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公开(公告)号:US5430072A
公开(公告)日:1995-07-04
申请号:US87359
申请日:1993-07-08
申请人: Louis Muller , Tu Pham , Gabriel Verhelst
发明人: Louis Muller , Tu Pham , Gabriel Verhelst
IPC分类号: C08G18/08 , C08G18/10 , C08G18/48 , C08G18/70 , C08G18/72 , C08G18/76 , C08G101/00 , C08J9/02
CPC分类号: C08G18/7664 , C08G18/0895 , C08G18/10 , C08G18/4837 , C08G2101/0008 , C08G2101/005 , C08G2101/0058 , C08G2101/0083 , Y10S521/917
摘要: A method for the preparation of flexible polymeric foam by reacting a polyisocyanate component with an isocyanate-reactive component comprising at least 50% by weight of water, the polyisocyanate component comprising at least two polyisocyanate compositions, one of them being a low NCO isocyanate terminated prepolymer and the second being a high NCO polyisocyanate.
摘要翻译: 一种通过使多异氰酸酯组分与包含至少50重量%水的异氰酸酯反应性组分反应来制备柔性聚合物泡沫的方法,所述多异氰酸酯组分包含至少两种多异氰酸酯组合物,其中一种是低NCO异氰酸酯封端的预聚物 第二个是高NCO多异氰酸酯。
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公开(公告)号:US5070114A
公开(公告)日:1991-12-03
申请号:US508726
申请日:1990-04-16
申请人: Arun Watts , Louis Muller , Gabriel Verhelst , Mireille De Witte , Tu Pham , Alain Parfondry
发明人: Arun Watts , Louis Muller , Gabriel Verhelst , Mireille De Witte , Tu Pham , Alain Parfondry
IPC分类号: C08G18/10 , C08G18/48 , C08G18/76 , C08G101/00
CPC分类号: C08G18/4837 , C08G18/10 , C08G18/7664 , C08G2101/0008 , C08G2101/0083
摘要: The invention relates to a liquid isocyanate-containing prepolymer composition having an average isocyanate functionality greater than 2 and an NCO content of from 2 to 15% by weight, as obtainable by reacting an isocyanate reactive polymer having an average nominal functionality of from 2 to 6 with a stoichiometric excess of a diphenylmethane diisocyanate composition containing at least 2% by weight of 2,4'-diphenylmethane diisocyanate and having an average isocyanate functionality in the range from 2 to 2.3. The invention also relates to a method for preparing a polyurethane foam, which comprises reacting such a prepolymer composition with water.
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公开(公告)号:US5624972A
公开(公告)日:1997-04-29
申请号:US415456
申请日:1995-04-03
申请人: Louis Muller , Tu Pham , Gabriel Verhelst
发明人: Louis Muller , Tu Pham , Gabriel Verhelst
IPC分类号: C08G18/08 , C08G18/10 , C08G18/48 , C08G18/70 , C08G18/72 , C08G18/76 , C08G101/00 , C08J9/02
CPC分类号: C08G18/7664 , C08G18/0895 , C08G18/10 , C08G18/4837 , C08G2101/0008 , C08G2101/005 , C08G2101/0058 , C08G2101/0083 , Y10S521/917
摘要: A method for the preparation of flexible polymeric foam by reacting a polyisocyanate component with an isocyanate-reactive component comprising at least 50% by weight of water, the polyisocyanate component comprising at least two polyisocyanate compositions, one of them being a low NCO isocyanate terminated prepolymer and the second being a high NCO polyisocyanate.
