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公开(公告)号：US20160002426A1
公开(公告)日：2016-01-07
申请号：US14851081
申请日：2015-09-11
IPC分类号： C08J9/00
CPC分类号： C08J9/0028 , C08G18/0838 , C08G18/16 , C08G18/185 , C08G18/4072 , C08G18/6552 , C08G2101/00 , C08G2101/0008 , C08J9/0033 , C08J9/0042 , C08J2205/05 , C08J2375/04 , C08J2375/08
摘要： A composition and process useful to make flexible polyurethane foams and in particular flexible molded polyurethane foams is disclosed. The usage of dipolar aprotic liquids such as DMSO, DMI, sulfolane, N-methyl-acetoacetamide, N,N-dimethylacetoacetamide as well as glycols containing hydroxyl numbers OH#≦1100 as cell opening aides for 2-cyanoacetamide or other similar molecules containing active methylene or methine groups to make a polyurethane foam is also disclosed. The advantage of using cell opener aids results in a) no foam shrinkage; b) lower use levels of cell opener; c) foam performance reproducibility d) optimum physical properties. In addition, combining the acid blocked amine catalyst together with the cell opener and the cell opener aid results in a less corrosive mixture as well as provides a method that does not require mechanical crushing for cell opening.
摘要翻译： 公开了用于制备柔性聚氨酯泡沫，特别是柔性模塑聚氨酯泡沫的组合物和方法。 使用偶极非质子液体如DMSO，DMI，环丁砜，N-甲基 - 乙酰乙酰胺，N，N-二甲基乙酰乙酰胺以及含有羟基数OH＃＆amp; 1100的二醇作为2-氰基乙酰胺或其它类似分子的开放助剂 还公开了制备聚氨酯泡沫的活性亚甲基或次甲基。 使用细胞开放助剂的优点导致a）没有泡沫收缩; b）细胞开放剂的使用水平较低; c）泡沫性能重现性d）最佳物理性能。 此外，将酸封闭的胺催化剂与开孔剂和开孔剂组合在一起导致较少的腐蚀性混合物，并且提供了不需要机械破碎以进行开孔的方法。
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2.发明申请AMINE CATALYST FOR IMPROVING THE STABILITY OF POLYURETHANE SYSTEMS HAVING HALOGEN CONTAINING BLOWING AGENTS 审中-公开用于改善含有蒸发剂的含卤素的聚氨酯体系的稳定性的胺催化剂公开(公告)号：US20150266994A1
公开(公告)日：2015-09-24
申请号：US14437070
申请日：2013-10-24
CPC分类号： C08G18/1858 , C08G18/092 , C08G18/1825 , C08G18/1833 , C08G18/2027 , C08G18/225 , C08G18/227 , C08G18/34 , C08G18/4027 , C08G18/5021 , C08G18/546 , C08G2101/0025 , C08G2105/02 , C08J9/02 , C08J9/144 , C08J2201/022 , C08J2203/162 , C08J2205/052 , C08J2205/10 , C08J2207/04 , C08J2375/04
摘要： Catalyst compositions useful in the production of insulating polyurethane or polyisocyanurate foam are disclosed. The catalyst compositions impart increased stability of a mixture of the catalyst, a halogen-containing blowing agent, and a polyol. These catalyst compositions comprise of at least 10% of a tetraalkylguanidine and at least 10% of a tertiary amine catalyst with an isocyanate reactive group. These improved catalysts can be used with any halogenated blowing agent, and provide substantial stability benefits with the use of hydrofluoroolefins and hydrofluorochloroolefins. In an exemplary embodiment, a process includes providing a pre-mix comprising a hydrohaloolefin blowing agent, at least one polyol, water, and a catalyst comprising 10-50% tetra methylguanidine and 10-90% of one or more of an amine catalyst containing an isocyanate reactive group.
