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公开(公告)号：US06429184B1
公开(公告)日：2002-08-06
申请号：US09659715
申请日：2000-09-11
申请人： Johannes Hendrikus Akkermans , Michael Frederick Edwards , Andreas Theodorus Groot , Cornelis Paulus Montanus , Roland Wilhelmus Pomeren , Korkut Ahmet Yuregir
发明人： Johannes Hendrikus Akkermans , Michael Frederick Edwards , Andreas Theodorus Groot , Cornelis Paulus Montanus , Roland Wilhelmus Pomeren , Korkut Ahmet Yuregir
IPC分类号： C11D1100
CPC分类号： C11D11/0088
摘要： A granular detergent product is made by spraying a liquid binder to contact a particulate solid starting material in a low shear granulator such as a fluidized bed apparatus. The d3,2 average droplet diameter of the liquid binder is not greater than ten times the d3,2 average particle diameter of that fraction of the solid starting material which has a d3,2 particle diameter of from 20 &mgr;m to 200 &mgr;m provided that if more than 90% by weight of the solid starting material has a d3,2 average particle diameter less than 20 &mgr;m then the d3,2 average particle diameter of the total solid starting materials shall be taken to be 20 &mgr;m. If more than 90% by weight of the solid starting material has a d3,2 average particle diameter greater than 200 &mgr;m than the d3,2 average particle diameter of the total starting solid material shall be taken to be 200 &mgr;m.
摘要翻译： 颗粒状洗涤剂产品是通过喷射液体粘合剂以在低剪切制粒机如流化床装置中接触颗粒状固体起始材料制成的。 液体粘合剂的d3,2平均液滴直径不大于具有d3,2粒径为20μm至200μm的固体原料的该部分的d3,2平均粒径的十倍，条件是如果 大于90重量％的固体起始材料具有小于20μm的d3,2平均粒径，则总固体原料的d3,2平均粒径应取为20μm。 如果90重量％以上的固体原料具有比起始固体材料的平均粒径d3,2平均粒径大于200μm的平均粒径d3,22，则应为200μm。
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公开(公告)号：US06274544B1
公开(公告)日：2001-08-14
申请号：US09097335
申请日：1998-06-15
申请人： Johannes Hendrikus Akkermans , Michael Frederick Edwards , Andreas Theodorus Groot , Cornelis Paulus Montanus , Roland Wilhelmus Pomeren , Korkut Ahmet Yuregir
发明人： Johannes Hendrikus Akkermans , Michael Frederick Edwards , Andreas Theodorus Groot , Cornelis Paulus Montanus , Roland Wilhelmus Pomeren , Korkut Ahmet Yuregir
IPC分类号： C11D1100
CPC分类号： C11D11/0088
摘要： A granular detergent product is made by spraying a liquid binder to contact a particulate solid starting material in a low shear granulator such as a fluidised bed apparatus. The d3,2 average droplet diameter is not greater than ten times the d3,2 average particle diameter of that fraction of the solid starting material which has a d3,2 particle diameter of from 20 &mgr;m to 200 &mgr;m provided that if more than 90% by weight of the solid starting material has a d3,2 average particle diameter less than 20 &mgr;m then the d3,2 average particle diameter of the total solid starting materials shall be taken to be 20 &mgr;m. If more than 90% by weight of the solid starting material has a d3,2 average particle diameter greater than 200 &mgr;m then the d3,2 average particle diameter of the total starting solid material shall be taken to be 200 &mgr;m.
摘要翻译： 颗粒状洗涤剂产品通过喷射液体粘合剂以在低剪切制粒机例如流化床装置中与颗粒状固体原料接触来制备。 d3,2平均液滴直径不大于具有d3,2粒径为20〜200μm的固体原料的该部分的d3,2平均粒径的十倍，条件是如果超过90％ 的固体原料具有小于20μm的d3,2平均粒径，则总固体原料的d3,2平均粒径应取为20μm。 如果大于90重量％的固体原料具有大于200μm的d3,2平均粒径，则总起始固体材料的d3,2平均粒径应取为200μm。
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公开(公告)号：US6056905A
公开(公告)日：2000-05-02
申请号：US94822
申请日：1998-06-15
申请人： Johannes Hendrikus Akkermans , Michael Frederick Edwards , Andreas Theodorus Groot , Cornelis Paulus Montanus , Roland Wilhelmus Pomeren , Korkut Ahmet Yuregir
发明人： Johannes Hendrikus Akkermans , Michael Frederick Edwards , Andreas Theodorus Groot , Cornelis Paulus Montanus , Roland Wilhelmus Pomeren , Korkut Ahmet Yuregir
IPC分类号： C11D11/00
CPC分类号： C11D11/0088
摘要： A process of forming a granular detergent products, is effected in a gas fluidisation granulator. A fluidised particulate solid material is contacted with a spray of liquid binder. The excess velocity (U.sub.e) of fluidisation gas relative to the mass or volume flux of the spray (q.sub.mliq or q.sub.vliq) when determined at the normalised nozzle-to-bed distance (D.sub.0) is set so that the flux number (FN.sub.m or FN.sub.v) as determined by ##EQU1## (where .rho..sub.p is the particle density) is at a critical value of at least 2 for at least 30% of the process.
