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    Method and apparatus for regenerating catalyst during oxygenates to olefins reaction
    1.
    发明授权
    Method and apparatus for regenerating catalyst during oxygenates to olefins reaction 有权
    在含氧化合物到烯烃反应过程中再生催化剂的方法和装置

    公开(公告)号：US08178741B2

    公开(公告)日：2012-05-15

    申请号：US12793340

    申请日：2010-06-03

    申请人： Chunshe J. Cao ,  James H. Beech, Jr. ,  Michael P. Nicoletti ,  Thomas H. Colle ,  Teng Xu ,  Stephen N. Vaughn

    发明人： Chunshe J. Cao ,  James H. Beech, Jr. ,  Michael P. Nicoletti ,  Thomas H. Colle ,  Teng Xu ,  Stephen N. Vaughn

    IPC分类号： C07C1/00 ,  B01J20/34 ,  B01J19/00

    CPC分类号： B01J38/02 ,  B01J29/90 ,  B01J38/32 ,  C07C1/20 ,  C07C2529/85 ,  Y02P20/584 ,  C07C11/02

    摘要： Disclosed herein is a method of recovery of the activity of a molecular sieve catalyst following use of the catalyst in an OTO conversion process. This is achieved by a regeneration apparatus and a method of regenerating a molecular sieve catalyst, comprising two stages. In a pretreatment stage, the catalyst is pretreated under pretreatment conditions by heating the catalyst to a temperature of between 320° C. to 700° C. in an oxygen depleted medium for a residence time of between 1 minute to two hours; and, in a regeneration stage, the catalyst is regenerated under regeneration conditions by heating the catalyst at a temperature of between 200° C. to 700° C. in an oxidizing medium for a residence time of between 1 to 60 minutes.

    摘要翻译： 本文公开了在OTO转化方法中使用催化剂后回收分子筛催化剂的活性的方法。 这是通过再生装置和再生分子筛催化剂的方法实现的，包括两个阶段。 在预处理阶段，催化剂在预处理条件下通过将催化剂在耗氧贫乏的介质中在320℃至700℃之间的温度下进行预处理，停留时间为1分钟至2小时; 并且在再生阶段，催化剂在再生条件下通过在氧化介质中在200℃至700℃的温度下加热催化剂，停留时间为1至60分钟而再生。

    Method And Apparatus For Regenerating Catalyst During Oxygenates To Olefins Reaction
    2.
    发明申请
    Method And Apparatus For Regenerating Catalyst During Oxygenates To Olefins Reaction 有权
    氧化催化剂再生催化剂对烯烃反应的方法与装置

    公开(公告)号：US20110021857A1

    公开(公告)日：2011-01-27

    申请号：US12793340

    申请日：2010-06-03

    申请人： Chunshe J. Cao ,  James H. Beech, JR. ,  Michael P. Nicoletti ,  Thomas H. Colle ,  Teng Xu ,  Stephen N. Vaughn

    发明人： Chunshe J. Cao ,  James H. Beech, JR. ,  Michael P. Nicoletti ,  Thomas H. Colle ,  Teng Xu ,  Stephen N. Vaughn

    IPC分类号： C07C1/00 ,  B01J20/34 ,  B01J19/00

    CPC分类号： B01J38/02 ,  B01J29/90 ,  B01J38/32 ,  C07C1/20 ,  C07C2529/85 ,  Y02P20/584 ,  C07C11/02

    摘要： Disclosed herein is a method of recovery of the activity of a molecular sieve catalyst following use of the catalyst in an OTO conversion process. This is achieved by a regeneration apparatus and a method of regenerating a molecular sieve catalyst, comprising two stages. In a pretreatment stage, the catalyst is pretreated under pretreatment conditions by heating the catalyst to a temperature of between 320° C. to 700° C. in an oxygen depleted medium for a residence time of between 1 minute to two hours; and, in a regeneration stage, the catalyst is regenerated under regeneration conditions by heating the catalyst at a temperature of between 200° C. to 700° C. in an oxidizing medium for a residence time of between 1 to 60 minutes.

