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    Antifoaming agent and/or deaerators for aqueous media tending to foam
    1.
    发明申请
    Antifoaming agent and/or deaerators for aqueous media tending to foam 有权
    用于水性介质的消泡剂和/或脱气剂倾向于发泡

    公开(公告)号：US20060111453A1

    公开(公告)日：2006-05-25

    申请号：US10519405

    申请日：2003-07-16

    申请人： Johann Bonn ,  Klaus Lorenz ,  Jorg Wehrle ,  Manfred Matz

    发明人： Johann Bonn ,  Klaus Lorenz ,  Jorg Wehrle ,  Manfred Matz

    IPC分类号： C09K3/00 ,  B01D17/00

    CPC分类号： D21H21/12 ,  B01D19/0404 ,  B01D19/0413 ,  B01D19/0422

    摘要： Antifoams and/or deaerators based on oil-in-water dispersions, whose oil phase contains at least one compound from the group consisting of the alcohols of at least 12 carbon atoms, alkoxylated fatty alcohols, mono-, di- and triglycerides of fatty acids, fatty acid esters of carboxylic acids of at least 12 carbon atoms and monohydric to tetrahydric alcohols of 1 to 24 carbon atoms, hydrocarbons having a boiling point above 200° C., fatty acids of 12 to 26 carbon atoms, 3-thiaalkan-1-ols, 3-thiaoxoalkan-1-ols, 3-thiadioxoalkanols and esters of thiaalkane compounds in combination with (i) at least one polyglyceryl ester which is obtainable by at least 20% esterification of polyglycerol with a carboxylic acid of 12 to 36 carbon atoms and (ii) at least one bisamide of ethylenediamine and carboxylic acids of 10 to 36 carbon atoms and whose aqueous phase contains at least one stabilizer, water and, if required, a thickener, for aqueous media which tend to form foam, are used for foam control of aqueous media which tend to form foam, in particular for foam control in pulp cooking, pulp washing, the beating of paper stock, papermaking and the dispersing of pigments for papermaking.

    摘要翻译： 基于油包水分散体的消泡剂和/或除氧器，其油相含有至少一种由至少12个碳原子的醇组成的组，烷氧基化脂肪醇，脂肪酸的一，二和三酸甘油酯 至少12个碳原子的羧酸的脂肪酸酯和1至24个碳原子的一羟基至四氢醇，沸点高于200℃的烃，12-26个碳原子的脂肪酸，3-硫杂烷-1- - 醇，3-硫代氧代烷-1-醇，3-硫代二烷基链烷醇和硫代烷烃化合物的酯与（i）至少一种聚甘油酯组合，所述聚甘油酯可通过聚甘油与12至36碳羧酸的酯化至少20％ 原子和（ii）至少一种具有10至36个碳原子的乙二胺和羧酸的二酰胺，并且其水相含有至少一种稳定剂，水和如果需要，增稠剂用于倾向于形成泡沫的水性介质， 用于泡沫控制 倾向于形成泡沫的水性介质，特别是用于纸浆蒸煮中的泡沫控制，纸浆清洗，纸浆的打浆，造纸和用于造纸的颜料的分散。

    Defoaming agent and/or deaerator for aqueous media tending to foam
    3.
    发明授权
    Defoaming agent and/or deaerator for aqueous media tending to foam 有权
    用于水性介质的消泡剂和/或脱气剂倾向于发泡