摘要翻译： 公开了可用于生产绝缘聚氨酯或聚异氰脲酸酯泡沫的催化剂组合物。 催化剂组合物赋予催化剂，含卤素发泡剂和多元醇的混合物更高的稳定性。 这些催化剂组合物包含至少10％的四烷基胍和至少10％的具有异氰酸酯反应性基团的叔胺催化剂。 这些改进的催化剂可以与任何卤代发泡剂一起使用，并且通过使用氢氟烯烃和氢氟氯烯烃提供显着的稳定性优点。 在一个示例性实施方案中，方法包括提供包含氢卤烯烃发泡剂，至少一种多元醇，水和包含10-50％四甲基胍和10-90％一种或多种胺催化剂的催化剂的预混合物，其含有 异氰酸酯反应性基团。
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公开(公告)号：US09273175B2
公开(公告)日：2016-03-01
申请号：US13633423
申请日：2012-10-02
发明人： Juan Jesus Burdeniuc , Jennifer Elizabeth Antoline Al-Rashid , Andrew Wilson Wang , Diana Sue Dunn , You-Moon Jeon , Jane Garrett Kniss , Stephan Hermann Wendel
IPC分类号： C08G18/18 , C07C209/84 , C08G18/20 , C08G18/63 , C08G18/76 , C08G18/12 , C08G18/40 , C08G18/65 , C08G101/00
CPC分类号： C08G18/1833 , C07C209/84 , C08G18/12 , C08G18/14 , C08G18/18 , C08G18/1825 , C08G18/20 , C08G18/2054 , C08G18/4072 , C08G18/4833 , C08G18/632 , C08G18/657 , C08G18/6688 , C08G18/7621 , C08G2101/0008 , C08G2101/005 , C08G2101/0083 , C08J9/14 , C08J2203/06 , C08J2205/06 , C08J2375/04 , C08J2375/08 , C08G18/3275
摘要： A composition and method for producing a tertiary amine is disclosed. The tertiary amine is contacted with an inert gas. The inert gas is nitrogen or more preferably argon. The amine composition is useful in producing polyurethane foam with lower levels of chemical emissions particularly lower emissions of toxic chemicals.
摘要翻译： 公开了一种用于制备叔胺的组合物和方法。 叔胺与惰性气体接触。 惰性气体是氮气，更优选氩气。 胺组合物可用于生产具有较低化学排放水平的聚氨酯泡沫体，特别是较低的有毒化学品排放。
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4.发明申请New Non-Emissive Amine Composition For Improved System Shelf Life Stability 有权用于改善系统保质期稳定性的新型非发射胺组合物公开(公告)号：US20150175735A1
公开(公告)日：2015-06-25
申请号：US14576308
申请日：2014-12-19
CPC分类号： C08G18/1866 , C08G18/14 , C08G18/1825 , C08G18/2825 , C08G18/42 , C08G18/48 , C08G18/7671 , C08G2101/0008 , C08G2101/0025 , C08G2101/0083
摘要： Catalyst compositions useful in the production of low or no amine emission flexible polyurethane foam as well as rigid insulating polyurethane foam produced with systems containing polyether, polyester, Mannich polyols as well as organic-halogen containing flame retardants and blowing agents, are disclosed. The catalysts are characterized by the presence of amine compositions containing unsaturated aliphatic substituent together with secondary hydroxyl groups able to bind to polyurethane polymers and render a low odor and no or low amine emissions finished product.
摘要翻译： 公开了用于生产低或不排放胺的柔性聚氨酯泡沫以及由含有聚醚，聚酯，曼尼希多元醇以及含有机卤素的阻燃剂和发泡剂的体系制备的刚性绝缘聚氨酯泡沫的催化剂组合物。 催化剂的特征在于存在含有不饱和脂肪族取代基的胺组合物以及能够结合聚氨酯聚合物并产生低气味和没有或低的胺排放成品的仲羟基。
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5.发明申请公开(公告)号：US20150148438A1
公开(公告)日：2015-05-28
申请号：US14387986
申请日：2012-03-30
发明人： Juan Jesus Burdeniuc , Boxun Leng , Torsten Panitzsch , Stephan Hermann Wendel , Renee Jo Keller
CPC分类号： C08J9/0019 , C08G18/163 , C08G18/1833 , C08G18/1875 , C08G18/246 , C08G18/2885 , C08G18/4009 , C08G18/4072 , C08G18/7621 , C08G2101/0008 , C08G2101/0016 , C08J9/142 , C08J2375/04
摘要： Disclosed are a process of producing a polyurethane foam product, a polyurethane foam product pre-mix, polyurethane foam product formulation, and a polyurethane foam product. The process of producing the polyurethane foam product includes contacting a halohydrin component with a polyurethane foam product pre-mix. The polyurethane foam product pre-mix includes the halohydrin component. The polyurethane foam product formulation includes a polyol component, an isocyanate component, and a halohydrin component. The polyurethane foam product is formed by the pre-mix having the halohydrin component.
