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    Semi continuous operational method for producing copolymers
    1.
    发明授权
    Semi continuous operational method for producing copolymers 有权
    用于生产共聚物的半连续操作方法

    公开(公告)号：US08541518B2

    公开(公告)日：2013-09-24

    申请号：US12920143

    申请日：2009-02-10

    申请人： Gerhard Albrecht ,  Klaus Lorenz ,  Christian Scholz ,  Petra Wagner

    发明人： Gerhard Albrecht ,  Klaus Lorenz ,  Christian Scholz ,  Petra Wagner

    IPC分类号： C08F2/04 ,  C08F224/00 ,  C08F2/10 ,  C04B28/28

    CPC分类号： C08F220/04 ,  C08F220/26

    摘要： A process for the preparation of a copolymer in a semicontinuous mode of operation in a polymerization apparatus containing a polymerization reactor connected to a metering device, in each case acid monomer being initially introduced into the metering device and polyether macromonomer and water into the polymerization reactor, acid monomer being metered from the metering device into the polymerization reactor, the metering of the acid monomer into the polymerization reactor being effected in such a way that first a polymerization pH is established in the aqueous medium and then, until the conversion of 70 mol % of the polyether macromonomer initially introduced into the polymerization reactor, acid monomer is passed into the polymerization reactor in an amount per unit time such that the pH in the aqueous medium deviates by not more than ±0.3 from the initially established polymerization pH.

    摘要翻译： 在含有连接到计量装置的聚合反应器的聚合装置中制备半连续操作模式的共聚物的方法，每种情况下，酸性单体最初引入计量装置和聚醚大分子单体和水进入聚合反应器， 酸性单体从计量装置计量到聚合反应器中，酸性单体计量到聚合反应器中的方式是首先在水性介质中建立聚合pH，然后直到70mol％ 的最初引入聚合反应器的聚醚大分子单体，酸单体以每单位时间的量进入聚合反应器，使得水介质中的pH从最初建立的聚合pH偏离不大于±0.3。

    Copolymers Based On Unsaturated Monocarboxylic or Dicarboxylic Acid Derivatives and Oxyalkylene Glycol Alkenyl Ethers, Process for Preparing Them and Their Use
    3.
    发明申请
    Copolymers Based On Unsaturated Monocarboxylic or Dicarboxylic Acid Derivatives and Oxyalkylene Glycol Alkenyl Ethers, Process for Preparing Them and Their Use 审中-公开
    基于不饱和单羧酸或二羧酸衍生物和氧亚烷基二醇乙烯基醚的共聚物，其制备方法及其应用

    公开(公告)号：US20090163622A1

    公开(公告)日：2009-06-25

    申请号：US12084665

    申请日：2006-12-20

    申请人： Gerhard Albrecht ,  Klaus Lorenz ,  Christian Scholz ,  Petra Wagner

    发明人： Gerhard Albrecht ,  Klaus Lorenz ,  Christian Scholz ,  Petra Wagner

    IPC分类号： C08F220/00 ,  C08F222/04 ,  C08F216/12 ,  C08K3/00 ,  C08K3/30

    CPC分类号： C04B24/2605 ,  C04B24/2647 ,  C04B24/267 ,  C04B24/2694 ,  C04B2103/30 ,  C04B2103/408 ,  C08F216/1416 ,  C08F220/06 ,  C08F222/06

    摘要： Copolymers based on unsaturated mono- or dicarboxylic acid derivatives, oxyalkylene glycol alkenyl ethers and optionally vinylic polyalkylene glycol or ester compounds are described and also their use as additives for aqueous suspensions based on mineral or bituminous binders, in particular cement, gypsum, lime, anhydrite, or other calcium sulphate-based binders, and based on pulverulent dispersion binders. The copolymers according to the invention impart to the aqueous binder suspensions a very good dispersing and liquefying action with, at the same time, simultaneous excellent processing properties. Moreover, the oxyalkylene glycol alkenyl ethers according to the invention are industrially relatively simple and inexpensive to prepare and need comparatively low initiator concentrations in the copolymerization.

