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公开(公告)号：US08383293B2
公开(公告)日：2013-02-26
申请号：US11562712
申请日：2006-11-22
申请人： Belabbes Merzougui , Jon C. Halalay , John T. Johnson , Gregory C. Garabedian , Michael P. Balogh , Swathy Swathirajan
发明人： Belabbes Merzougui , Jon C. Halalay , John T. Johnson , Gregory C. Garabedian , Michael P. Balogh , Swathy Swathirajan
IPC分类号： H01M4/90
CPC分类号： H01M4/90 , H01M4/9091 , H01M4/92 , H01M4/925 , H01M4/96 , H01M2008/1095
摘要： An electrocatalyst for fuel cell applications includes a catalyst support and a noble metal or noble metal-based alloy catalyst supported upon the catalyst support. The catalyst support characteristically includes a Group IV-VI transition metal silicide with or without the mixing of carbon. A fuel cell incorporating the electrocatalyst into the anode and/or cathode is disclosed. Such fuel cell exhibit improved cycling and operating performance.
摘要翻译： 用于燃料电池应用的电催化剂包括催化剂载体和负载在催化剂载体上的贵金属或贵金属基合金催化剂。 催化剂载体的特征在于包括具有或不具有碳的混合物的IV-VI族过渡金属硅化物。 公开了将电催化剂并入阳极和/或阴极的燃料电池。 这种燃料电池表现出改善的循环和操作性能。
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公开(公告)号：US20080118818A1
公开(公告)日：2008-05-22
申请号：US11562712
申请日：2006-11-22
申请人： Belabbes Merzougui , Ion C. Halalay , John T. Johnson , Gregory C. Garabedian , Michael P. Balogh , Swathy Swathirajan
发明人： Belabbes Merzougui , Ion C. Halalay , John T. Johnson , Gregory C. Garabedian , Michael P. Balogh , Swathy Swathirajan
CPC分类号： H01M4/90 , H01M4/9091 , H01M4/92 , H01M4/925 , H01M4/96 , H01M2008/1095
摘要： An electrocatalyst for fuel cell applications includes a catalyst support and a noble metal or noble metal-based alloy catalyst supported upon the catalyst support. The catalyst support characteristically includes a Group IV-VI transition metal silicide with or without the mixing of carbon. A fuel cell incorporating the electrocatalyst into the anode and/or cathode is disclosed. Such fuel cell exhibit improved cycling and operating performance.
摘要翻译： 用于燃料电池应用的电催化剂包括催化剂载体和负载在催化剂载体上的贵金属或贵金属基合金催化剂。 催化剂载体的特征在于包括具有或不具有碳的混合物的IV-VI族过渡金属硅化物。 公开了将电催化剂并入阳极和/或阴极的燃料电池。 这种燃料电池表现出改善的循环和操作性能。
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3.发明授权公开(公告)号：US08557485B2
公开(公告)日：2013-10-15
申请号：US12332440
申请日：2008-12-11
申请人： Ion C. Halalay , Belabbes Merzougui , Gregory C. Garabedian , Michael P. Balogh , Swathy Swathirajan
发明人： Ion C. Halalay , Belabbes Merzougui , Gregory C. Garabedian , Michael P. Balogh , Swathy Swathirajan
IPC分类号： H01M4/02
CPC分类号： H01M8/04216 , H01M4/8647 , H01M4/92 , H01M4/926 , H01M8/1007
摘要： The incorporation of tungsten-containing hydrogen spillover materials into a composite fuel cell anode can be helpful in preserving the carbon catalyst support materials in the fuel cell cathode during periods of hydrogen starvation. Preferred examples of such tungsten-containing hydrogen spillover materials are tungsten oxides and tungsten silicides. These materials, when physically mixed with catalyst-loaded carbon support particles in a composite anode, have shown the ability to promote hydrogen storage in amounts that, during a disruption of hydrogen gas flow, can postpone an anodic potential excursion into the oxygen evolution region for a period of at least several seconds.