    公开(公告)号：US07763664B2

    公开(公告)日：2010-07-27

    申请号：US10519405

    申请日：2003-07-16

    申请人： Johann Bonn ,  Klaus Lorenz ,  Joerg Wehrle ,  Manfred Matz

    发明人： Johann Bonn ,  Klaus Lorenz ,  Joerg Wehrle ,  Manfred Matz

    IPC分类号： B01D19/04 ,  D21C3/28 ,  D21H21/12 ,  B01F3/12

    CPC分类号： D21H21/12 ,  B01D19/0404 ,  B01D19/0413 ,  B01D19/0422

    摘要： A defoaming agent and/or deaerator for aqueous foamable media based on oil-in-water dispersions. The oil phase contains at least one compound from fatty alcohols, fatty acid monoglycerides, diglycerides, and triglycerides, fatty acid ester of fatty acids and monovalent to trivalent alcohols, 3-thiaalkane-1-ole, 3-thiaoxide alkane-1-ole, 3-thiadioxide-alkane-ole, and thiaalkane esters in combination with (i) at least one polyglycerine that is obtained by esterification of at least 20 percent of polyglycerine with 12 to 36 C carboxylic acid, and (ii) at least one bisamide consisting of ethylene diamine and 10 to 36 C atom carboxylic acids, while the aqueous phase thereof contains at least one stabilizer, water, and an optional thickener, for aqueous media that tend to foam. Also disclosed are methods of controlling foam by adding the dispersions to a process, particularly during cellulose boiling, cellulose washing, grinding of paper pulp, paper production, and dispersion of pigments used for paper production.

    摘要翻译： 一种基于水包油分散体的含水可发泡介质的消泡剂和/或脱气剂。 油相包含至少一种脂肪醇，脂肪酸单甘油酯，甘油二酯和甘油三酸酯，脂肪酸脂肪酸酯和一价至三价醇的化合物，3-硫代烷-1-烯，3-硫氧化物烷-1-醇， 三硫代 - 烷烃 - 烯烃和硫代烷烃酯与（i）至少一种通过至少20％的聚甘油与12至36℃羧酸酯化获得的聚甘油，和（ii）至少一种双酰胺 的乙二胺和10至36C原子的羧酸，而其水相含有至少一种稳定剂，水和任选的增稠剂，用于易于发泡的水性介质。 还公开了通过将分散体加入到方法中，特别是在纤维素沸腾，纤维素洗涤，纸浆研磨，造纸和用于纸张生产的颜料的分散体中来控制泡沫的方法。

    Defoaming agents devoid of emulsifiers, method for producing said agents and use thereof
    4.
    发明申请
    Defoaming agents devoid of emulsifiers, method for producing said agents and use thereof 审中-公开
    不含乳化剂的消泡剂，生产所述试剂的方法及其用途

    公开(公告)号：US20060276554A1

    公开(公告)日：2006-12-07

    申请号：US10570154

    申请日：2004-08-27

    申请人： Rainer Dyllick-Brenzinger ,  Markus Schmid ,  Jorg Wehrle ,  Klaus Lorenz ,  Stefan Bruhns ,  Michael Senge

    发明人： Rainer Dyllick-Brenzinger ,  Markus Schmid ,  Jorg Wehrle ,  Klaus Lorenz ,  Stefan Bruhns ,  Michael Senge

    IPC分类号： B01D17/05

    CPC分类号： B01D19/0422 ,  B01D19/0404

    摘要： Emulsifier-free antifoams are obtainable by mixing a) from 80 to 99% by weight of at least one finely divided, virtually water-insoluble, inert solid with b) from 1 to 20% by weight of at least one hydrophobic, organic compound which has an antifoam action and is solid at room temperature in the absence of a solvent in a shear gradient such that the particle size of the compounds (b) which have an antifoam action is reduced to a mean particle size of from 0.5 to 15 μm, emulsifier-free oil-in-water dispersions of mixtures of (a) and (b) are prepared by mixing the component (a) in an amount of from 80 to 99% by weight with the compounds of component (b) in an amount of from 1 to 20% by weight in the absence of emulsifiers in an extruder or kneader in a manner such that the mean particle size of the component (b) in the mixture is brought to 0.5 to 15 μm, at up to 100° C., and emulsifying the mixture in water, and the oil-in-water dispersions thus obtainable are used as antifoams and/or deaerators for aqueous, disperse or nondisperse liquids, in particular as antifoams and/or deaerators in the paper industry, in the food industry and in wastewater treatment plants.