    摘要翻译： 描述了基于不饱和单羧酸或二羧酸衍生物，氧亚烷基二醇烯基醚和任选的乙烯基聚亚烷基二醇或酯化合物的共聚物，也用作基于矿物或沥青粘合剂，特别是水泥，石膏，石灰，无水石膏 ，或其它基于硫酸钙的粘合剂，并且基于粉末分散粘合剂。 根据本发明的共聚物赋予水性粘合剂悬浮液非常好的分散和液化作用，同时具有同时优异的加工性能。 此外，根据本发明的氧亚烷基二醇烯基醚在工业上相对简单且制备成本低，并且在共聚中需要相对较低的引发剂浓度。

    Dispersing agent containing copolymer mixture
    4.
    发明授权
    Dispersing agent containing copolymer mixture 有权
    分散剂含共聚物混合物

    公开(公告)号：US08907016B2

    公开(公告)日：2014-12-09

    申请号：US13133022

    申请日：2009-11-25

    申请人： Mario Vierle ,  Klaus Lorenz ,  Gerhard Albrecht ,  Christian Scholz ,  Petra Wagner ,  Barbara Wimmer

    发明人： Mario Vierle ,  Klaus Lorenz ,  Gerhard Albrecht ,  Christian Scholz ,  Petra Wagner ,  Barbara Wimmer

    IPC分类号： C04B24/26 ,  C08L29/10 ,  C08L33/02 ,  C08L35/08 ,  C04B103/40

    CPC分类号： C04B24/2694 ,  C04B24/2647 ,  C04B2103/408 ,  C08L29/10 ,  C08L33/02 ,  C08L35/08 ,  C08L2205/02 ,  C08L2666/04

    摘要： The invention relates to a polymer composition containing 5 to 95% by weight of a copolymer H and 2 to 60% by weight of a copolymer K, the copolymers H and K each having polyether macromonomer structural units and acid monomer structural units, which are present in the copolymers H and K in each case in a molar ratio of 1:20 to 1:1, and at least 20 mol % of all structural units of the copolymer H and at least 25 mol % of all structural units of the copolymer K being present in each case in the form of acid monomer structural units, the polyether macromonomer structural units of the copolymer H having side chains containing in each case at least 5 ether oxygen atoms, the number of ether oxygen atoms per side chain of the polyether macromonomer structural units of the copolymer H varying in such a way that the corresponding frequency distribution diagram, in which the number of ether oxygen atoms per side chain of a polyether macromonomer structural unit is plotted along the abscissa and the associated frequency for the copolymer H is plotted along the ordinate, contains at least 2 maxima.

    摘要翻译： 本发明涉及一种聚合物组合物，其含有5〜95重量％的共聚物H和2〜60重量％的共聚物K，共聚物H和K各自具有聚醚大分子单体结构单元和酸单体结构单元，其存在 在共聚物H和K中的摩尔比为1:20至1:1的共聚物中，和共聚物H的所有结构单元的至少20摩尔％和共聚物K的所有结构单元的至少25摩尔％ 在各种情况下以酸性单体结构单元的形式存在，共聚物H的聚醚大分子单体结构单元具有侧链含有至少5个醚氧原子，每个侧链上的醚氧原子的数量为聚醚大分子单体 共聚物H的结构单元以这样的方式变化，其中相应的频率分布图，其中聚醚大分子单体结构单元的每个侧链的醚氧原子的数量沿着横坐标绘制， 共聚物H的相关频率沿纵坐标绘制，含有至少2个最大值。

    Dispersant comprising copolymer mixture
    5.
    发明授权
    Dispersant comprising copolymer mixture 有权
    分散剂包括共聚物混合物

    公开(公告)号：US08772377B2

    公开(公告)日：2014-07-08

    申请号：US13133043

    申请日：2009-11-25

    申请人： Klaus Lorenz ,  Mario Vierle ,  Gerhard Albrecht ,  Barbara Wimmer ,  Petra Wagner ,  Christian Scholz