摘要翻译： 公开了生产聚氨酯泡沫产品，聚氨酯泡沫塑料产品预混物，聚氨酯泡沫产品配方和聚氨酯泡沫产品的方法。 生产聚氨酯泡沫产品的方法包括将卤代醇组分与聚氨酯泡沫产品预混物接触。 聚氨酯泡沫产品预混物包括卤代醇组分。 聚氨酯泡沫产品配方包括多元醇组分，异氰酸酯组分和卤代醇组分。 通过具有卤代醇组分的预混物形成聚氨酯泡沫产品。
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6.发明申请Polyester Polyol-Containing Polyurethane Systems Having Improved Hydrolytic Stability 有权具有改善水解稳定性的聚酯多元醇聚氨酯体系公开(公告)号：US20140100298A1
公开(公告)日：2014-04-10
申请号：US14105276
申请日：2013-12-13
IPC分类号： C08G18/18
CPC分类号： C08G18/18 , C08G18/161 , C08G18/1808 , C08G18/546
摘要： An isocyanate reactive composition for making a polyurethane foam includes a tertiary amine urethane catalyst comprising a di(C1-C4)alkyl fatty alkyl amine and a polyester polyol. The use of one or more of fatty alkyl tertiary amine serves to reduce hydrolysis of the polyester polyol in the isocyanate reactive composition.
摘要翻译： 用于制备聚氨酯泡沫的异氰酸酯反应性组合物包括含有二（C 1 -C 4）烷基脂肪烷基胺和聚酯多元醇的叔胺氨基甲酸酯催化剂。 使用一种或多种脂肪烷基叔胺用于减少异氰酸酯反应性组合物中聚酯多元醇的水解。
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7.发明申请Processes, Products, and Compositions Having Tetraalkylguanidine Salt of Aromatic Carboxylic Acid 有权具有芳族羧酸四烷基胍盐的方法，产品和组合物公开(公告)号：US20130131276A1
公开(公告)日：2013-05-23
申请号：US13678736
申请日：2012-11-16
CPC分类号： C07C63/20 , C08G18/08 , C08G18/1858 , C08G18/1875 , C08G18/3206 , C08G18/3275 , C08G18/4072 , C08G18/42 , C08G18/4841 , C08G18/546 , C08G18/632 , C08G18/6674 , C08G18/6688 , C08G18/7621 , C08G18/7671 , C08G65/00 , C08G2101/0008 , C08G2101/0025 , C08G2101/0083
摘要： Disclosed are processes, products, and compositions having tetraalkylguanidine salt of aromatic acid. The processes include providing a pre-mix comprising an aromatic carboxylic acid component and contacting a tetraalkylguanidine with the aromatic carboxylic acid component in the pre-mix to form the tetraalkylguanidine salt of aromatic carboxylic acid or producing a catalyst composition by contacting the tetraalkylguanidine with the aromatic carboxylic acid component to form the tetraalkylguanidine salt of aromatic carboxylic acid. The compositions include the tetraalkylguanidine salt of aromatic carboxylic acid. The product is formed by the tetraalkylguanidine salt of aromatic carboxylic acid.
