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公开(公告)号：US20110206532A1
公开(公告)日：2011-08-25
申请号：US12710691
申请日：2010-02-23
申请人： Francesco Sorbo , Lawrence Bernard Kool , William Clarke Brooks , Massimo Giannozzi , Eugenio Giorni , Thomas Lancsek , Steven Alfred Tysoe , Dennis Michael Gray , Todd Charles Curtis
发明人： Francesco Sorbo , Lawrence Bernard Kool , William Clarke Brooks , Massimo Giannozzi , Eugenio Giorni , Thomas Lancsek , Steven Alfred Tysoe , Dennis Michael Gray , Todd Charles Curtis
CPC分类号： C23C18/32 , Y10T428/12944 , Y10T428/31678
摘要： The present invention provides a method for preparing an electroless nickel coating composition that includes (a) coating a substrate with an electroless nickel coating to provide a coated substrate; and (b) subjecting the coated substrate to a heating protocol comprising heating to a temperature in a range from about 550° C. to about 700° C. for a period of from about 7 to about 30 hours. An article made from the method is also provided.
摘要翻译： 本发明提供一种制备无电镍涂料组合物的方法，其包括（a）用无电镀镍涂层涂覆基材以提供涂覆的基材; 和（b）使涂覆的基材经受加热方案，包括加热至约550℃至约700℃的温度约7至约30小时。 还提供了从该方法制成的文章。
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公开(公告)号：US20090302005A1
公开(公告)日：2009-12-10
申请号：US12132805
申请日：2008-06-04
申请人： Lawrence Bernard Kool , Michael David Feldstein , Eugenio Giorni , Dennis Michael Gray , Thomas Stephen Lancsek , Francesco Sorbo , Steven Alfred Tysoe
发明人： Lawrence Bernard Kool , Michael David Feldstein , Eugenio Giorni , Dennis Michael Gray , Thomas Stephen Lancsek , Francesco Sorbo , Steven Alfred Tysoe
CPC分类号： C23F1/26 , C23C18/1834 , C23C18/1844 , C23C18/32 , C23F1/28 , F01D5/005 , F01D5/288 , F05D2230/80
摘要： Process for roughening a surface of a base metal substrate includes contacting the surface with an aqueous solution comprising oxalic acid, sulfuric acid, and hydrogen peroxide at a temperature and for a period of time effective to roughen the surface to an average roughness greater than 60 Ra, removing a modest amount of base material, and generating no narrow and deep crevices at all. The surface is roughened prior to application of an electroless coating onto the substrate.
摘要翻译： 用于使基底金属基材的表面粗糙化的方法包括使表面与包含草酸，硫酸和过氧化氢的水溶液在有效使表面粗糙至大于60Ra的平均粗糙度的温度和时间 ，去除适量的基材，并且根本不产生狭窄和深的裂缝。 在将无电涂层施加到基底之前，将表面粗糙化。
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3.发明申请公开(公告)号：US20090286104A1
公开(公告)日：2009-11-19
申请号：US12122060
申请日：2008-05-16
申请人： Steven Alfred Tysoe , Eugenio Giorni , Dennis Michael Gray , Lawrence Bernard Kool , Francesco Sorbo
发明人： Steven Alfred Tysoe , Eugenio Giorni , Dennis Michael Gray , Lawrence Bernard Kool , Francesco Sorbo
CPC分类号： C23C18/1834 , C23C18/1651 , C23C18/1692 , C23C18/36 , Y10T428/12625 , Y10T428/12937
摘要： Multiple layers of nickel phosphorous coatings are formed by electroless plating onto a base metal substrate such as a turbine component. In one embodiment, a first nickel layer metallurgical bonded by a heat treatment process to a surface of the base metal substrate, the first nickel layer containing about 4 to about 6 weight percent phosphorous with the balance being essentially nickel; and a second nickel layer deposited onto the first layer, the second nickel layer containing about 8 to about 12 weight percent phosphorous with the balance being essentially nickel, wherein the first and second layers are formed by electroless plating. In this manner, adhesion is maximized without degrading the properties of the second layer such as corrosion resistance and ductility. Also disclosed are processes for forming the multilayered nickel phosphorus coatings.
