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1.发明授权
公开(公告)号：US4795581A
公开(公告)日：1989-01-03
申请号：US36650
申请日：1987-04-10
IPC分类号： B01F17/00 , C10M173/02
CPC分类号： B01F17/0042 , C10M173/02 , C10M2201/02 , C10M2207/022 , C10M2215/042 , C10N2240/08 , C10N2250/02
摘要： Aqueous fluids are thickened with fatty acid modified polyoxyalkylene diamines. The polyoxyalkylene diamines are of the formula:H.sub.2 NCH(CH.sub.3)CH.sub.2 O(CH.sub.2 CH(R)O).sub.x CH.sub.2 CH(CH.sub.3)NH.sub.2wherein:R is methyl or hydrogen andx is a number selected to give the diamine a molecular weight of 3000 to 9000.The fatty acid is a hydrophobic mono- or dicarboxylaic acid of 12 to 36 carbon atoms. The ratio of amine equivalent: acid ranges from 1:0.5 to 1:1.The aqueous fluids optionally incorporate ethylene glycol. They are useful for water/glycol based hydraulic fluids, cosmetics and surfactants.
摘要翻译： 水性流体用脂肪酸改性聚氧化烯二胺增稠。 聚氧化烯二胺具有下式：H 2 NCH（CH 3）CH 2 O（CH 2 CH（R）O）x CH 2 CH（CH 3）NH 2其中：R是甲基或氢，x是选定的数字，得到二胺的分子量为3000-9000。 脂肪酸是12至36个碳原子的疏水单羧酸或二羧酸。 胺当量：酸的比例为1:0.5至1:1。 含水流体任选地加入乙二醇。 它们可用于水/乙二醇型液压油，化妆品和表面活性剂。
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2.发明授权Bis(2,2',6,6'-tetramethyl-4-aminoethyleneamidopiperidyl) polyoxyalkylene 失效聚（2,2'，6,6'-四甲基-4-氨基亚乙基氨基哌啶基）聚氧化烯
公开(公告)号：US5210195A
公开(公告)日：1993-05-11
申请号：US789500
申请日：1991-11-08
申请人： Jiang-Jen Lin , George P. Speranza
发明人： Jiang-Jen Lin , George P. Speranza
IPC分类号： C07D211/58 , C08G65/332 , C08G65/333 , C08K5/3435
CPC分类号： C08K5/3435 , C07D211/58 , C08G65/3322 , C08G65/33317
摘要： Polyoxyalkylene diamines react with excess acrylate to form diesters which react with 2,2',6,6'-tetramethyl-4-aminopiperidines to give a product of formula 1, useful as photostabilizer for photosensitive materials. ##STR1##
摘要翻译： 聚氧化烯二胺与过量的丙烯酸酯反应形成二酯，其与2,2'，6,6'-四甲基-4-氨基哌啶反应，得到式1的产物，其用作感光材料的光稳定剂。 公式1
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公开(公告)号：US5128441A
公开(公告)日：1992-07-07
申请号：US519080
申请日：1990-05-04
申请人： George P. Speranza , Jiang-Jen Lin
发明人： George P. Speranza , Jiang-Jen Lin
摘要： A block polyamido primary amine condensation product prepared by reacting a defined polyoxyalkylene polyamine having terminal primary amine groups with an amount of a defined dicarboxylic acid or an anhydride or a C.sub.1 to C.sub.4 alkyl ester thereof, sufficient to react one mole of the dicarboxylic acid reactant with each primary amine group of the polyoxyalkylene polyamine to thereby prepare an intermediate condensation reaction product containing terminal carboxyl groups, and reacting one mole of a defined organic di-primary amine with each terminal carboxyl group of the said intermediate condensation reaction product to thereby provide, as the principal product of the reaction a block polyamido primary amine condensation product.
摘要翻译： 通过使具有末端伯胺基的规定的聚氧化烯多胺与一定量的二羧酸或其酸酐或其C1-C4烷基酯反应制备的嵌段聚酰氨基伯胺缩合产物，其足以使一摩尔二羧酸反应物与 从而制备含有末端羧基的中间缩合反应产物，并使一摩尔限定的有机二伯胺与所述中间缩合反应产物的每个末端羧基反应，从而提供作为 反应的主要产物是嵌段聚酰胺伯胺缩合产物。
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公开(公告)号：US5120817A
公开(公告)日：1992-06-09
申请号：US661142
申请日：1991-02-27
IPC分类号： C08G14/06 , C08G14/073 , C08G14/14 , C08G59/00 , C08G59/40 , C08G59/50 , C08G59/62 , C08L63/00
摘要： An epoxy resin composition comprises an vicinal polyepoxide and a Mannich condensation reaction product curing agent. The curing agent is the Mannich condensation reaction product of a phenol, formaldehyde and a polyoxyethylenediamine of the formula:NH.sub.2 (CH.sub.2 CH.sub.2 O).sub.x --CH.sub.2 CH.sub.2 NH.sub.2,and wherein: x ranges from 1 to 3. These epoxy resin compositions are useful in coatings, adhesives, encapsulations and composite matrices.
