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    Combinatorial preparation and testing of heterogeneous catalysts
    6.
    发明申请
    Combinatorial preparation and testing of heterogeneous catalysts 审中-公开
    组合制备和非均相催化剂的试验

    公开(公告)号：US20060127287A1

    公开(公告)日：2006-06-15

    申请号：US11336843

    申请日：2006-01-23

    申请人： Hartmut Hibst ,  Andreas Tenten ,  Dirk Demuth ,  Ferdi Schueth ,  Stephan Schunk

    发明人： Hartmut Hibst ,  Andreas Tenten ,  Dirk Demuth ,  Ferdi Schueth ,  Stephan Schunk

    IPC分类号： D21C11/00

    CPC分类号： B01J19/0046 ,  B01J37/0215 ,  B01J37/0217 ,  B01J2219/00286 ,  B01J2219/00306 ,  B01J2219/00511 ,  B01J2219/00585 ,  B01J2219/0059 ,  B01J2219/00599 ,  B01J2219/00747

    摘要： The array of heterogeneous catalysts and/or their precursors, is made up of a body which has, preferably parallel, through-channels and in which at least n channels comprise n different heterogeneous catalysts and/or their precursors, where n is 2, preferably 10, particularly preferably 100, in particular 1000, especially 10,000. A process for preparing arrays comprising the following steps: a1) preparing solutions, emulsions and/or dispersions of elements and/or element compounds of the elements present in the catalyst and/or catalyst precursor and, if appropriate preparing dispersions of inorganic support materials, a2) if appropriate introducing adhesion promoters, binders, viscosity regulators, pH regulators and/or solid inorganic supports into the solutions, emulsions and/or dispersions, a3) simultaneously or successively coating the channels of the body with the solutions, emulsions and/or dispersions, a predetermined amount of the solutions, emulsions and/or dispersions being introduced into each channel to obtain a predetermined composition and a4) if appropriate heating the coated body in the presence or absence of inert gases or reactive gases to a temperature in the range from 20 to 1500° C. to dry, with or without sintering or calcining, the catalysts and/or catalyst precursors.

    摘要翻译： 非均相催化剂和/或其前体的阵列由具有优选平行的通道的主体组成，其中至少n个通道包含n个不同的非均相催化剂和/或其前体，其中n为2，优选为 10，特别优选100，特别是1000，特别是10,000。 一种制备阵列的方法，包括以下步骤：a1）制备存在于催化剂和/或催化剂前体中的元素和/或元素化合物的溶液，乳液和/或分散体，以及如果合适的话，制备无机载体材料的分散体， a2）如果合适，将粘合促进剂，粘合剂，粘度调节剂，pH调节剂和/或固体无机载体引入溶液，乳液和/或分散体中，a3）用溶液，乳液和/或分散体同时或连续地涂覆身体的通道 分散体，预定量的溶液，乳液和/或分散体被引入每个通道以获得预定的组合物和a）如果在存在或不存在惰性气体或反应气体的情况下适当地加热涂覆体到达该范围内的温度 20至1500℃，用或不用烧结或煅烧来干燥催化剂和/或催化剂前体。

    Combinatorial preparation and testing of heterogeneous catalysts
    7.
    发明申请
    Combinatorial preparation and testing of heterogeneous catalysts 审中-公开
    组合制备和非均相催化剂的试验

    公开(公告)号：US20050037426A1

    公开(公告)日：2005-02-17

    申请号：US10726185

    申请日：2003-12-03

    申请人： Stephan Schunk ,  Dirk Demuth ,  Hartmut Hibst

    发明人： Stephan Schunk ,  Dirk Demuth ,  Hartmut Hibst

    IPC分类号： B01J19/00 ,  B01J35/04 ,  B01J37/02 ,  C40B30/08 ,  C40B40/18 ,  G01N33/53 ,  G01N33/543

    CPC分类号： B01J37/02 ,  B01J19/0046 ,  B01J35/04 ,  B01J2219/0052 ,  B01J2219/00585 ,  B01J2219/00603 ,  B01J2219/00659 ,  B01J2219/00704 ,  B01J2219/00745 ,  B01J2219/00747 ,  C40B30/08 ,  C40B40/18 ,  Y10T436/175383 ,  Y10T436/18 ,  Y10T436/20 ,  Y10T436/205831 ,  Y10T436/25875

    摘要： A process for preparing arrays of heterogeneous catalysts and/or their precursors, made up of a body which has, preferably parallel, through-channels and in which at least n channels comprise n different heterogeneous catalysts and/or their precursors, where n is 2, preferably 10, particularly preferably 100, comprises the following steps: a1) preparing solutions, emulsions and/or dispersions of elements and/or element compounds of the chemical elements present in the catalyst and/or catalyst precursor and, if appropriate preparing dispersions of inorganic support materials, a2) if appropriate introducing adhesion promoters, binders, viscosity regulators, pH regulators and/or solid inorganic supports into the solutions, emulsions and/or dispersions, a3) simultaneously or successively coating the channels of the body with the solutions, emulsions and/or dispersions, a predetermined amount of the solutions, emulsions and/or dispersions being introduced into each channel to obtain a predetermined composition, a4) treating and reacting with one or more reactive gases the freshly impregnated moist channels obtained after the coating, and a5) if appropriate heating the coated body in the presence or absence of inert gases or reactive gases to a temperature in the range from 20 to 1500° C. to dry, with or without sintering or calcining, the catalysts and/or catalyst precursors.

