301 , H02K11/00 , H02K7/08 , Y02E30/39
摘要： A control rod mechanism for transmitting the rotation of an electric motor via a drive shaft to an elevator apparatus for raising and lowering a hollow piston on an upper end thereof, which is provided a control rod that controls the output of a nuclear reactor. The control rod mechanism is used to insert the control rod into a reactor core or remove it therefrom, and also to rapidly insert the control rod into the reactor core by the injection of hot water to force the hollow piston upward. The control rod mechanism includes a magnetic coupling having an inner magnet, which is divided into a plurality of parts and is disposed at a lower portion of the drive shaft in order to transmit the rotational power of the electric motor to the drive shaft. The control rod mechanism also includes a drive-side outer magnet, which is divided into a plurality of parts and is provided on a rotary shaft of the electric motor in an arrangement on an outer side of the inner magnet. The control rod mechanism further includes a circular cylindrical outer yoke on an inner surface of which the outer magnet is mounted on. The radial-direction position of an outer magnet installation surface on the outer yoke is the same as or further inward with respect to the radial-direction position of an inner surface of the outer yoke that is above the outer magnet installation surface.
摘要翻译： 一种控制杆机构，用于通过驱动轴将电动机的旋转传递到用于升高和降低其上端的中空活塞的电梯装置，该控制棒设置有控制核反应堆的输出的控制棒。 控制杆机构用于将控制棒插入反应堆芯或从其中移除，并通过注入热水将控制杆快速插入反应堆芯，以迫使中空活塞向上。 控制杆机构包括具有内部磁体的磁耦合器，该内部磁体被分成多个部分并且设置在驱动轴的下部，以将电动机的旋转动力传递到驱动轴。 控制杆机构还包括驱动侧外部磁体，该驱动侧外部磁体被分成多个部分，并且设置在电动机的旋转轴上，该内部磁体在外部的外侧。 控制杆机构还包括在外表面上安装外磁体的圆柱形外磁轭。 外磁轭的外磁铁安装面的径向位置相对于位于外磁铁安装面以上的外磁轭的内表面的径向位置相同或更靠内侧。
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8.发明授权Process for the production of polyol ester and ester-containing lubricating oil 失效用于生产多元醇酯和含酯润滑油的方法
公开(公告)号：US5705459A
公开(公告)日：1998-01-06
申请号：US578994
申请日：1995-12-27
IPC分类号： C10M105/38 , C10M171/00 , C10M105/32
CPC分类号： C10M105/38 , C10M171/008 , C10M2207/281 , C10M2207/282 , C10M2207/283 , C10M2207/286 , C10M2211/022 , C10M2211/06 , C10N2240/00 , C10N2240/22 , C10N2240/30 , C10N2240/50 , C10N2240/52 , C10N2240/54 , C10N2240/56 , C10N2240/58 , C10N2240/60 , C10N2240/66
摘要： A process for the production of a high-performance hybrid polyol ester having excellent compatibility with hydrofluorocarbons which are regarded as the most likely refrigerant and having excellent resistance to hydrolysis which esters are liable to undergo, the polyol ester having a plurality of branched fatty acid residues at least one of which has a different number of carbon atoms from that of the other branched fatty acid residue or those of the other branched fatty acid residues, the process comprising reacting at least two kinds of olefins having different numbers of carbon atoms, carbon monoxide and a polyhydric alcohol in the presence of hydrogen fluoride.
摘要翻译： 一种与被认为是最可能的制冷剂并且具有优异的耐水解性的氢氟烃的相容性优异的高性能混合多元醇酯的制备方法，所述多元醇酯具有多个支链脂肪酸残基 其中至少一个与其它支链脂肪酸残基或其它支链脂肪酸残基的碳原子数不同，所述方法包括使至少两种具有不同碳原子数的烯烃，一氧化碳 和多元醇在氟化氢存在下反应。
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9.发明授权Process for recovering catalyst for use in preparing .alpha.-(4-isobutylphenyl)propionic acid 失效用于回收用于制备α-（4-异丁基苯基）丙酸的催化剂的方法
公开(公告)号：US4988652A
公开(公告)日：1991-01-29
申请号：US456313
申请日：1989-12-26
申请人： Yoshikazu Shima , Kazuo Tanaka , Yoshifumi Sato
发明人： Yoshikazu Shima , Kazuo Tanaka , Yoshifumi Sato
CPC分类号： B01J31/0231 , B01J31/0267 , B01J31/20 , B01J31/403 , B01J31/4053 , C07C51/48 , B01J2231/34 , B01J2531/847 , B01J31/30 , Y02P20/584
摘要： An efficient process for recovering a catalyst used in the preparation of .alpha.-(4-isobutylphenyl)propionic acid, which comprises recovering part of a nickel catalyst component, such as nickel carbonyl, from a purge gas, concentrating a reaction product mixture, adding an organic solvent thereto to extract the reaction product, then separating and recovering the majority of the catalyst components from the extraction residue.
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公开(公告)号：US07231388B2
公开(公告)日：2007-06-12
申请号：US10206595
申请日：2002-07-29
IPC分类号： G06F10/30
CPC分类号： G06F17/3069 , Y10S707/99933 , Y10S707/99934 , Y10S707/99935
摘要： Similar document retrieving method and system for retrieving similar documents from a document database storing plural documents written in different languages with high accuracy while suppressing retrieval noise even when difference is found in the number of registered documents in dependence on the species of description languages. Statistical information concerning the registration-subjected documents is collected on a language-by-language basis upon registration thereof. Upon retrieval of documents similar to a query document, weights of words extracted from the query document are taken into account and on a language-by-language basis by referencing the statistical information.
摘要翻译： 相似的文件检索方法和系统，用于从存储多种写入不同语言的多种文件的文件数据库中检索类似的文档，同时抑制检索噪声，即使在依赖于描述语言的种类的登记文件的数量上存在差异的情况下。 有关登记受影响的文件的统计资料，在登记后将逐一收集。 在检索与查询文档类似的文档时，通过参考统计信息考虑从查询文档中提取的单词的权重，并且逐个语言地考虑。
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