摘要翻译： 环氧树脂组合物包含邻位聚环氧化物和曼尼希缩合反应产物固化剂。 固化剂是苯酚，甲醛和下列通式为：NH 2（CH 2 CH 2 O）x -CH 2 CH 2 NH 2的聚氧乙烯二胺的曼尼希缩合反应产物，其中：x为1至3.这些环氧树脂组合物可用于涂料，粘合剂， 封装和复合矩阵。
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公开(公告)号：US5101060A
公开(公告)日：1992-03-31
申请号：US615104
申请日：1990-11-19
申请人： George P. Speranza , Jiang-Jen Lin
发明人： George P. Speranza , Jiang-Jen Lin
IPC分类号： C07C217/08 , C07C255/24
CPC分类号： C07C217/08 , C07C255/24
摘要： Normally liquid final Mannich condensates prepared by reacting a para C.sub.1 -C.sub.15 alkyl phenol with formaldehyde and a first polyoxyalkylene diamine to form an intermediate Mannich condensate that is reacted with formaldehyde and a second polyoxyalkylene diamine to form a final Mannich condensate, the first and second polyoxyalkylene diamines having the formula: ##STR1## wherein R represents hydrogen or methyl and R' represents an alkyl group containing 1 to 4 carbon atoms or cyanoethyl group, and n represents positive numbers having a value of 1 to about 6, the final Mannich condensate having the formula: ##STR2## wherein X and Y are polyoxyalkylene amine groups derived from the first and second polyoxyalkylene diamines and formaldehyde.
摘要翻译： 通常将对位C 1 -C 15烷基苯酚与甲醛和第一聚氧化烯二胺反应制备的通常为液体的最终曼尼希缩合物，以形成与甲醛和第二聚氧化烯二胺反应形成最终曼尼希缩合物的中间曼尼希缩合物，第一和第二聚氧化烯 具有下式的二胺：其中R表示氢或甲基，R'表示含有1至4个碳原子的烷基或氰乙基，n表示1至6的正数，最终 具有下式的曼尼希缩合物：其中X和Y是衍生自第一和第二聚氧化烯二胺和甲醛的聚氧化烯胺基团。
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6.发明授权Isocyanate prepolymers and secondary amines from disecondary amines and alkyl diisocyanates 失效异氰酸酯丙烯酸酯和二异丙基胺与二异丙基氨基甲酸酯
公开(公告)号：US5084202A
公开(公告)日：1992-01-28
申请号：US377355
申请日：1989-07-10
申请人： Jiang-Jen Lin , George P. Speranza
发明人： Jiang-Jen Lin , George P. Speranza
IPC分类号： C07C273/02 , C07C273/18 , C07C275/18 , C07C275/26 , C07C275/28 , C08G18/32 , C08G18/50 , C08G18/80
CPC分类号： C07C273/1827 , C08G18/3228 , C08G18/5024 , C08G18/8038
摘要： Disclosed are novel isocyanate prepolymers and novel secondary amines, both prepared from alkyl diisocyanates and secondary isopropyl derivatives of polyoxyalkylene diamines. The molar ratios, reaction procedures (i.e. inverse addition of reactants) and solvent determine the products. Most of the products are light colored and nongelled.The isocyanate prepolymers are useful in the field of polyurethanes and the novel secondary amines are useful in epoxy coatings applications.
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公开(公告)号：US4940770A
公开(公告)日：1990-07-10
申请号：US270897
申请日：1988-11-14
申请人： George P. Speranza , Jiang-Jen Lin
发明人： George P. Speranza , Jiang-Jen Lin
CPC分类号： C08G59/184 , C08L63/00
摘要： Disclosed are novel compositions useful in mixed epoxy material synthesis, poly(epoxy)-(urea) synthesis and cases where epoxy curing agents require flexibility which are essentially the reaction products of polyoxyalkylene polyamines and epoxides. Specifically the amine reactants comprise polyoxypropylene triamines, amine terminated alkylene glycols and polyoxypropylene diols, such as those represented by Texaco Chemical Company's JEFFAMINE.RTM. T-series, JEFFAMINE.RTM. EDR series and JEFFAMINE.RTM. D-series amines, respectively. The epoxide component prepolymers essentially comprise Bisphenol A diglycidyl ethers. The ratio of JEFFAMINE.RTM. amine to epoxide and the use of acetone are essential to prepare non-gelled products.