摘要翻译： 公开了具有芳族酸四烷基胍盐的方法，产品和组合物。 所述方法包括提供包含芳族羧酸组分的预混物，并将四烷基胍与预混物中的芳族羧酸组分接触以形成芳族羧酸的四烷基胍盐，或通过使四烷基胍与芳族羧酸接触来制备催化剂组合物 羧酸组分形成芳族羧酸的四烷基胍盐。 组合物包括芳族羧酸的四烷基胍盐。 产物由芳族羧酸的四烷基胍盐形成。
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公开(公告)号：US20160229945A1
公开(公告)日：2016-08-11
申请号：US15097734
申请日：2016-04-13
发明人： Juan Jesus Burdeniuc
CPC分类号： C08G18/7621 , B01J31/0237 , B01J31/0238 , B01J31/0239 , C08G18/161 , C08G18/163 , C08G18/165 , C08G18/166 , C08G18/18 , C08G18/1808 , C08G18/1825 , C08G18/1833 , C08G18/1875 , C08G18/225 , C08G18/246 , C08G18/4018 , C08G18/4072 , C08G18/42 , C08G18/4208 , C08G18/48 , C08G18/4829 , C08G18/546 , C08G18/63 , C08G18/633 , C08G18/7664 , C08G2101/00 , C08G2101/0008 , C08G2101/0025 , C08G2101/005 , C08L67/00
摘要： This invention discloses the use of sulfite salts as catalysts to make polyurethane polymers. In particular, this invention discloses the use of metal salts such as alkali metal salts as well as alkyl ammonium salts such as tetralkyl ammonium salts as catalysts to make polyurethane polymers. The sulfite salts are useful to make a wide variety of polyurethane polymers and polyurethane foam polymer products such as flexible polyurethane foam polymers, rigid foam polyurethane polymers, semi-rigid polyurethane polymer, microcellular polyurethane polymer, and spray foam polyurethane polymer as well as any polymeric material that requires the assistance of catalysts to promote the formation of urethane and urea bonds such as those found in polyurethane emusions for paints, coatings, protective coatings, lacquer, etc as well as other polyurethane or polyurethane containing materials such as thermoplastic polymers, thermoplastic polyurethane polymers, elastomers, adhesives, sealants, etc. Examples of catalysts comprising the invention include sodium sulfite, potassium sulfite, lithium sulfite, tetramethylammonium sulfite and the like.
摘要翻译： 本发明公开了使用亚硫酸盐作为催化剂制备聚氨酯聚合物。 特别地，本发明公开了使用金属盐如碱金属盐以及烷基铵盐如四烷基铵盐作为催化剂来制备聚氨酯聚合物。 亚硫酸盐可用于制备各种聚氨酯聚合物和聚氨酯泡沫聚合物产品，例如柔性聚氨酯泡沫聚合物，刚性泡沫聚氨酯聚合物，半刚性聚氨酯聚合物，微孔聚氨酯聚合物和喷雾泡沫聚氨酯聚合物以及任何聚合物 需要辅助催化剂促进氨基甲酸酯和脲键形成的材料，例如在用于涂料，涂料，保护涂料，漆等的聚氨酯乳液中发现的那些，以及其它聚氨酯或聚氨酯包含的材料如热塑性聚合物，热塑性聚氨酯 聚合物，弹性体，粘合剂，密封剂等。包含本发明的催化剂的实例包括亚硫酸钠，亚硫酸钾，亚硫酸锂，亚硫酸四甲基铵等。
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公开(公告)号：US20160102169A1
公开(公告)日：2016-04-14
申请号：US14881544
申请日：2015-10-13
发明人： Juan Jesus Burdeniuc
CPC分类号： C08G18/7621 , B01J31/0237 , B01J31/0238 , B01J31/0239 , C08G18/161 , C08G18/163 , C08G18/165 , C08G18/166 , C08G18/18 , C08G18/1808 , C08G18/1825 , C08G18/1833 , C08G18/1875 , C08G18/225 , C08G18/246 , C08G18/4018 , C08G18/4072 , C08G18/42 , C08G18/4208 , C08G18/48 , C08G18/4829 , C08G18/546 , C08G18/63 , C08G18/633 , C08G18/7664 , C08G2101/00 , C08G2101/0008 , C08G2101/0025 , C08G2101/005 , C08L67/00
摘要： This invention discloses the use of sulfite salts as catalysts to make polyurethane polymers. In particular, this invention discloses the use of metal salts such as alkali metal salts as well as alkyl ammonium salts such as tetralkyl ammonium salts as catalysts to make polyurethane polymers. The sulfite salts are useful to make a wide variety of polyurethane polymers and polyurethane foam polymer products such as flexible polyurethane foam polymers, rigid foam polyurethane polymers, semi-rigid polyurethane polymer, microcellular polyurethane polymer, and spray foam polyurethane polymer as well as any polymeric material that requires the assistance of catalysts to promote the formation of urethane and urea bonds such as those found in polyurethane emusions for paints, coatings, protective coatings, lacquer, etc as well as other polyurethane or polyurethane containing materials such as thermoplastic polymers, thermoplastic polyurethane polymers, elastomers, adhesives, sealants, etc. Examples of catalysts comprising the invention include sodium sulfite, potassium sulfite, lithium sulfite, tetramethylammonium sulfite and the like.
