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    Tin free silyl-terminated polymers
    1.
    发明授权
    Tin free silyl-terminated polymers 有权
    无锡甲硅烷基封端的聚合物

    公开(公告)号：US08877885B2

    公开(公告)日：2014-11-04

    申请号：US13704162

    申请日：2011-06-29

    申请人： Kamesh R. Vyakaranam ,  Ling Zhang ,  William A. Koonce ,  Juan Carlos Medina ,  Ganesh Kailasam ,  Rajat Duggal ,  Nathan Wilmot

    发明人： Kamesh R. Vyakaranam ,  Ling Zhang ,  William A. Koonce ,  Juan Carlos Medina ,  Ganesh Kailasam ,  Rajat Duggal ,  Nathan Wilmot

    IPC分类号： C08G18/20

    CPC分类号： C08G18/222 ,  C08G18/18 ,  C08G18/20 ,  C08G18/289 ,  C08G18/3893 ,  C08G18/4825 ,  C08G18/718 ,  C08G18/7621 ,  C08G18/7671 ,  C08G18/837

    摘要： Embodiments of the invention provide for methods of producing a composition comprising a crosslinkable silane-terminated polymer having at least one crosslinkable silyl group in each molecule. The method comprises providing a polymer having at least one unsaturated group and at least one alcoholic hydroxyl group in each molecule, adding to the polymer a compound having a hydrogen-silicon bond and a crosslinkable silyl group in each molecule and a hydrosilylation catalyst to thereby carry out a hydrosilylation reaction to form a composition comprising hydrosilylated polyoxyalkylene polymers, reacting the hydrosilylated polyoxyalkylene polymers with at least one isocyanate in the presence of a first tin-free catalyst to form an isocyanate reacted hydrosilylated polymer, and optionally reacting the isocyanate reacted hydrosilylated polymer with a polyol having a nominal functionality of at least 2 to form a polyol reacted crosslinkable silane-terminated polymer.

    摘要翻译： 本发明的实施方案提供了制备包含在每个分子中具有至少一个可交联甲硅烷基的可交联的硅烷端基聚合物的组合物的方法。 该方法包括在每个分子中提供具有至少一个不饱和基团和至少一个醇羟基的聚合物，向该聚合物中加入每个分子中具有氢 - 硅键和交联性甲硅烷基的化合物和氢化硅烷化催化剂从而携带 进行氢化硅烷化反应以形成包含氢化硅烷化聚氧化烯聚合物的组合物，在第一无锡催化剂存在下使氢化硅烷化聚氧化烯聚合物与至少一种异氰酸酯反应，以形成异氰酸酯反应的氢化硅烷化聚合物，以及任选地使异氰酸酯反应的硅烷化聚合物与 具有至少2的标称官能度的多元醇以形成多元醇反应的可交联的硅烷封端的聚合物。

    COMPRESSION SET PROPERTY IN SILYLATED POLYMERS
    3.
    发明申请
    COMPRESSION SET PROPERTY IN SILYLATED POLYMERS 有权
    在SILYLATED聚合物中的压缩集合

    公开(公告)号：US20140228515A1

    公开(公告)日：2014-08-14

    申请号：US14342652

    申请日：2012-09-17

    申请人： Kamesh R. Vyakaranam ,  Ling Zhang ,  Venkat S. Minnikanti ,  Dwight Latham ,  Sara Arshad ,  Rajat Duggal ,  William A. Koonce

    发明人： Kamesh R. Vyakaranam ,  Ling Zhang ,  Venkat S. Minnikanti ,  Dwight Latham ,  Sara Arshad ,  Rajat Duggal ,  William A. Koonce

    IPC分类号： C08L71/00

    CPC分类号： C08L71/00 ,  C08G65/336 ,  C08K5/0025 ,  C08L71/02 ,  C08L75/04 ,  C08L75/08 ,  C08L83/00 ,  C08L83/06 ,  C08L101/10

    摘要： Moisture curable compositions including silylated polymers and methods for producing the same are provided. A two component moisture curable system for producing a cured or cross-linked silylated polymer having improved compression set properties is provided. The two component system comprises a first formulation and a second formulation. The first formulation comprises a silylated polymer, water, and filler and the second formulation comprises the silylated polymer, a curing catalyst comprising at least one Brønsted acid, and a moisture scavenger. The final cured formulation may have a compression set, determined by ASTM D395 or ISO 815-1, of less than 100%, and in some examples less than 50% and in some examples less than 15%. This demonstrated improvement in compression set not only allows the silylated polymers to be used in applications where cyclic loads are applied but also enhances product durability.

