-
公开(公告)号：US06214962B1
公开(公告)日：2001-04-10
申请号：US09453467
申请日：1999-12-02
申请人： Masaharu Takahashi , Yutaka Hagiwara , Minoru Igarashi , Keiji Shibata , Kenji Tawara , Yoshio Tomizawa
发明人： Masaharu Takahashi , Yutaka Hagiwara , Minoru Igarashi , Keiji Shibata , Kenji Tawara , Yoshio Tomizawa
IPC分类号： B29B700
摘要： An organopolysiloxane gum is continuously prepared by (I) mixing at least one cyclopolysiloxane with an end capping agent, (II) feeding the mixture to a self-cleaning reactor along with a polymerization catalyst of thermal decomposition type, and effecting polymerization at a temperature of 80-130° C., (III) heating the reaction mixture of step (II) at a temperature of 130-200° C. under subatmospheric pressure for deactivating the catalyst, thereby terminating the polymerization reaction, and (IV) continuously removing the cyclopolysiloxane and volatile components from the reaction product.
摘要翻译： 通过（I）将至少一种环状聚硅氧烷与封端剂混合来连续制备有机聚硅氧烷胶，（II）将该混合物与热分解型聚合催化剂一起进料至自清洁反应器，并在 80-130℃，（III）在低于大气压下在130-200℃的温度下加热步骤（II）的反应混合物以使催化剂失活，从而终止聚合反应，和（IV）连续除去 环聚硅氧烷和来自反应产物的挥发性组分。
-
公开(公告)号：US06288195B1
公开(公告)日：2001-09-11
申请号：US09453465
申请日：1999-12-02
IPC分类号： C08G7708
摘要： An organopolysiloxane gum is prepared by polymerizing a cyclic organopolysiloxane with a low molecular weight linear organopolysiloxane end-blocked with a triorganosilyl group in the presence of a thermally decomposable catalyst. After the polymerization reaction, the catalyst is deactivated by heating the reaction product under a subatmospheric pressure of typically up to 500 mmHg.
摘要翻译： 通过在可热分解的催化剂的存在下，用三有机甲硅烷基封端的低分子线性有机聚硅氧烷聚合环状有机聚硅氧烷来制备有机聚硅氧烷胶。 在聚合反应之后，通常在典型地高达500mmHg的低于大气压的压力下加热反应产物使催化剂失活。
-
公开(公告)号：US06177506B1
公开(公告)日：2001-01-23
申请号：US09148502
申请日：1998-09-04
IPC分类号： C08K336
CPC分类号： C08L83/04 , B29B7/7495 , B29C47/40 , B29C47/822 , C08G77/16 , C08G77/20 , C08G77/24 , C08G77/26 , C08G77/70 , C08K3/36 , C08L83/00 , C08L2666/54 , C08L2666/44
摘要： In a first step, basic components including (A) 100 parts by weight of an organopolysiloxane gum, (B) 5-100 parts by weight of a reinforcing silica filler, and (C) 0.1-30 parts by weight of a processing aid are fed batchwise to a closed mixer for mixing them until uniform. In a second step, the mixture is continuously fed into a kneader/extruder for heat treating. The first step achieves quick dispersion and cooperates with the second step for the efficient production of a heat-curable silicone rubber compound.
摘要翻译： 在第一步中，包括（A）100重量份有机聚硅氧烷胶，（B）5-100重量份增强二氧化硅填料和（C）0.1-30重量份加工助剂的基础组分是 分批进料到密闭混合器中以混合它们直到均匀。 在第二步中，将混合物连续进料到用于热处理的捏合机/挤出机中。 第一步实现快速分散，与第二步合作，有效地生产可热固化的硅橡胶化合物。
-
公开(公告)号：US6001917A
公开(公告)日：1999-12-14
申请号：US109967
申请日：1998-06-27
摘要： In a first step, basic components including (A) 100 parts by weight of an organopolysiloxane gum, (B) 5-100 parts by weight of a reinforcing silica filler, and (C) 0.1-30 parts by weight of a processing aid are fed batchwise to a closed mixer for mixing them at a temperature of room temperature to 150.degree. C. In a second step, the mixture is fed into a kneader/mixer for heat treating at a temperature of 150-250.degree. C. The first step achieves quick dispersion and cooperates with the second step to form a heat-curable silicone rubber compound in an efficient manner.