摘要翻译： 多层镍磷涂层通过无电电镀形成在诸如涡轮机部件的基底金属基底上。 在一个实施方案中，通过热处理工艺冶金地结合到贱金属基底的表面的第一镍层，所述第一镍层含有约4至约6重量％的磷，余量基本上为镍; 和沉积到第一层上的第二镍层，第二镍层含有约8至约12重量％的磷，余量基本上为镍，其中第一和第二层通过无电镀形成。 以这种方式，最大限度地发挥粘附性，而不降低第二层的性能，例如耐腐蚀性和延展性。 还公开了形成多层镍磷涂层的方法。
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公开(公告)号：US20110027576A1
公开(公告)日：2011-02-03
申请号：US12510677
申请日：2009-07-28
申请人： Lawrence Bernard Kool , Eugenio Giorni , Dennis Michael Gray , Francesco Sorbo , Steven Alfred Tysoe
发明人： Lawrence Bernard Kool , Eugenio Giorni , Dennis Michael Gray , Francesco Sorbo , Steven Alfred Tysoe
CPC分类号： C23C18/1601 , C23C18/1689 , C23C18/36 , Y10T428/249994
摘要： The present invention provides a method for sealing pinholes in an electroless metal coating, said method comprising: (a) coating a substrate with an electroless metal coating layer to provide a coated article comprising an electroless metal coating in contact with the surface of the substrate, said electroless metal coating being characterized by the presence of pinhole imperfections which allow fluid communication between the substrate and the environment; (b) applying a layer of a curable epoxy sealant over the electroless metal coating layer and filling the pinhole imperfections; (c) curing the curable epoxy sealant to provide a cured epoxy overcoating layer; and (d) removing a substantial portion of the cured epoxy overcoating layer to provide an article comprising an electroless metal coating which is substantially free of pinhole imperfections allowing fluid communication between the substrate and the environment.
摘要翻译： 本发明提供了一种密封无电金属涂层中的针孔的方法，所述方法包括：（a）用无电金属涂层涂覆基底，以提供包括与基底表面接触的无电金属涂层的涂覆制品， 所述无电金属涂层的特征在于存在允许衬底和环境之间的流体连通的针孔缺陷; （b）在无电金属涂层上涂一层可固化环氧密封胶并填充针孔缺陷; （c）固化可固化环氧密封剂以提供固化的环氧树脂涂层; 和（d）去除大部分固化的环氧树脂外涂层以提供包含无电金属涂层的制品，其基本上没有针孔缺陷，从而允许衬底和环境之间的流体连通。
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公开(公告)号：US20130143031A1
公开(公告)日：2013-06-06
申请号：US13512813
申请日：2010-11-24
CPC分类号： B05D5/00 , B32B5/16 , C23C18/1662 , C23C18/34 , Y10T428/25
摘要： Methods for coating a substrate with wear resistant particles by electroless nickel (Ni) plating. A method includes immersing the substrate in a bath provided in a cell, the bath having a Ni salt; adding cubic Boron Nitride (cBN) particles having a predetermined size to the bath so as to produce a predetermined concentration of cBN; maintaining the substrate in the bath with the cBN particles for a predetermined time; and removing the substrate, wherein the removed substrate has a coating of cBN and Ni in a first range.
摘要翻译： 通过无电镀镍（Ni）电镀涂覆耐磨颗粒的基材的方法。 一种方法包括将基底浸入设置在电池中的浴中，该浴具有Ni盐; 向所述浴中加入具有预定尺寸的立方氮化硼（cBN）颗粒以产生预定浓度的cBN; 用cBN颗粒将衬底保持在浴中预定的时间; 并且去除所述基板，其中所述移除的基板在第一范围内具有cBN和Ni的涂层。
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