    摘要翻译： 本文公开了在OTO转化方法中使用催化剂后回收分子筛催化剂的活性的方法。 这是通过再生装置和再生分子筛催化剂的方法实现的，包括两个阶段。 在预处理阶段，催化剂在预处理条件下通过将催化剂在耗氧贫乏的介质中在320℃至700℃之间的温度下进行预处理，停留时间为1分钟至2小时; 并且在再生阶段，催化剂在再生条件下通过在氧化介质中在200℃至700℃的温度下加热催化剂，停留时间为1至60分钟而再生。

    Method of circulating catalyst between a catalyst regenerator and an external catalyst cooler
    4.
    发明授权
    Method of circulating catalyst between a catalyst regenerator and an external catalyst cooler 有权
    在催化剂再生器和外部催化剂冷却器之间循环催化剂的方法

    公开(公告)号：US07906697B2

    公开(公告)日：2011-03-15

    申请号：US12059717

    申请日：2008-03-31

    申请人： James H. Beech, Jr. ,  Chunshe Cao ,  Michael P. Nicoletti ,  James R. Lattner ,  Jesse F. Goellner ,  Rutton D. Patel ,  Timothy M. Healy

    发明人： James H. Beech, Jr. ,  Chunshe Cao ,  Michael P. Nicoletti ,  James R. Lattner ,  Jesse F. Goellner ,  Rutton D. Patel ,  Timothy M. Healy

    IPC分类号： C07C2/04

    CPC分类号： C07C1/20 ,  B01J29/90 ,  B01J38/30 ,  B01J38/32 ,  C07C2529/40 ,  C07C2529/70 ,  C07C2529/83 ,  C07C2529/85 ,  C10G3/49 ,  C10G3/62 ,  C10G2300/802 ,  C10G2400/20 ,  Y02P20/584 ,  Y02P30/20 ,  C07C11/02

    摘要： This invention relates to efficiently regenerating catalyst particles by minimizing the formation of localized “hot spots” and “cold spots” in a regeneration zone. Specifically this invention relates to a method for controlling regenerator temperature in an oxygenates-to-olefins system, comprising the steps of: contacting an oxygenate feed in a reactor with a catalytically effective amount of molecular sieve-containing catalyst under conditions effective for converting said oxygenate to a product containing light olefins and forming a coked catalyst; contacting a portion of the coked catalyst in a regenerator, having a catalyst bed height (Hc), an inlet height (Hi), and an outlet height (Ho), with an oxygen-containing regeneration medium under conditions effective to at least partially regenerate the coked catalyst; and conducting a portion of the catalyst from the regenerator to a catalyst cooler to form a cooled catalyst portion, wherein Ho is greater than Hi.

    摘要翻译： 本发明涉及通过最小化再生区中局部“热点”和“冷点”的形成来有效地再生催化剂颗粒。 具体地说，本发明涉及一种用于控制含氧化合物至烯烃体系中的再生器温度的方法，其包括以下步骤：在有效转化所述含氧化合物的条件下使反应器中的含氧化合物进料与催化有效量的含分子筛催化剂接触 涉及含有轻质烯烃并形成焦化催化剂的产品; 在具有催化剂床高度（Hc），入口高度（Hi）和出口高度（Ho））的再生器中使一部分焦化催化剂与含氧再生介质在有效至少部分再生的条件下接触 焦化催化剂; 并将催化剂的一部分从再生器导入催化剂冷却器以形成冷却的催化剂部分，其中Ho大于Hi。

    Method Of Circulating Catalyst Between A Catalyst Regenerator And An External Catalyst Cooler
    7.
    发明申请
    Method Of Circulating Catalyst Between A Catalyst Regenerator And An External Catalyst Cooler 有权
    催化剂再生器与外部催化剂冷却器之间循环催化剂的方法

    公开(公告)号：US20090192341A1

    公开(公告)日：2009-07-30

    申请号：US12059717

    申请日：2008-03-31

    申请人： James H. Beech, JR. ,  Chunshe Cao ,  Michael P. Nicoletti ,  James R. Lattner ,  Jesse F. Goellner ,  Rutton D. Patel ,  Timothy M. Healy

    发明人： James H. Beech, JR. ,  Chunshe Cao ,  Michael P. Nicoletti ,  James R. Lattner ,  Jesse F. Goellner ,  Rutton D. Patel ,  Timothy M. Healy

    IPC分类号： C07C2/04

    CPC分类号： C07C1/20 ,  B01J29/90 ,  B01J38/30 ,  B01J38/32 ,  C07C2529/40 ,  C07C2529/70 ,  C07C2529/83 ,  C07C2529/85 ,  C10G3/49 ,  C10G3/62 ,  C10G2300/802 ,  C10G2400/20 ,  Y02P20/584 ,  Y02P30/20 ,  C07C11/02