    摘要翻译： 提供了包含甲硅烷基化聚合物的水溶性组合物及其制备方法。 提供了用于制备具有改进的压缩永久变形特性的固化或交联的甲硅烷基化聚合物的双组分湿气可固化体系。 双组分体系包括第一制剂和第二制剂。 第一制剂包含甲硅烷基化聚合物，水和填料，第二制剂包含甲硅烷基化聚合物，包含至少一种布朗斯台德酸的固化催化剂和除湿剂。 最终固化的制剂可以具有通过ASTM D395或ISO 815-1测定的压缩永久变形小于100％，在一些实例中小于50％，在一些实例中小于15％。 这表明压缩变形的改进不仅允许将甲硅烷基化的聚合物用于应用循环载荷的应用中，而且可以提高产品的耐久性。

    Compression set property in silylated polymers
    4.
    发明授权
    Compression set property in silylated polymers 有权
    甲硅烷基化聚合物的压缩性能

    公开(公告)号：US09181428B2

    公开(公告)日：2015-11-10

    申请号：US14342652

    申请日：2012-09-17

    申请人： Kamesh R. Vyakaranam ,  Ling Zhang ,  Venkat S. Minnikanti ,  Dwight Latham ,  Sara Arshad ,  Rajat Duggal ,  William A. Koonce

    发明人： Kamesh R. Vyakaranam ,  Ling Zhang ,  Venkat S. Minnikanti ,  Dwight Latham ,  Sara Arshad ,  Rajat Duggal ,  William A. Koonce

    IPC分类号： C08G77/06 ,  C08L71/00 ,  C08G65/336 ,  C08L101/10 ,  C08L71/02 ,  C08L75/08 ,  C08L75/04 ,  C08L83/00 ,  C08L83/06 ,  C08K5/00

    CPC分类号： C08L71/00 ,  C08G65/336 ,  C08K5/0025 ,  C08L71/02 ,  C08L75/04 ,  C08L75/08 ,  C08L83/00 ,  C08L83/06 ,  C08L101/10

    摘要： Moisture curable compositions including silylated polymers and methods for producing the same are provided. A two component moisture curable system for producing a cured or cross-linked silylated polymer having improved compression set properties is provided. The two component system comprises a first formulation and a second formulation. The first formulation comprises a silylated polymer, water, and filler and the second formulation comprises the silylated polymer, a curing catalyst comprising at least one Brønsted acid, and a moisture scavenger. The final cured formulation may have a compression set, determined by ASTM D395 or ISO 815-1, of less than 100%, and in some examples less than 50% and in some examples less than 15%. This demonstrated improvement in compression set not only allows the silylated polymers to be used in applications where cyclic loads are applied but also enhances product durability.

    摘要翻译： 提供了包含甲硅烷基化聚合物的水溶性组合物及其制备方法。 提供了用于制备具有改进的压缩永久变形特性的固化或交联的甲硅烷基化聚合物的双组分湿气可固化体系。 双组分体系包括第一制剂和第二制剂。 第一制剂包含甲硅烷基化聚合物，水和填料，第二制剂包含甲硅烷基化聚合物，包含至少一种布朗斯台德酸的固化催化剂和除湿剂。 最终固化的制剂可以具有通过ASTM D395或ISO 815-1测定的压缩永久变形小于100％，在一些实例中小于50％，在一些实例中小于15％。 这表明压缩变形的改进不仅允许将甲硅烷基化的聚合物用于应用循环载荷的应用中，而且可以提高产品的耐久性。

    Process for making low viscosity, fast curing silane terminated polymers
    5.
    发明授权
    Process for making low viscosity, fast curing silane terminated polymers 有权
    制备低粘度，快速固化硅烷封端聚合物的方法