摘要翻译： 公开了可用于混合环氧材料合成，聚（环氧） - （尿素）合成和环氧固化剂需要柔性的情况的新型组合物，其基本上是聚氧化烯多胺和环氧化物的反应产物。 具体地，胺反应物分别包括聚氧丙烯三胺，胺封端的亚烷基二醇和聚氧丙烯二醇，例如由Texaco Chemical Company的JEFFAMINE TM T系列，JEFFAMINE TM EDR系列和JEFFAMINE TM D系列胺代表的那些。 环氧化物组分预聚物基本上包含双酚A二缩水甘油醚。 JEFFAMINE TM胺与环氧化物的比例和使用丙酮对于制备非凝胶产品是至关重要的。
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8.发明授权Liquid cleaning compositions containing polyether amide surfactants as thickening agents 失效含有聚醚酰胺表面活性剂作为增稠剂的液体清洗组合物
公开(公告)号：US4828757A
公开(公告)日：1989-05-09
申请号：US168024
申请日：1988-03-14
IPC分类号： C08G65/332 , C11D1/52 , C11D3/37 , C11D17/00
CPC分类号： C11D1/528 , C08G65/3322 , C11D17/003 , C11D3/3707
摘要： A method of thickening an aqueous solution containing from 5 to 50 wt% of a surfactant is disclosed comprising the addition of from about 0.1 to 10 wt% to the solution of a polyether amide derivative having the general formula: ##STR1## wherein R=C.sub.9 -C.sub.23 and a=1 to about 5 and b=1 to 500.
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公开(公告)号：US5248821A
公开(公告)日：1993-09-28
申请号：US846986
申请日：1992-03-09
申请人： Jiang-Jen Lin , George P. Speranza
发明人： Jiang-Jen Lin , George P. Speranza
IPC分类号： C07C273/18 , C07C275/26 , C08G18/10 , C08G18/50
CPC分类号： C08G18/5024 , C07C273/1827 , C08G18/10
摘要： High molecular weight active polyoxyalkylene reaction product formed in two steps and containing urea or urethane and urea linkages are disclosed which contain as the principle reaction component, a diamine having the formula: ##STR1## or a diol having the formula: ##STR2## wherein R' independently represents hydrogen or methyl and x is a number having an average value of at least 1 to about 70 and a diisocyanate of the formula: ##STR3## an active amine selected from the group consisting of amine terminated triethylene glycol, amine terminated tetraethylene glycol, isophorone diamine, dipropylene triamine, or diethylene triamine.
摘要翻译： 公开了分两步形成并含有尿素或氨基甲酸酯和尿素键的高分子量活性聚氧化烯反应产物，其包含作为主要反应组分的具有下式的二胺或具有下式的二醇：其中R '独立地表示氢或甲基，x是平均值至少为1至约70的数，并且具有下式的二异氰酸酯：选自胺封端的三亚乙基 二醇，胺封端的四甘醇，异佛尔酮二胺，二丙烯三胺或二亚乙基三胺。
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公开(公告)号：US5239048A
公开(公告)日：1993-08-24
申请号：US519078
申请日：1990-05-04
申请人： George P. Speranza , Jiang-Jen Lin
发明人： George P. Speranza , Jiang-Jen Lin
IPC分类号： C07C233/69
CPC分类号： C07C233/69 , C07C2102/08
摘要： Block polyamido polyamine condensation products of an aromatic polycarboxylic acid component with a polyoxyalkylene polyamine component prepared by reacting the polycarboxylic acid component with an amount of the polyoxyalkylene polyamine component sufficient to react each carboxyl group with 1 mole of the polyoxyalkylene polyamine component.The polyoxyalkylene polyamine being selected from the group consisting of polyoxypropylene diamines, polyoxyethylene diamines, polyoxyethylene/oxypropylene diamines and polyoxypropylene triamines, and the aromatic polycarboxylic acid component being selected from the group consisting of C.sub.8 to C.sub.28 benzene dicarboxylic acids, benzene tricarboxylic acids, naphthalene carboxylates, hemimellitic acid, 1,1,3-trimethyl-3-phenylindan-4',5-dicarboxylic acid, trimellitic acid, and anhydrides and C.sub.1 to C.sub.4 alkyl esters thereof.
摘要翻译： 通过使多元羧酸组分与足以使每个羧基与1摩尔聚氧化烯多胺组分反应的聚氧化烯多胺组分反应制备的芳族多元羧酸组分的聚酰胺多胺缩合产物与聚氧化烯多胺组分。 聚氧亚烷基多胺选自聚氧丙烯二胺，聚氧乙烯二胺，聚氧乙烯/氧丙烯二胺和聚氧丙烯三胺，芳香族多元羧酸成分选自C8〜C28苯二羧酸，苯三羧酸，萘羧酸 ，偏苯三酸，1,1,3-三甲基-3-苯基茚满-4'，5-二羧酸，偏苯三酸和酸酐及其C1-C4烷基酯。
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