Process for the removal of residual constituents
    3.
    发明授权
    Process for the removal of residual constituents 失效
    去除残留成分的方法

    公开(公告)号:US4637857A

    公开(公告)日:1987-01-20

    申请号:US671263

    申请日:1984-11-14

    CPC分类号: B01D3/38 B01D1/14 Y10S159/10

    摘要: The instant invention is directed to a process for stripping of a residual component from a liquid having a viscosity of from 300 to 10,000 poises in which the liquid flows in the form of a ring flow supported by a gas stream flowing in the core, through a tube into a separator vessel, the tube having a continuous coil shape and a conduit diameter to helix diameter of from 0.1:1 to 0.04:1, the improvement comprising adding to the gas stream from 10 to 90%, by weight, of externally generated steam and/or an inert gas at an adjusted pressure of from 50 m bars to 1 bar in the separator vessel for a gas and/or steam velocity in the tube of from 100 m/sec to the speed of sound. The added gas and/or steam generates thorough transverse mixing in the liquid ring flow.

    摘要翻译: 本发明涉及一种从粘度为300至10,000泊的液体中除去残留组分的方法,其中液体以由在芯中流动的气流支撑的环流的形式流动,通过 管进入分离器容器,该管具有连续的线圈形状和直径为0.1:1至0.04:1的螺旋直径,其改进包括将气流从10至90重量%加入到外部产生的 蒸汽和/或在分离器容器中调节压力为50m至1bar的惰性气体,其中管道中的气体和/或蒸汽速度为100m / sec至声速。 添加的气体和/或蒸汽在液体环流中产生彻底的横向混合。

    Continuous process for the separation of solutions and suspensions
    6.
    发明授权
    Continuous process for the separation of solutions and suspensions 失效
    用于分离溶液和悬浮液的连续方法

    公开(公告)号:US5164030A

    公开(公告)日:1992-11-17

    申请号:US673727

    申请日:1991-03-22

    摘要: In the thermal separation of solutions and suspensions into a free-flowing solid and into a largely solid-free distillate, the useful product can be almost completely recovered in a pure state, and the amount of waste product can thus be reduced, by carrying out the concentrating in a first heatable flow pipe (6) up to an upper limit which is given by a creeping coverage of the inside wall with solid and/or by a total blockage of the flow cross-section and then continuing the concentrating in a second flow pipe (9) which is made as a rotary pipe or as a paddle shaft apparatus and whose inside wall (12) is scraped continuously, and separating the vapors and solids from one another at the end of this flow pipe (9).

    摘要翻译: 在将溶液和悬浮液热分解成自由流动的固体并进入大部分无固体的馏出物中时,有用的产物可以在纯的状态下几乎完全回收,从而可以减少废物的量,通过进行 集中在第一可加热流动管道(6)中,直到达到上限,其由固体内壁的蠕变覆盖和/或通过流动横截面的完全堵塞而给出,然后在第二个 流动管(9),其形成为旋转管或作为桨轴装置,并且其内壁(12)被连续地刮擦,并且在该流管(9)的端部处彼此分离蒸气和固体。

    Process for the production of polycarbonate agglomerate
    7.
    发明授权
    Process for the production of polycarbonate agglomerate 失效
    生产聚碳酸酯聚集体的方法

    公开(公告)号:US5852157A

    公开(公告)日:1998-12-22

    申请号:US810263

    申请日:1997-03-03

    CPC分类号: B01J2/02

    摘要: This invention relates to a process for the production of polycarbonate agglomerate of high bulk density from polycarbonate solutions, in which the organic solvent is stripped from a solution of polycarbonate by means of steam, and which is characterised in that the resulting suspension of polycarbonate particles, condensed water and water- and solvent vapor is fed in a tube or tubular heat exchanger to a separator which is partially filled with water and which is under elevated pressure. The polycarbonate agglomerates are discharged, together with part of the water, via a pressure lock at the bottom of the separator.