摘要翻译： 形成颗粒状洗涤剂产品的方法在气体流化造粒机中进行。 流化的颗粒固体材料与液体粘合剂的喷雾物接触。 流化气体相对于喷雾质量或体积通量（+ E，点q + EE mliq或+ E，点q + EE vliq）的超速度（Ue） D0）被设定为使得由（其中rho p是粒子密度）确定的通量（FNm或FNv）在至少30％的过程中处于至少2的临界值。
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公开(公告)号：US07053038B2
公开(公告)日：2006-05-30
申请号：US10214695
申请日：2002-08-08
IPC分类号： C11D11/00
CPC分类号： C11D3/042 , C11D1/143 , C11D1/146 , C11D1/22 , C11D1/29 , C11D3/10 , C11D3/2075 , C11D11/0088 , C11D11/04
摘要： A low shear mechanical granulation process for the production of detergent granules, the process comprising contacting an acid precursor of an anionic surfactant, a non-surfactant acid and a solid carbonated neutralising agent wherein the solid carbonated neutralizing agent has a d3,2 average particle size no more than 90 μm, preferably no more than 80 μm, more preferably no more than 70 μm, still more preferably no more than 60 μm, yet more preferably no more than 50 μm and especially no more than 40 μm.
摘要翻译： 用于生产洗涤剂颗粒的低剪切机械造粒方法，该方法包括使阴离子表面活性剂的酸前体，非表面活性剂酸和固体碳酸化中和剂接触，其中固体碳酸中和剂具有 平均粒径不超过90μm，优选不超过80μm，更优选不超过70μm，还更优选不超过60μm，还更优选不大于50μm，特别是不大于50μm。 40个妈妈
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公开(公告)号：US06518233B2
公开(公告)日：2003-02-11
申请号：US09957228
申请日：2001-09-20
IPC分类号： C11D1700
CPC分类号： C11D11/04 , C11D11/0082
摘要： In process for producing detergent particles, an acid precursor of an anionic surfactant and a neutralizing agent are fed into a horizontal thin-film evaporator/drier where they are neutralized, granulated and dried. The neutralizing agent is present in an amount equal to or in excess that required for stoichiometric neutralization and has a D50 mean particle size of less than 40 &mgr;m.
摘要翻译： 在制造洗涤剂颗粒的过程中，将阴离子表面活性剂的酸前体和中和剂加入水平薄膜蒸发器/干燥器中，将其中和，造粒和干燥。 中和剂以等于或超过化学计量中和所需的量存在，并且具有小于40μm的D50平均粒度。
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公开(公告)号：US06514930B2
公开(公告)日：2003-02-04
申请号：US09957326
申请日：2001-09-20
IPC分类号： C11D1700
CPC分类号： C11D3/128 , C11D11/0082 , C11D11/04
摘要： A process for the production of detergent particles comprises feeding an acid precursor of an anionic surfactant, a neutralizing agent and aluminosilicate detergency builder into a horizontal thin-film evaporator/drier. The evaporator/drier comprises a mixing region, a drying region and a cooling region. Neutralization of the acid precursor is effected, together with granulation, drying and cooling, to form the detergent particles. At least some of the aluminosilicate builder is fed into the thin-film evaporator/drier between the drying region and the cooling region and/or into the cooling region. When all of he aluminosilicate builder is fed into the cooling region, the aluminosilicate is in an amount of more than 20% by weight of the particles exiting the cooling region.
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7.发明授权公开(公告)号：US06221831B1
公开(公告)日：2001-04-24
申请号：US09084567
申请日：1998-05-26
申请人： William Derek Emery , Andreas Theodorus Groot , Terry Instone , Seeng Djiang Liem , Kenneth Metcalfe , Richard George Smith , Gilbert Martin Verschelling
发明人： William Derek Emery , Andreas Theodorus Groot , Terry Instone , Seeng Djiang Liem , Kenneth Metcalfe , Richard George Smith , Gilbert Martin Verschelling
IPC分类号： C11D102
摘要： A free-flowing built particulate laundry detergent composition comprises: (i) at least 27% by weight of non-soap organic detergent surfactant, (ii) one or more detergency builders, but not more than 7% by weight of alkali metal aluminosilicate, the weight ratio of surfactant to builder being at least 1.2:1.
摘要翻译： 一种自由流动的颗粒状洗衣洗涤剂组合物包含：（i）至少27重量％的非皂有机洗涤剂表面活性剂，（ii）一种或多种去污助洗剂，但不超过7重量％的碱金属铝硅酸盐， 表面活性剂与助洗剂的重量比至少为1.2:1。
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公开(公告)号：US06680288B1
公开(公告)日：2004-01-20
申请号：US09718468
申请日：2000-11-21
IPC分类号： C11D1100
CPC分类号： C11D11/0082 , C11D17/06
摘要： A process for preparing a free-flowing granular detergent composition with improved storage stability involves granulation of a solid starting material comprising a hydratable salt with a liquid binder and treating the resulting granules in a low shear mixer with from 0.5 to 20 wt % of water.
摘要翻译： 制备具有改善的储存稳定性的自由流动的颗粒洗涤剂组合物的方法包括将含有可水合盐的固体起始材料与液体粘合剂造粒，并在0.5至20重量％的水的低剪切混合器中处理所得颗粒。
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公开(公告)号：US06518234B2
公开(公告)日：2003-02-11
申请号：US09957227
申请日：2001-09-20
IPC分类号： C11D1700
CPC分类号： C11D11/0082 , C11D11/04
摘要： A process for the production of detergent particles, comprises feeding an acid precursor of an anionic surfactant and a neutralising agent into a horizontal thin-film evaporator/drier comprising a mixing region, a drying region and a cooling region. The resultant detergent particles are graded to separate an oversize granule fraction in which at least 70 wt % of the particles have a minimum diameter of 1000 &mgr;m. This fraction is fed back into the process.
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