    摘要翻译： 一种制备非均相催化剂和/或其前体阵列的方法，其由具有优选平行通过通道并且其中至少n个通道包含n个不同的非均相催化剂和/或其前体的主体组成，其中n为2 ，优选10，特别优选100，包括以下步骤：a1）制备催化剂和/或催化剂前体中存在的化学元素的元素和/或元素化合物的溶液，乳液和/或分散体，并且如果合适，制备 无机载体材料，a2）如果合适的话，将粘合促进剂，粘合剂，粘度调节剂，pH调节剂和/或固体无机载体引入溶液，乳液和/或分散体中，a3）用溶液同时或连续地涂覆身体的通道， 乳液和/或分散体，将预定量的溶液，乳液和/或分散体引入每个通道以获得预 a4）在涂覆后获得的新鲜浸渍的湿通道处理和反应一种或多种反应性气体，以及a）如果在存在或不存在惰性气体或反应性气体的情况下适当地加热涂覆体到达该范围内的温度 20至1500℃，用或不用烧结或煅烧来干燥催化剂和/或催化剂前体。

    Device and process for the simultaneous agitation of reaction mixtures
    10.
    发明申请
    Device and process for the simultaneous agitation of reaction mixtures 审中-公开
    用于同时搅拌反应混合物的装置和方法

    公开(公告)号：US20060182667A1

    公开(公告)日：2006-08-17

    申请号：US10543074

    申请日：2004-02-06

    申请人： Torsten Zech ,  Stephan Schunk ,  Alfred Haas

    发明人： Torsten Zech ,  Stephan Schunk ,  Alfred Haas

    IPC分类号： B01J19/00

    CPC分类号： C10G2/32 ,  B01F13/0255 ,  B01J19/0046 ,  B01J2219/00283 ,  B01J2219/00286 ,  B01J2219/00333 ,  B01J2219/0036 ,  B01J2219/00389 ,  B01J2219/00418 ,  B01J2219/00423 ,  B01J2219/00481 ,  B01J2219/00484 ,  B01J2219/00493 ,  B01J2219/00495 ,  B01J2219/00585 ,  B01J2219/00596 ,  B01J2219/00599 ,  B01J2219/00689 ,  B01J2219/00707 ,  B01J2219/0072 ,  B01J2219/00738 ,  B01J2219/00745 ,  B01J2219/00747 ,  C10G2/34 ,  C40B30/08 ,  C40B40/18 ,  C40B50/08 ,  C40B60/14

    摘要： The present invention is in the field of the high-throughput research for liquid and multi-phase reactions. Thereby, the invention relates to a process for the simultaneous realization of at least one chemical reaction in at least two separate reaction vessels (10), wherein said process comprises at least the following steps: (i) providing at least one reaction mixture per reaction vessel (10); to (ii) pneumatic agitation of the reaction mixture in at least one reaction vessel by means of bringing the reaction mixture into contact with at least one fluid phase (18), wherein the at least one chemical reaction is carried out in at least one of the reaction vessels (10) in the batch mode and the reaction mixture contains at least one liquid phase (14). Thereby, the fluid phase (18) is supplied to the at least one reaction vessel (10) within a defined period and is at least partially discharged from the reaction vessel. The reaction mixturee may further comprise another immiscible liquid phase (14′) and/or solid phase (16). Furthermore, the present invention relates to the device, which pertains to the process.

    摘要翻译： 本发明在液相和多相反应的高通量研究领域。 因此，本发明涉及在至少两个分离的反应容器（10）中同时实现至少一种化学反应的方法，其中所述方法至少包括以下步骤：（i）每次反应提供至少一种反应混合物 容器（10）; （ii）通过使反应混合物与至少一个流化相（18）接触，在至少一个反应容器中气动搅拌反应混合物，其中至少一个化学反应在 分批模式的反应容器（10）和反应混合物含有至少一个液相（14）。 因此，流体相（18）在规定的时间内被供给到至少一个反应容器（10），并且至少部分地从反应容器排出。 反应混合物还可以包含另一个不混溶的液相（14'）和/或固相（16）。 此外，本发明涉及与该方法有关的装置。