Apparatus for measuring temperatures in tubular reactors
    9.
    发明授权
    Apparatus for measuring temperatures in tubular reactors 失效
    用于测量管式反应器中的温度的装置

    公开(公告)号:US06333011B1

    公开(公告)日:2001-12-25

    申请号:US09064310

    申请日:1998-04-23

    IPC分类号: B01J806

    摘要: A reactor apparatus comprises at least two same-type tubular reactors which are filled with solid particles, at least one tubular reactor containing a temperature measuring unit, the tubular reactors being designed such that both the ratio of the mass of the solid particles to the free cross-sectional area of the respective tubular reactor and the pressure drop measured by an inert gas being conducted transversely to the free cross-sectional area are identical across the respective tubular reactor. The apparatus is suitable for treating fluid masses while generating or consuming thermal energy, the temperature being measured.

    摘要翻译: 反应器装置包括填充有固体颗粒的至少两个相同类型的管式反应器,至少一个包含温度测量单元的管状反应器,该管式反应器设计成使得固体颗粒的质量与自由 各管式反应器的横截面面积和通过横向于自由横截面积进行的惰性气体测量的压降在相应的管式反应器中是相同的。 该装置适用于在产生或消耗热能,待测温度的同时处理流体物质。

    Separation by rectification of unsaturated carboxylic acids from solvents
    10.
    发明授权
    Separation by rectification of unsaturated carboxylic acids from solvents 失效
    通过不饱和羧酸从溶剂中的精馏分离

    公开(公告)号:US5728272A

    公开(公告)日:1998-03-17

    申请号:US696193

    申请日:1996-08-13

    CPC分类号: C07C51/44 Y10S203/22

    摘要: In a process for the separation by rectification of unsaturated carboxylic acids from solvents in which the acids were absorbed after the synthesis reaction, the rectification is briefly interrupted and the rectification column is flushed with a basic solution. The interruption is carried out at regular time intervals. The basic solution used is an aqueous solution of alkali metal and/or alkaline earth metal hydroxide, preferably NaOH, KOH, Ca(OH).sub.2 or their anhydrous oxides; alkaline polar organic solvents as amines or amides can be used, too.

    摘要翻译: 在由合成反应后吸收酸的溶剂中分离不饱和羧酸的方法中,精馏被短暂中断,精馏塔用碱性溶液冲洗。 中断是以规律的时间间隔进行的。 使用的碱性溶液是碱金属和/或碱土金属氢氧化物,优选NaOH,KOH,Ca(OH)2或其无水氧化物的水溶液; 也可以使用作为胺或酰胺的碱性极性有机溶剂。