摘要翻译： 将含钨氢气溢出物质掺入复合燃料电池阳极可有助于在氢气饥饿期间保持燃料电池阴极中的碳催化剂载体材料。 这种含钨氢气溢出材料的优选实例是钨氧化物和硅化钨。 这些材料在复合阳极中与催化剂负载的碳载体颗粒物理混合时已经显示出促进氢储存的能力，其量在氢气流动破坏期间可以将阳极电位偏移推迟到氧气进入区域 至少几秒的时间。
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公开(公告)号：US20100151295A1
公开(公告)日：2010-06-17
申请号：US12332440
申请日：2008-12-11
申请人： Ion C. Halalay , Belabbes Merzougui , Gregory C. Garabedian , Michael P. Balogh , Swathy Swathirajan
发明人： Ion C. Halalay , Belabbes Merzougui , Gregory C. Garabedian , Michael P. Balogh , Swathy Swathirajan
IPC分类号： H01M8/10
CPC分类号： H01M8/04216 , H01M4/8647 , H01M4/92 , H01M4/926 , H01M8/1007
摘要： The incorporation of tungsten-containing hydrogen spillover materials into a composite fuel cell anode can be helpful in preserving the carbon catalyst support materials in the fuel cell cathode during periods of hydrogen starvation. Preferred examples of such tungsten-containing hydrogen spillover materials are tungsten oxides and tungsten silicides. These materials, when physically mixed with catalyst-loaded carbon support particles in a composite anode, have shown the ability to promote hydrogen storage in amounts that, during a disruption of hydrogen gas flow, can postpone an anodic potential excursion into the oxygen evolution region for a period of at least several seconds.
摘要翻译： 将含钨氢气溢出物质掺入复合燃料电池阳极可有助于在氢气饥饿期间保持燃料电池阴极中的碳催化剂载体材料。 这种含钨氢气溢出材料的优选实例是钨氧化物和硅化钨。 这些材料在复合阳极中与催化剂负载的碳载体颗粒物理混合时已经显示出促进氢储存的能力，其量在氢气流动破坏期间可以将阳极电位偏移推迟到氧气进入区域 至少几秒的时间。
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公开(公告)号：US08257979B2
公开(公告)日：2012-09-04
申请号：US11938521
申请日：2007-11-12
IPC分类号： G01N27/00
CPC分类号： H01M8/1004 , G01N15/088 , G01N2015/0846
摘要： A method for evaluating the composition of an MEA for a fuel cell. The method includes soaking the MEA in an unsaturated organic compound for a predetermined period of time, and then allowing the MEA to dry. The method then includes staining the MEA with osmium tetroxide (OsO4) in a closed container. The stained MEA is then encased in an epoxy. Thin sections of the encapsulated MEA are then prepared, and the sections are viewed through a transmission electron microscope. The stained MEA will show dark regions where the ionomer and carbon particles are located and lighter regions that are epoxy filled pores.
摘要翻译： 一种用于评估燃料电池的MEA的组成的方法。 该方法包括将MEA浸渍在不饱和有机化合物中预定的时间，然后使MEA干燥。 然后该方法包括在密闭容器中用四氧化锇（OsO 4）染色MEA。 然后将染色的MEA包裹在环氧树脂中。 然后制备包封的MEA的薄截面，并通过透射电子显微镜观察切片。 染色的MEA将显示离子交联聚合物和碳颗粒位于的较暗区域以及环氧树脂填充孔的较浅的区域。
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6.发明授权公开(公告)号：US07695974B2
公开(公告)日：2010-04-13
申请号：US12021675
申请日：2008-01-29
IPC分类号： G01N21/75
CPC分类号： G01N23/04
摘要： A method for evaluating the spatial distribution of an ionomer in a fuel cell MEA. The method includes embedding the MEA in an epoxy, and then slicing thin sections from the MEA. The sliced sections are then exposed to a titanium tetrachloride vapor that stains the epoxy. The stained sections are then viewed with, for example, a transmission electron microscope (TEM) where the lighter regions in the TEM image show the ionomer distribution.
摘要翻译： 一种用于评估燃料电池MEA中离聚物的空间分布的方法。 该方法包括将MEA嵌入环氧树脂中，然后从MEA切片薄切片。 然后将切片切片暴露于污染环氧树脂的四氯化钛蒸汽。 然后用例如透射电子显微镜（TEM）观察染色部分，其中TEM图像中的较亮区域显示离聚物分布。
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公开(公告)号：US07651732B2
公开(公告)日：2010-01-26
申请号：US11851594
申请日：2007-09-07
摘要： Films of magnesium mixed with titanium are produced by non-equilibrium alloying processes such as electron beam evaporation of magnesium and titanium ingots in a very low pressure chamber. Such magnesium-titanium films form as single phase solid solutions. Titanium is inherently resistant to corrosion and its admixture with magnesium in solid solution provides a new composition that is less subject to intra-film galvanic corrosion. The magnesium-titanium films also provide relatively hard and strong coatings.