    公开(公告)号：US08987401B2

    公开(公告)日：2015-03-24

    申请号：US14119072

    申请日：2012-06-14

    申请人： Kamesh R. Vyakaranam ,  Ling Zhang ,  Venkat S. Minnikanti ,  Rajat Duggal ,  William A. Koonce ,  Amarnath Singh ,  Phillip S. Athey

    发明人： Kamesh R. Vyakaranam ,  Ling Zhang ,  Venkat S. Minnikanti ,  Rajat Duggal ,  William A. Koonce ,  Amarnath Singh ,  Phillip S. Athey

    IPC分类号： C08G77/06 ,  C08G18/10 ,  C08G18/28 ,  C08G18/71 ,  C08G18/76

    CPC分类号： C08G18/10 ,  C08G18/289 ,  C08G18/718 ,  C08G18/7621 ,  C08G2190/00 ,  C08G18/4825 ,  C08G18/4829

    摘要： Methods of producing a composition comprising a crosslinkable silane-terminated polymer having at least one crosslinkable silyl group in each molecule are provided. The method may comprise providing a polymer having at least one unsaturated group and at least one alcohol hydroxyl group in each molecule and having a number average molecular weight between about 100 and about 5,000, adding to the polymer a compound having a hydrogen-silicon bond and a crosslinkable silyl group in each molecule and a hydrosilylation catalyst to thereby carry out a hydrosilylation reaction to form a composition comprising hydrosilylated polymers, wherein the hydrosilylation reaction has a hydrosilylation efficiency greater than 50% as determined by 1H-NMR, capping the hydrosilylated polymers by adding the hydrosilylated polymer to at least one isocyanate at an index of between about 100 and about 250, and reacting the isocyanate capped hydrosilylated polymer with a polyol having a nominal functionality of at least 2 to form the composition comprising a crosslinkable silane-terminated polymer.

    摘要翻译： 提供了包含在每个分子中具有至少一个交联性甲硅烷基的可交联硅烷封端的聚合物的组合物的方法。 该方法可以包括提供在每个分子中具有至少一个不饱和基团和至少一个醇羟基并且数均分子量在约100和约5,000之间的聚合物，向聚合物中加入具有氢 - 硅键的化合物和 每个分子中的可交联甲硅烷基和氢化硅烷化催化剂，由此进行氢化硅烷化反应以形成包含氢化硅烷化聚合物的组合物，其中氢化硅烷化反应的氢化硅烷化效率大于50％，如通过1 H-NMR确定的，氢化硅烷化聚合物由 将氢化硅烷化聚合物以约100至约250的指数加入到至少一种异氰酸酯中，并使异氰酸酯封端的硅烷化聚合物与标称官能度至少为2的多元醇反应，以形成包含可交联硅烷封端的聚合物的组合物。

    Low viscosity silyl-terminated polymers
    6.
    发明授权
    Low viscosity silyl-terminated polymers 有权
    低粘度甲硅烷基封端的聚合物

    公开(公告)号：US08822606B2

    公开(公告)日：2014-09-02

    申请号：US13805952

    申请日：2011-06-29

    申请人： Ling Zhang ,  Kamesh R. Vyakaranam ,  Sara Arshad ,  William A. Koonce

    发明人： Ling Zhang ,  Kamesh R. Vyakaranam ,  Sara Arshad ,  William A. Koonce

    IPC分类号： C08G18/10 ,  C08G18/50

    CPC分类号： C08G18/3893 ,  C08G18/10 ,  C08G18/289 ,  C08G18/4825 ,  C08G18/4829 ,  C08G18/5096 ,  C08G18/718 ,  C08G18/7621 ,  C08G18/809 ,  C08G18/837 ,  C08G77/46 ,  C08G18/48

    摘要： Embodiment of the invention provide for compositions having at least one crosslinkable silyl group in each molecule. The crosslinkable silane-terminated polymer may include a reaction product of at least a polyol having a nominal functionality of at least 2 and a isocyanate capped hydrosilylated polymer. The isocyanate capped hydrosilylated polymer may include a reaction product of at least one isocyanate and a hydrosilylated polymer. The hydrosilylated polymer may include a reaction product of a the reaction of at least a) a polymer having at least one unsaturated group and at least one alcoholic hydroxyl group in each molecule and having a number average molecular weight of between about 100 and about 5000 and b) a compound having a hydrogen-silicon bond and a crosslinkable silyl group in each molecule.