    摘要： This invention relates to efficiently regenerating catalyst particles by minimizing the formation of localized “hot spots” and “cold spots” in a regeneration zone. Specifically this invention relates to a method for controlling regenerator temperature in an oxygenates-to-olefins system, comprising the steps of: contacting an oxygenate feed in a reactor with a catalytically effective amount of molecular sieve-containing catalyst under conditions effective for converting said oxygenate to a product containing light olefins and forming a coked catalyst; contacting a portion of the coked catalyst in a regenerator, having a catalyst bed height (Hc), an inlet height (Hi), and an outlet height (Ho), with an oxygen-containing regeneration medium under conditions effective to at least partially regenerate the coked catalyst; and conducting a portion of the catalyst from the regenerator to a catalyst cooler to form a cooled catalyst portion, wherein Ho is greater than Hi.

    摘要翻译： 本发明涉及通过最小化再生区中局部“热点”和“冷点”的形成来有效地再生催化剂颗粒。 具体地说，本发明涉及一种用于控制含氧化合物至烯烃体系中的再生器温度的方法，包括以下步骤：在有效转化所述含氧化合物的条件下使反应器中的含氧化合物进料与催化有效量的含分子筛的催化剂接触 涉及含有轻质烯烃并形成焦化催化剂的产品; 在具有催化剂床高度（Hc），入口高度（Hi）和出口高度（Ho））的再生器中使一部分焦化催化剂与含氧再生介质在有效至少部分再生的条件下接触 焦化催化剂; 并将催化剂的一部分从再生器导入催化剂冷却器以形成冷却的催化剂部分，其中Ho大于Hi。

    Method Of Separating Condensed Liquid From An Olefin Stream
    9.
    发明申请
    Method Of Separating Condensed Liquid From An Olefin Stream 有权
    从烯烃流中分离浓缩液体的方法

    公开(公告)号：US20080188700A1

    公开(公告)日：2008-08-07

    申请号：US12023459

    申请日：2008-01-31

    申请人： Gerald G. McGlamery ,  Michael P. Nicoletti ,  Thomas H. Colle

    发明人： Gerald G. McGlamery ,  Michael P. Nicoletti ,  Thomas H. Colle

    IPC分类号： C07C1/00 ,  C07C7/10

    CPC分类号： C07C7/10 ,  C07C1/20 ,  C07C11/02

    摘要： This invention is to a process for separating condensed water and entrained solids from an olefin stream so that fouling of the separation equipment by the entrained solids is reduced or eliminated. The process involves injecting an antifouling agent into a water condensing or quench system in an amount to maintain a zeta potential of fouling liquid and a zeta potential of the surface of the quench system both in a positive range or both in a negative range.

    摘要翻译： 本发明涉及从烯烃流中分离冷凝水和夹带固体的方法，从而减少或消除夹带的固体污染分离设备。 该方法包括将防污剂注入到水冷凝或骤冷系统中，其量使得维持窒息液体的ζ电位和猝灭系统表面的ζ电位均处于正的范围，或者在负的范围内。

    Method of separating condensed liquid from an olefin stream
    10.
    发明授权
    Method of separating condensed liquid from an olefin stream 有权
    从烯烃流中分离冷凝液的方法

    公开(公告)号：US07893310B2

    公开(公告)日：2011-02-22

    申请号：US12023459

    申请日：2008-01-31

    申请人： Gerald G. McGlamery, Jr. ,  Michael P. Nicoletti ,  Thomas H. Colle

    发明人： Gerald G. McGlamery, Jr. ,  Michael P. Nicoletti ,  Thomas H. Colle

    IPC分类号： C07C1/00 ,  C07C7/10

    CPC分类号： C07C7/10 ,  C07C1/20 ,  C07C11/02

    摘要： This invention is to a process for separating condensed water and entrained solids from an olefin stream so that fouling of the separation equipment by the entrained solids is reduced or eliminated. The process involves injecting an antifouling agent into a water condensing or quench system in an amount to maintain a zeta potential of fouling liquid and a zeta potential of the surface of the quench system both in a positive range or both in a negative range.

    摘要翻译： 本发明涉及从烯烃流中分离冷凝水和夹带固体的方法，从而减少或消除夹带的固体污染分离设备。 该方法包括将防污剂注入到水冷凝或骤冷系统中，其量使得维持窒息液体的ζ电位和猝灭系统表面的ζ电位均处于正的范围，或者在负的范围内。