摘要翻译： 与钛混合的薄膜是通过非平衡合金化工艺制造的，例如在非常低的压力室中的镁和钛锭的电子束蒸发。 这种镁 - 钛膜形成为单相固溶体。 钛本身具有耐腐蚀性，并且与固体溶液中的镁的混合物提供了较少受到膜内电镀腐蚀的新组合物。 镁 - 钛膜也提供相对硬和强的涂层。
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8.发明申请公开(公告)号：US20080274033A1
公开(公告)日：2008-11-06
申请号：US11743826
申请日：2007-05-03
申请人： Gregory P. Meisner , Aimee G. Bailey , Michael P. Balogh , Frederick E. Pinkerton , Martin S. Meyer
发明人： Gregory P. Meisner , Aimee G. Bailey , Michael P. Balogh , Frederick E. Pinkerton , Martin S. Meyer
CPC分类号： C01B3/065 , C01B6/04 , C01B6/21 , C01C1/026 , Y02E60/327 , Y02E60/362 , Y02E60/364
摘要： Methods of generating hydrogen-containing streams having a minimal concentration of gaseous reactive nitrogen-containing compounds, e.g., ammonia, are provided. Hydrogen storage material systems are also provided that generate such hydrogen-containing streams. A first composition comprising a nitride, a second composition comprising a hydride, and a third composition having a cation selected from the group consisting of: alkali metals, alkaline earth metals, and mixtures thereof are combined together. The hydrogen-containing stream thus generated has a minimal concentration of gaseous reactive nitrogen-containing compounds.
摘要翻译： 提供了产生具有最小浓度的气态反应性含氮化合物例如氨的含氢气流的方法。 还提供了产生这种含氢流的储氢材料体系。 包含氮化物的第一组合物，包含氢化物的第二组合物和具有选自碱金属，碱土金属及其混合物的阳离子的第三组合物组合在一起。 由此产生的含氢气流具有最小浓度的气态反应性含氮化合物。
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公开(公告)号：US07029649B2
公开(公告)日：2006-04-18
申请号：US10649923
申请日：2003-08-26
CPC分类号： C01B3/065 , C01B3/001 , C01B6/04 , C01B21/0923 , C01B21/0926 , Y02E60/324 , Y02E60/362 , Y02E60/364
摘要： The invention provides a method of reversibly producing a source of hydrogen gas comprising mixing together a plurality of hydrogen-containing starting materials; and then heating the mixed materials at a temperature sufficient to release hydrogen. Upon release of hydrogen, there is formed a residue which comprises at least one material different from the starting materials. There is also synergy whereby it is possible to regenerate at least one of the hydrogen-containing starting materials by exposing hydrogen gas to the aforesaid residue.
摘要翻译： 本发明提供了可逆地生产氢气源的方法，包括将多个含氢原料混合在一起; 然后在足以释放氢气的温度下加热混合材料。 在释放氢时，形成残渣，该残渣包含至少一种不同于原料的材料。 还有协同作用，通过将氢气暴露于上述残留物中，可以再生含氢原料中的至少一种。
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10.发明申请公开(公告)号：US20130330654A1
公开(公告)日：2013-12-12
申请号：US13493113
申请日：2012-06-11
申请人： Michael P. Balogh , Gayatri Vyas Dadheech , Nicholas P. Irish , Misle M. Tessema , Daniel P. Miller , Mahmoud H. Abd Elhamid
发明人： Michael P. Balogh , Gayatri Vyas Dadheech , Nicholas P. Irish , Misle M. Tessema , Daniel P. Miller , Mahmoud H. Abd Elhamid
CPC分类号： C25D3/48 , C25D5/50 , H01M8/0206 , H01M8/0228
摘要： A method of depositing a thin gold coating on bipolar plate substrates for use in fuel cells includes depositing a gold coating onto at least one surface of the bipolar plate substrate followed by annealing the gold coating at a temperature between about 200° C. to 500° C. The annealed gold coating has a reduced porosity in comparison with a coating which has not been annealed, and provides improved corrosion resistance to the underlying metal comprising the bipolar plate.
摘要翻译： 在用于燃料电池的双极板基板上沉积薄金涂层的方法包括将金涂层沉积在双极板基板的至少一个表面上，然后在约200℃至500℃的温度下退火金涂层 与未经退火的涂层相比，退火的金涂层具有降低的孔隙率，并且对包含双极板的底层金属提供改善的耐腐蚀性。
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