    摘要翻译： 本发明的实施方案提供了在每个分子中具有至少一个可交联甲硅烷基的组合物。 可交联硅烷封端的聚合物可以包括至少具有至少2的标称官能度的多元醇和异氰酸酯封端的氢化硅烷化聚合物的反应产物。 异氰酸酯封端的氢化硅烷化聚合物可以包括至少一种异氰酸酯和氢化硅烷化聚合物的反应产物。 氢化硅烷化聚合物可以包括至少一种在每个分子中具有至少一个不饱和基团和至少一个醇羟基的聚合物与数均分子量为约100至约5000的反应的反应产物和数均分子量为约100至约5000的反应产物，以及 b）在每个分子中具有氢 - 硅键和交联性甲硅烷基的化合物。

    LOW VISCOSITY SILYL-TERMINATED POLYMERS
    7.
    发明申请
    LOW VISCOSITY SILYL-TERMINATED POLYMERS 有权
    低粘度SILYL-TERMINATED聚合物

    公开(公告)号：US20130090429A1

    公开(公告)日：2013-04-11

    申请号：US13805952

    申请日：2011-06-29

    申请人： Ling Zhang ,  Kamesh R. Vyakaranam ,  Sara Arshad ,  William A. Koonce

    发明人： Ling Zhang ,  Kamesh R. Vyakaranam ,  Sara Arshad ,  William A. Koonce

    IPC分类号： C08G18/38

    CPC分类号： C08G18/3893 ,  C08G18/10 ,  C08G18/289 ,  C08G18/4825 ,  C08G18/4829 ,  C08G18/5096 ,  C08G18/718 ,  C08G18/7621 ,  C08G18/809 ,  C08G18/837 ,  C08G77/46 ,  C08G18/48

    摘要： Embodiment of the invention provide for compositions having at least one crosslinkable silyl group in each molecule. The crosslinkable silane-terminated polymer may include a reaction product of at least a polyol having a nominal functionality of at least 2 and a isocyanate capped hydrosilylated polymer. The isocyanate capped hydrosilylated polymer may include a reaction product of at least one isocyanate and a hydrosilylated polymer. The hydrosilylated polymer may include a reaction product of a the reaction of at least a) a polymer having at least one unsaturated group and at least one alcoholic hydroxyl group in each molecule and having a number average molecular weight of between about 100 and about 5000 and b) a compound having a hydrogen-silicon bond and a crosslinkable silyl group in each molecule.

    摘要翻译： 本发明的实施方案提供了在每个分子中具有至少一个可交联甲硅烷基的组合物。 可交联硅烷封端的聚合物可以包括至少具有至少2的标称官能度的多元醇和异氰酸酯封端的氢化硅烷化聚合物的反应产物。 异氰酸酯封端的氢化硅烷化聚合物可以包括至少一种异氰酸酯和氢化硅烷化聚合物的反应产物。 氢化硅烷化聚合物可以包括至少一种在每个分子中具有至少一个不饱和基团和至少一个醇羟基的聚合物与数均分子量为约100至约5000的反应的反应产物和数均分子量为约100至约5000的反应产物，以及 b）在每个分子中具有氢 - 硅键和交联性甲硅烷基的化合物。

    Silane terminated polymer for coating, adhesives, sealant and elastomer applications
    8.
    发明授权
    Silane terminated polymer for coating, adhesives, sealant and elastomer applications 有权
    用于涂料，粘合剂，密封剂和弹性体应用的硅烷封端聚合物