摘要翻译： 本发明公开了使用亚硫酸盐作为催化剂制备聚氨酯聚合物。 特别地，本发明公开了使用金属盐如碱金属盐以及烷基铵盐如四烷基铵盐作为催化剂来制备聚氨酯聚合物。 亚硫酸盐可用于制备各种聚氨酯聚合物和聚氨酯泡沫聚合物产品，例如柔性聚氨酯泡沫聚合物，刚性泡沫聚氨酯聚合物，半刚性聚氨酯聚合物，微孔聚氨酯聚合物和喷雾泡沫聚氨酯聚合物以及任何聚合物 需要辅助催化剂促进氨基甲酸酯和脲键形成的材料，例如在用于涂料，涂料，保护涂料，漆等的聚氨酯乳液中发现的那些，以及其它聚氨酯或聚氨酯包含的材料如热塑性聚合物，热塑性聚氨酯 聚合物，弹性体，粘合剂，密封剂等。包含本发明的催化剂的实例包括亚硫酸钠，亚硫酸钾，亚硫酸锂，亚硫酸四甲基铵等。
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10.发明申请公开(公告)号：US20160032042A1
公开(公告)日：2016-02-04
申请号：US14867114
申请日：2015-09-28
CPC分类号： C08G18/14 , C08G18/302 , C08G18/3206 , C08G18/343 , C08G18/36 , C08G18/4841 , C08G18/6696 , C08G18/7621 , C08G2101/0008 , C08G2101/005 , C08G2101/0083 , C08J2205/06 , C08K5/0008 , C08K5/05 , C08K5/06 , C08K5/20 , C08K5/315 , C08K5/3445 , C08K5/41 , C08K5/45
摘要： A composition and process useful to make flexible polyurethane foams and in particular flexible molded polyurethane foams is disclosed. The usage of dipolar aprotic liquids such as DMSO, DMI, sulfolane, N-methyl-acetoacetamide, N, N-dimethylacetoacetamide as well as glycols containing hydroxyl numbers OH#≦1100 as cell opening aides for 2-cyanoacetamide or other similar molecules containing active methylene or methine groups to make a polyurethane foam is also disclosed. The advantage of using cell opener aids results in a) no foam shrinkage; b) lower use levels of cell opener; c) foam performance reproducibility d) optimum physical properties. In addition, combining the acid blocked amine catalyst together with the cell opener and the cell opener aid results in a less corrosive mixture as well as provides a method that does not require mechanical crushing for cell opening.
摘要翻译： 公开了用于制备柔性聚氨酯泡沫，特别是柔性模塑聚氨酯泡沫的组合物和方法。 使用偶极非质子液体如DMSO，DMI，环丁砜，N-甲基 - 乙酰乙酰胺，N，N-二甲基乙酰乙酰胺以及含有羟基数OH＃＆amp; 1100的二醇作为2-氰基乙酰胺或其它类似分子的开放助剂 还公开了制备聚氨酯泡沫的活性亚甲基或次甲基。 使用细胞开放助剂的优点导致a）没有泡沫收缩; b）细胞开放剂的使用水平较低; c）泡沫性能重现性d）最佳物理性能。 此外，将酸封闭的胺催化剂与开孔剂和开孔剂组合在一起导致较少的腐蚀性混合物，并且提供了不需要机械破碎以进行开孔的方法。
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