摘要翻译: 一种通过使多异氰酸酯组分与包含至少50重量%水的异氰酸酯反应性组分反应来制备柔性聚合物泡沫的方法,所述多异氰酸酯组分包含至少两种多异氰酸酯组合物,其中一种是低NCO异氰酸酯封端的预聚物 第二个是高NCO多异氰酸酯。
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公开(公告)号:US5278274A
公开(公告)日:1994-01-11
申请号:US774768
申请日:1991-10-10
申请人: Gabriel Verhelst , Louis Muller , Alain Parfondry
发明人: Gabriel Verhelst , Louis Muller , Alain Parfondry
CPC分类号: C08G18/0895 , C08G18/10 , C08G18/7664 , C08G2101/0008 , C08G2101/005 , C08G2101/0083
摘要: A continuous process for the preparation of an isocyanate-terminated prepolymer having an NCO content in the range from 2 to 15% by weight, said process comprising the steps of:(A) continuously delivering to a reaction zone an organic polyisocyanate composition and an isocyanate reactive compound having an average molecular weight of at least 1000 the relative proportions of isocyanate composition and isocyanate reactive compound being appropriate for the formation of a prepolymer having an NCO content in the indicated range;(B) allowing the isocyanate composition and the isocyanate reactive compound to react in the reaction zone to form an isocyanate-terminated prepolymer, and(C) continuously removing the prepolymer from the reaction zone.
摘要翻译: 一种用于制备NCO含量在2至15重量%范围内的异氰酸酯封端的预聚物的连续方法,所述方法包括以下步骤:(A)连续地向反应区输送有机多异氰酸酯组合物和异氰酸酯 平均分子量为1000以上的反应性化合物,其特征在于,所述异氰酸酯组合物和异氰酸酯反应性化合物的相对比例适合于形成指定范围内NCO含量的预聚物; (B)使异氰酸酯组合物和异氰酸酯反应性化合物在反应区中反应形成异氰酸酯封端的预聚物,(C)从反应区连续除去预聚物。
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公开(公告)号:US5334689A
公开(公告)日:1994-08-02
申请号:US180740
申请日:1994-01-12
申请人: Louis Muller , Gabriel Verhelst
发明人: Louis Muller , Gabriel Verhelst
CPC分类号: C08G18/4804 , C08G18/12 , C08G2101/0008 , C08G2101/005 , C08G2101/0075 , C08G2101/0083
摘要: Process for preparing a flexible foam by reacting an isocyanate prepolymer having a free NCO content of 2-15% by weight, an isocyanate prepolymer having a free content of 25-31% by weight and an isocyanate-reactive composition comprising water.
摘要翻译: 通过使游离NCO含量为2-15重量%的异氰酸酯预聚物与游离含量为25-31重量%的异氰酸酯预聚物和包含水的异氰酸酯反应性组合物反应制备柔性泡沫的方法。
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公开(公告)号:US5270348A
公开(公告)日:1993-12-14
申请号:US48094
申请日:1993-04-12
申请人: Louis Muller , Gabriel Verhelst
发明人: Louis Muller , Gabriel Verhelst
IPC分类号: C08G18/10 , C08G18/12 , C08G18/48 , C08G101/00 , C08G18/14
CPC分类号: C08G18/4804 , C08G18/12 , C08G2101/0008 , C08G2101/005 , C08G2101/0075 , C08G2101/0083
摘要: Process for preparing a flexible foam by reacting an isocyanate prepolymer having a free NCO content of 2-15% by weight, an isocyanate prepolymer having a free content of 25-31% by weight and an isocyanate-reactive composition comprising water.
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公开(公告)号:US4910231A
公开(公告)日:1990-03-20
申请号:US247467
申请日:1988-09-21
申请人: Tu Pham , Louis Muller
发明人: Tu Pham , Louis Muller
CPC分类号: C08G18/48 , C08G18/08 , C08G18/5024 , C08G18/727 , C08G18/7664 , C08G18/78 , C08G2101/0008 , C08G2101/005 , C08G2101/0075 , C08G2101/0083
摘要: Substantially water blown flexible polyurethane foams, based on methylene diphenyl isocyanates, having a density ranging from 15-45 kg/m.sup.3.Such foams may be obtained through a process substantially avoiding halocarbon blowing agents, which comprises reacting methylene diphenyl isocyanates with water and one or more isocyanate-reactive compounds selected from polyols and polyamines with a functionality of 2-4 and an average equivalent weight ranging from 750-5000, while the isocyanate index ranges from 10 to 60, and weight ratio of the isocyanate-reactive compound(s) to water is less than 20.