    公开(公告)号：US08907014B2

    公开(公告)日：2014-12-09

    申请号：US14113318

    申请日：2012-06-14

    申请人： Kamesh R. Vyakaranam ,  William A. Koonce ,  Ling Zhang ,  Jean-Luc Roser

    发明人： Kamesh R. Vyakaranam ,  William A. Koonce ,  Ling Zhang ,  Jean-Luc Roser

    IPC分类号： C08G81/02 ,  C08G18/70 ,  C08G18/10 ,  C08G18/28 ,  C08G18/63 ,  C08G18/71 ,  C08G18/76

    CPC分类号： C08G81/025 ,  C08G18/10 ,  C08G18/289 ,  C08G18/632 ,  C08G18/718 ,  C08G18/7621 ,  C08G18/63

    摘要： A copolymer-filled crosslinkable silane-terminated polymer having at least one crosslinkable silyl group in each molecule is provided. The copolymer-filled crosslinkable silane-terminated polymer is the reaction product of a copolymer-filled polyol and an isocyanate capped hydrosilylated polymer. The isocyanate capped hydrosilylated polymer is the reaction product of at least one isocyanate and a hydrosilylated polymer. The hydrosilylated polymer is the reaction product of a polymer having at least one unsaturated group and at least one alcoholic group in each molecule and a compound having a hydrogen-silicon bond and a crosslinkable silyl group in each molecule. The copolymer-filled crosslinkable silane-terminated polymers exhibit improved modulus and tensile strength properties while maintaining elongation properties.

    摘要翻译： 提供了在每个分子中具有至少一个可交联甲硅烷基的共聚物填充的可交联硅烷封端的聚合物。 共聚物填充的可交联硅烷封端的聚合物是共聚物填充的多元醇和异氰酸酯封端的氢化硅烷化聚合物的反应产物。 异氰酸酯封端的氢化硅烷化聚合物是至少一种异氰酸酯和氢化硅烷化聚合物的反应产物。 氢化硅烷化聚合物是每个分子中具有至少一个不饱和基团和至少一个醇基团的聚合物的反应产物和在每个分子中具有氢 - 硅键和交联性甲硅烷基的化合物。 共聚物填充的可交联硅烷封端的聚合物在保持伸长性能的同时表现出改善的模量和拉伸强度性能。

    SILANE TERMINATED POLYMER FOR COATING, ADHESIVES, SEALANT AND ELASTOMER APPLICATIONS
    9.
    发明申请
    SILANE TERMINATED POLYMER FOR COATING, ADHESIVES, SEALANT AND ELASTOMER APPLICATIONS 有权
    用于涂料，胶粘剂，密封剂和弹性体应用的硅烷封端聚合物

    公开(公告)号：US20140309372A1

    公开(公告)日：2014-10-16

    申请号：US14113318

    申请日：2012-06-14

    申请人： Kamesh R. Vyakaranam ,  William A. Koonce ,  Ling Zhang ,  Jean-Luc Roser

    发明人： Kamesh R. Vyakaranam ,  William A. Koonce ,  Ling Zhang ,  Jean-Luc Roser

    IPC分类号： C08G81/02

    CPC分类号： C08G81/025 ,  C08G18/10 ,  C08G18/289 ,  C08G18/632 ,  C08G18/718 ,  C08G18/7621 ,  C08G18/63

    摘要： A copolymer-filled crosslinkable silane-terminated polymer having at least one crosslinkable silyl group in each molecule is provided. The copolymer-filled crosslinkable silane-terminated polymer is the reaction product of a copolymer-filled polyol and an isocyanate capped hydrosilylated polymer. The isocyanate capped hydrosilylated polymer is the reaction product of at least one isocyanate and a hydrosilylated polymer. The hydrosilylated polymer is the reaction product of a polymer having at least one unsaturated group and at least one alcoholic group in each molecule and a compound having a hydrogen-silicon bond and a crosslinkable silyl group in each molecule. The copolymer-filled crosslinkable silane-terminated polymers exhibit improved modulus and tensile strength properties while maintaining elongation properties.

    摘要翻译： 提供了在每个分子中具有至少一个可交联甲硅烷基的共聚物填充的可交联硅烷封端的聚合物。 共聚物填充的可交联硅烷封端的聚合物是共聚物填充的多元醇和异氰酸酯封端的氢化硅烷化聚合物的反应产物。 异氰酸酯封端的氢化硅烷化聚合物是至少一种异氰酸酯和氢化硅烷化聚合物的反应产物。 氢化硅烷化聚合物是每个分子中具有至少一个不饱和基团和至少一个醇基团的聚合物的反应产物和在每个分子中具有氢 - 硅键和交联性甲硅烷基的化合物。 共聚物填充的可交联硅烷封端的聚合物在保持伸长性能的同时表现出改善的模量和拉伸强度性能。