    发明人： Klaus Lorenz ,  Mario Vierle ,  Gerhard Albrecht ,  Barbara Wimmer ,  Petra Wagner ,  Christian Scholz

    IPC分类号： C04B28/02 ,  C08J3/02 ,  C08L39/04 ,  C08L33/14 ,  C04B24/26 ,  C08L33/26 ,  C08L43/02 ,  C04B40/00 ,  C04B28/00 ,  C08J3/00 ,  C08L39/00 ,  C08L33/00 ,  C04B103/40 ,  C04B103/32

    CPC分类号： C04B24/2647 ,  C04B24/2658 ,  C04B24/267 ,  C04B40/0039 ,  C04B2103/32 ,  C04B2103/408 ,  C08G65/2609 ,  C08L29/10 ,  C08L33/02 ,  C08L33/066 ,  C08L33/14 ,  C08L33/26 ,  C08L35/08 ,  C08L43/02 ,  C08L71/02 ,  C08L2205/02 ,  C08L2666/04 ,  C08L2666/22

    摘要： The invention relates to a polymer composition containing 3 to 95% by weight of a copolymer H and 3 to 95% by weight of a copolymer K, the copolymers H and K each having polyether macromonomer structural units and acid monomer structural units, which are present in the copolymers H and K in each case in a molar ratio of 1:20 to 1:1, and at least 20 mol % of all structural units of the copolymer H and at least 25 mol % of all structural units of the copolymer K being present in each case in the form of acid monomer structural units, the polyether macromonomer structural units of the copolymers H and K having side chains containing in each case at least 5 ether oxygen atoms, the number of ether oxygen atoms per side chain of the polyether macromonomer structural units of the copolymers H and K varying in each case in such a way that the corresponding frequency distribution diagrams, in which the number of ether oxygen atoms per side chain of a polyether macromonomer structural unit is plotted in each case along the abscissae and the respectively associated frequencies for the copolymers H or K are plotted in each case along the ordinates, contain in each case at least 2 maxima whose abscissa values differ in each case by more than 7 ether oxygen atoms from one another, the frequency distribution diagrams of the copolymers H and K differing from one another in that the abscissa value of at least one maximum of the copolymer H differs in each case by more than 5 ether oxygen atoms from the abscissa values of all maxima of the copolymer K and/or that the arithmetic means of the ether oxygen atoms of the polyether macromonomer structural units of the copolymers H and K differ from one another by more than 5 ether oxygen atoms.

    摘要翻译： 本发明涉及含有3〜95重量％共聚物H和3〜95重量％共聚物K的聚合物组合物，共聚物H和K各自具有聚醚大分子单体结构单元和酸单体结构单元，其存在 在共聚物H和K中的摩尔比为1:20至1:1的共聚物中，和共聚物H的所有结构单元的至少20摩尔％和共聚物K的所有结构单元的至少25摩尔％ 在各种情况下以酸单体结构单元的形式存在，共聚物H和K的聚醚大分子单体结构单元具有侧链，每种情况下含有至少5个醚氧原子，每个侧链的醚氧原子数 共聚物H和K的聚醚大分子单体结构单元在每种情况下变化，使得相应的频率分布图，其中聚醚大分子单体结构单元每侧链的醚氧原子数为pl 在每个情况下沿着横坐标分别表示，并且在每种情况下沿着纵坐标绘制共聚物H或K的分别相关联的频率，每种情况下包含至少2个最大值，其横坐标值在每种情况下不同于7个以上的醚氧原子 另一方面，共聚物H和K的频率分布图彼此不同，因为共聚物H的至少一个最大值的横坐标值在每种情况下都不同于5个以上的醚氧原子，从所有最大值的横坐标值 共聚物K和/或共聚物H和K的聚醚大分子单体结构单元的醚氧原子的算术手段彼此间隔超过5个醚氧原子。