    摘要翻译: 本发明涉及由聚碳酸酯溶液制备高堆积密度的聚碳酸酯聚集体的方法,其中有机溶剂通过蒸汽从聚碳酸酯溶液中剥离,其特征在于所得的聚碳酸酯颗粒悬浮液, 冷凝水和水和溶剂蒸汽在管或管式热交换器中进料到部分被水填充并且处于升高压力下的分离器中。 聚碳酸酯附聚物与部分水一起通过分离器底部的压力锁定排出。

    Method for isolating polymers from solutions
    9.
    发明授权
    Method for isolating polymers from solutions 失效
    从溶液中分离聚合物的方法

    公开(公告)号:US06506281B1

    公开(公告)日:2003-01-14

    申请号:US09719891

    申请日:2001-03-02

    IPC分类号: B01D122

    摘要: A process of evaporating a viscous polymer solution is described. The process includes: (a) providing a viscous polymer solution including at least 30 wt. % of solvents and monomers; (b) introducing the viscous polymer solution into a heated helix (5), the heated helix having a vapor exit velocity of 200 to 300 m/s, (a film flow including a two-phase mixture of polymer melt, and solvent vapors and monomer vapors being formed within the helix); (c) forwarding the film flow from helix (5) into a heated vapor separator (6); (d) expanding the two-phase mixture of polymer melt, and solvent vapors and monomer vapors of the film flow within vapor separator (6) at an absolute pressure of 10 mbar to 800 mbar, (a bottom product including a concentrated melt of the polymer is formed within the vapor separator); and (e) withdrawing the bottom product from vapor separator (6). Each of the helix (5) and vapor separator (6) have a separate heating device, and each of heating device independently provides a temperature that is above the softening point of the polymer.

    摘要翻译: 描述蒸发粘性聚合物溶液的方法。 该方法包括:(a)提供粘性聚合物溶液,其包含至少30wt。 %的溶剂和单体; (b)将粘性聚合物溶液引入加热的螺旋(5)中,加热的螺旋具有200-300m / s的蒸气出口速度(包括聚合物熔体和溶剂蒸气的两相混合物的膜流和 单体蒸气在螺旋内形成); (c)将膜流从螺旋(5)转移到加热的蒸气分离器(6)中; (d)在10毫巴至800毫巴的绝对压力下,将蒸气分离器(6)内的聚合物熔体和溶剂蒸气和单体蒸气的溶剂蒸气和单体蒸气膨胀(包括含有 聚合物形成在蒸气分离器内); 和(e)从蒸气分离器(6)中取出底部产物。 螺旋(5)和蒸汽分离器(6)中的每一个具有单独的加热装置,并且每个加热装置独立地提供高于聚合物软化点的温度。

    Continuous process for concentrating solutions containing salts and
resins
    10.
    发明授权
    Continuous process for concentrating solutions containing salts and resins 失效
    用于浓缩含有盐和树脂的溶液的连续方法

    公开(公告)号:US5268073A

    公开(公告)日:1993-12-07

    申请号:US957678

    申请日:1992-10-07

    IPC分类号: B01D1/02

    CPC分类号: B01D1/02 Y10S159/13

    摘要: In concentrating solutions containing 1 to 10% by weight of salts and resins, the yield and economics and trouble-free running can be improved by using a flow tube which has a steady curvature at least in the last third and is sized in its diameter in such a way that the mean flow velocity at the tube outlet is at least 50 m/second, and at least 90% by weight of the vaporizable components are evaporated off at driving temperature gradients of 20.degree. to 200.degree. C. between the heating medium and the solution.

    摘要翻译: 在含有1至10重量%盐和树脂的浓缩溶液中,可以通过使用至少在最后三分之一具有稳定曲率并且其直径大小的流管来提高产量和经济性和无故障运行 这样一种方式使得管出口处的平均流速至少为50m /秒,并且在20至200℃的驱动温度梯度下,可蒸发组分的至少90重量%在加热介质 和解决方案。