    摘要翻译： 不含无乳化剂的消泡剂可通过将a）80至99重量％的至少一种细分的，实际上不溶于水的惰性固体与b）1至20重量％的至少一种疏水性有机化合物 具有消泡作用，并且在不存在溶剂的剪切梯度的情况下在室温下是固体，使得具有消泡作用的化合物（b）的粒度降低至0.5至15μm的平均粒度， （a）和（b）的混合物的无乳化剂的水包油分散体通过将组分（a）以80至99重量％的量与组分（b）的化合物的量以 在挤出机或捏合机中，在不存在乳化剂的情况下为1至20重量％，使混合物中组分（b）的平均粒度达到0.5至15μm，在高达100℃ 并将混合物乳化在水中，并且由此获得的水包油分散体用作消泡剂和/或 用于水性，分散或非分散液体的脱气器，特别是在造纸工业，食品工业和废水处理厂中的消泡剂和/或脱气剂。

    Process for producing polyester polyols having secondary OH end groups
    7.
    发明授权
    Process for producing polyester polyols having secondary OH end groups 有权
    制备具有次级OH端基的聚酯多元醇的方法

    公开(公告)号：US09193822B2

    公开(公告)日：2015-11-24

    申请号：US13318157

    申请日：2010-05-04

    申请人： Hartmut Nefzger ,  Erika Bauer ,  Jörg Hofmann ,  Klaus Lorenz ,  Bert Klesczewski

    发明人： Hartmut Nefzger ,  Erika Bauer ,  Jörg Hofmann ,  Klaus Lorenz ,  Bert Klesczewski

    IPC分类号： C07C69/675 ,  C08G63/91 ,  C08G18/42 ,  C08G63/87

    CPC分类号： C08G63/914 ,  C08G18/4261 ,  C08G63/87

    摘要： The invention relates to a process for producing polyester polyols with secondary hydroxyl end groups, including the step of the reaction of a polyester including carboxyl end groups with an epoxide of the general formula (1): wherein R1 stands for an alkyl residue or an aryl residue and the reaction is carried out in the presence of a catalyst that includes at least one nitrogen atom per molecule. The process is distinguished in that the polyester including carboxyl end groups exhibits an acid value from ≧25 mg KOH/g to ≦400 mg KOH/g and a hydroxyl value from ≦5 mg KOH/g and in that the polyester including carboxyl end groups is produced by ≧1.03 mol to ≦1.90 mol carboxyl groups or carboxyl-group equivalents of an acid component being employed per mol hydroxyl groups of an alcohol. The polyester polyols obtained, including secondary hydroxyl end groups, can be used for the purpose of producing polyurethane polymers.

    摘要翻译： 本发明涉及一种生产具有仲羟基端基的聚酯多元醇的方法，包括包括羧基端基的聚酯与通式（1）的环氧化物反应的步骤：其中R1代表烷基或芳基 残基，反应在每分子包含至少一个氮原子的催化剂存在下进行。 该方法的区别在于包括羧基端基的聚酯显示出≥25mgKOH / g至≥1000的KOH值，400mg KOH / g的酸值和来自＆lt; NEE的5K KOH / g的羟值，并且包括羧基的聚酯 端基是由醇的每摩尔羟基使用的≥1.03摩尔至1升; 1.90摩尔羧基或酸组分的羧基当量。 得到的聚酯多元醇（包括仲羟基端基）可用于制备聚氨酯聚合物。

    METHOD FOR PRODUCING POLYTHER POLYOLS
    10.
    发明申请
    METHOD FOR PRODUCING POLYTHER POLYOLS 有权
    生产多聚多元醇的方法

    公开(公告)号：US20130204047A1

    公开(公告)日：2013-08-08

    申请号：US13582786

    申请日：2011-03-09

    申请人： Klaus Lorenz

    发明人： Klaus Lorenz

    IPC分类号： C07C41/02

    CPC分类号： C07C41/02 ,  C08G18/283 ,  C08G18/4883 ,  C08G65/2609 ,  C08G65/2696 ,  C08G2650/26

    摘要： The present invention relates to is coupling process for the preparation of polyether polyols starting from highly functional starter compounds that are solid or highly viscous under reaction conditions and monofunctional starter compounds that are liquid under reaction conditions with Zerewitinoff-active hydrogen atoms.

    摘要翻译： 本发明涉及用于制备聚醚多元醇的偶合方法，其起始于在反应条件下为固体或高粘度的高官能起始化合物，以及在具有齐来维诺 - 活性氢原子的反应条件下为液体的单官能起始化合物。