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公开(公告)号:US4916168A
公开(公告)日:1990-04-10
申请号:US247453
申请日:1988-09-21
申请人: Tu Pham , Louis Muller
发明人: Tu Pham , Louis Muller
CPC分类号: C08G18/7664 , C08G18/7806 , C08G18/79 , C08G2101/0008 , C08G2101/0041 , C08G2101/0075 , C08G2101/0083
摘要: Flexible polyurethane foam based on methylene diphenyl isocyanates and isocyanate-reactive compounds selected from polyols and polyamines, for which the ratio of the density expressed in kg/m.sup.3 to the compression hardness at 40% compression, expressed in kPa, has a value of at least 20.Such foams may be obtained through a process which comprises reacting methylene diphenyl isocyanates with one or more isocyanate-reactive compounds selected from polyols and polyamines with a functionality of 2-4 and an average equivalent weight ranging from 750-5000 and from 0 to 5 parts by weight of water per 100 parts of polyols and/or polyamine, optionally together with additives conventional in the art, and optionally together with blowing agents other than water, whereas the isocyanate index ranges from 10 to 60.
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公开(公告)号:US5043360A
公开(公告)日:1991-08-27
申请号:US456737
申请日:1989-12-26
申请人: Tu Pham , Louis Muller
发明人: Tu Pham , Louis Muller
CPC分类号: C08G18/48 , C08G18/08 , C08G18/5024 , C08G18/727 , C08G18/7664 , C08G18/78 , C08G2101/0008 , C08G2101/005 , C08G2101/0075 , C08G2101/0083
摘要: Substantially water blown flexible polyurethane foams, based on methylene diphenyl isocyanates, having a density ranging from 15-45 kg/m.sup.3. Such foams may be obtained through a process substantially avoiding halocarbon blowing agents, which comprises reacting methylene diphenyl isocyanates with water and one or more isocyanate-reactive compounds selected from polyols and polyamines with a functionality of 2-4 and an average equivalent weight ranging from 750-5000, while the isocyanate index ranges from 10 to 60, and weight ratio of the isocyanate-reactive compound(s) to water is less than 20.
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公开(公告)号:US06387972B1
公开(公告)日:2002-05-14
申请号:US09784546
申请日:2001-02-15
申请人: Hassan El Ghobary , Louis Muller
发明人: Hassan El Ghobary , Louis Muller
IPC分类号: C08J900
CPC分类号: C08G18/1825 , C08G18/089 , C08G18/4072 , C08G18/7664 , C08G2101/0008 , C08G2101/005 , C08G2101/0083
摘要: An improved process to enhance polyurethane foam performance is described. Polyurethane foam is prepared by reactions between a polyisocyanate and a polyfunctional isocyanate-reactive component wherein said reactions are conducted in the presence of catalysts composed of (a) a specific reactive tertiary amine compound selected from the group consisting of bis(dimethylaminopropyl)amino-2-propanol, bis(dimethylaminopropyl)amine, dimethylaminopropyldipropanolamine, bis(dimethylamino)-2-propanol, N,N,N′-trimethyl-N′-hydroxyethyl-bis(aminoethyl)ether and mixtures thereof; and (b) at least one carboxylic acid salt of the specific reactive tertiary amine compound selected from the group consisting of hydroxy-carboxylic acid salts and halo-carboxylic acid salts.
摘要翻译: 描述了改进聚氨酯泡沫性能的改进方法。 通过多异氰酸酯和多官能异氰酸酯反应性成分之间的反应制备聚氨酯泡沫,其中所述反应在催化剂存在下进行,所述催化剂由(a)选自二(二甲基氨基丙基)氨基-2 - 丙醇,双(二甲基氨基丙基)胺,二甲基氨基丙基二丙醇胺,双(二甲基氨基)-2-丙醇,N,N,N'-三甲基-N'-羟乙基 - 双(氨基乙基)醚及其混合物; 和(b)至少一种选自羟基羧酸盐和卤代羧酸盐的比活性叔胺化合物的羧酸盐。
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