公开(公告)号：US5696407A

公开(公告)日：1997-12-09

申请号：US731174

申请日：1996-10-07

申请人： Klaus-Dieter Thiel ,  Herbert Heinisch

发明人： Klaus-Dieter Thiel ,  Herbert Heinisch

IPC分类号： C07C277/06 ,  C06B21/00 ,  C06B25/00 ,  C06B25/34 ,  C07C277/08 ,  C07C279/06 ,  C07C279/34

CPC分类号： C07C277/08 ,  C06B21/0091 ,  C06B25/34 ,  C07C279/34 ,  Y10S149/111

摘要： In the production of spherulitic nitroguanidine having a high bulk and tap ensity nitroguanidine is dissolved in dipolar, aprotic solvents, e.g. DMF, DMSO, NMP, etc., by heating to above the saturation temperature t.sub.s and the supersaturated solution is cooled with a controlled temperature gradient (.degree.C./min), crystallization being assisted by the addition of particulate, spherulitic material. In order to obtain spherical nitroguanidine with high yield in a continuous process and with mother liquor reuse, during the heating to above the saturation temperature t.sub.s, spherical control particles with a diameter of 5 to 500 .mu.m are regularly added to the solution in a quantity of 0.05 to 5.00 mass %. The particle size is chosen in such a way that, as a function of the solution behaviour of the nitroguanidine used and its concentration, on dropping below the saturation temperature spherical control particles are still present in the indicated quantity in the supersaturated solution.

摘要翻译： 在生产具有高体积和振实密度的球形硝基胍的情况下，将硝基胍溶解于偶极，非质子溶剂，例如， DMF，DMSO，NMP等，通过加热到饱和温度ts以上，过饱和溶液用受控的温度梯度（℃/ min）冷却，通过加入颗粒状球晶材料来辅助结晶。 为了在连续的方法中获得高产率的球形硝基胍，并且在母液再利用中，在加热到高于饱和温度ts之前，将一定直径为5至500μm的球形控制颗粒定量地添加到溶液中 为0.05〜5.00质量％。 选择粒径是这样一种方式：使用的硝基胍的溶液行为及其浓度随着饱和温度的降低而降低，球形控制颗粒在过饱和溶液中仍以指定量存在。

公开(公告)号：US5063036A

公开(公告)日：1991-11-05

申请号：US542059

申请日：1990-06-22

申请人： Walter Engel ,  Norbert Eisenreich ,  Klaus-Dieter Thiel

发明人： Walter Engel ,  Norbert Eisenreich ,  Klaus-Dieter Thiel

IPC分类号： C01C1/18 ,  C06B31/28

CPC分类号： C01C1/18 ,  C06B31/28

摘要： In a process for producing phase-stabilized ammonium nitrate (AN), a diammine complex of Ni or Cu is incorporated into the AN lattice, in which the diammine complex is produced in a solid-state reaction of AN and metal oxide at 110.degree. to 170.degree. C. and in a proportion of up to 10% is either mixed with further AN and melted, homogenized and subsequently transferred into the solid state, or mixed with further AN is incorporated into the AN lattice at between 80.degree. and 170.degree. C. in a solid-state reaction.

摘要翻译： 在生产相稳定化硝酸铵（AN）的方法中，将Ni或Cu的二氨基络合物引入到AN晶格中，其中在AN和金属氧化物的固相反应中，在110°至 170℃，并且至多10％的比例与另外的AN混合并熔化，均化并随后转移到固体状态，或者进一步混合AN在80-170℃下加入到AN晶格中 在固态反应中。

公开(公告)号：US20050145647A1

公开(公告)日：2005-07-07

申请号：US10502573

申请日：2003-01-21

申请人： Jochen Neutz ,  Klaus-Dieter Thiel ,  Franz Weller ,  Wilhelm Eckl ,  Norbert Eisenreich ,  Hans Ebeling

发明人： Jochen Neutz ,  Klaus-Dieter Thiel ,  Franz Weller ,  Wilhelm Eckl ,  Norbert Eisenreich ,  Hans Ebeling

IPC分类号： G08B15/02 ,  B67D5/00

CPC分类号： G08B15/02

摘要： The invention relates to a self-defence module comprising a housing containing a chamber that holds a free-flowing active medium and comprising a compressed gas source for spontaneously dispensing the active medium from the chamber. In order to be able to miniaturise the self-defence module, the compressed gas source is configured from a pyrotechnic gas generator and an ignition unit that interacts with the generator. According to the application, the ignition unit can be triggered manually or by a sensor. The invention also relates to the use of a self-defence module of this type for the protection of persons, buildings, means of transport or valuables.

摘要翻译： 本发明涉及一种自卫模块，其包括壳体，该壳体包含容纳自由流动活性介质的室，并且包括用于从腔室中自发分配活性介质的压缩气体源。 为了能够使自卫模块小型化，压缩气体源由烟火气体发生器和与发生器相互作用的点火单元构成。 根据应用，点火单元可以手动触发或由传感器触发。 本发明还涉及这种用于保护人，建筑物，运输工具或贵重物品的自卫模块的使用。