摘要翻译： 在第一步中，包括（A）100重量份有机聚硅氧烷胶，（B）5-100重量份增强二氧化硅填料和（C）0.1-30重量份加工助剂的基础组分是 在室温至150℃的温度下分批进料至密闭混合器中混合。在第二步中，将混合物进料到捏合机/混合器中，在150-250℃的温度下进行热处理。第一步 实现快速分散，并与第二步配合，以有效的方式形成可热固化的硅橡胶。
-
公开(公告)号：US06339124B1
公开(公告)日：2002-01-15
申请号：US09592418
申请日：2000-06-12
申请人： Minoru Igarashi , Yutaka Hagiwara
发明人： Minoru Igarashi , Yutaka Hagiwara
IPC分类号： C08K336
CPC分类号： C08L83/04 , C08G77/12 , C08G77/16 , C08G77/18 , C08G77/20 , C08G77/24 , C08G77/26 , C08G77/70 , C08L2666/44 , C08L2666/54 , C08L83/00
摘要： A silicone rubber composition comprising an organopolysiloxane containing at least two alkenyl radicals and having a degree of polymerization of at least 100, an organopolysiloxane or organosilane, reinforcing silica, and an alkali metal salt of phosphoric acid has minimized plasticity recovery with time and improved storage stability and cures with an organic peroxide or addition reaction curing agent into a silicone rubber having improved compression set and yellowing resistance.
摘要翻译： 包含含有至少两个烯基并且聚合度至少为100的有机聚硅氧烷，有机聚硅氧烷或有机硅烷，增强二氧化硅和磷酸碱金属盐的硅橡胶组合物具有随时间降低的可塑性恢复和改善的储存稳定性 并用有机过氧化物或加成反应固化剂固化成具有改进的压缩永久变形和耐黄变性的硅橡胶。
-
6.发明授权公开(公告)号：US08754160B2
公开(公告)日：2014-06-17
申请号：US13457828
申请日：2012-04-27
申请人： Yutaka Hagiwara , Minoru Igarashi
发明人： Yutaka Hagiwara , Minoru Igarashi
CPC分类号： C08J3/24 , C08J2383/04 , C08K3/36 , C08K5/5419 , C08L83/04
摘要： A method for producing a silicone rubber compound in a reduced blending time, and which imparts excellent resistance to plasticity reversion and the cured silicone rubber prepared without heat treatment has excellent resistance to compression set. (A) an organopolysiloxane with polymerization degree of at least 100 represented by the following average compositional formula (I): R1aSiO(4-a)/2 (I) (R1: a substituted or unsubstituted monovalent hydrocarbon group, a: 1.95 to 2.05), (B) a reinforcing silica having a specific surface area (BET) of at least 50 m2/g, and (C) a preliminary hydrolysis product of (C-1) an alkoxysilane represented by the following formula (II): R2mSi(OR3)4-m (II) (R2: hydrogen atom or a substituted or unsubstituted monovalent hydrocarbon group, R3: a substituted or unsubstituted alkyl group, m: 0, 1, 2, or 3), and (C-2) water at a molar amount 0.3 to 5 times the alkoxy group in the alkoxysilane of component (C-1) are mixed and heated.
摘要翻译： 缩短混合时间制造硅橡胶化合物的方法，具有优异的耐回缩性和不经热处理制备的固化的硅橡胶具有优异的耐压缩变形性。 （A）由以下平均组成式（I）表示的聚合度为至少100的有机聚硅氧烷：R1aSiO（4-a）/ 2（I）（R1：取代或未取代的单价烃基，a：1.95〜2.05 ），（B）比表面积（BET）为50m 2 / g以上的增强二氧化硅，（C）由下式（II）表示的（C-1）烷氧基硅烷的预水解产物：R2mSi （OR 3）4-m（II）（R 2：氢原子或取代或未取代的一价烃基，R 3：取代或未取代的烷基，m：0,1,2或3）和（C-2） 将组分（C-1）的烷氧基硅烷中的烷氧基的摩尔量为0.3至5倍的水混合并加热。
-
7.发明申请METHOD FOR PRODUCING SILICONE RUBBER COMPOUND AND SILICONE RUBBER COMPOSITION 审中-公开生产硅橡胶化合物和硅橡胶组合物的方法公开(公告)号：US20120277362A1
公开(公告)日：2012-11-01
申请号：US13458845
申请日：2012-04-27
申请人： Minoru IGARASHI , Yutaka Hagiwara
发明人： Minoru IGARASHI , Yutaka Hagiwara
IPC分类号： C08K3/34
CPC分类号： C08J3/24 , C08G77/20 , C08J2383/04 , C08K3/36 , C08K5/5419 , C08L83/04
摘要： A method for producing a silicone rubber compound in a reduced blending time and which imparts excellent resistance to plasticity reversion, and the cured silicone rubber prepared without heat treatment has excellent resistance to compression set. The method comprises mixing components: (A) an organopolysiloxane having a polymerization degree of at least 100 represented by the following average compositional formula (I): R1aSiO(4−a)/2 (I) wherein R1 is independently a substituted or unsubstituted monovalent hydrocarbon group, and a is 1.95 to 2.05; (B) a reinforcing silica having a specific surface area as measured by BET absorption method of at least 50 m2/g, (C) an alkoxysilane represented by the following formula (II): R2mSi(OR3)4−m (II) wherein R2 is independently hydrogen atom or a substituted or unsubstituted monovalent hydrocarbon group, R3 is independently a substituted or unsubstituted alkyl group, and m is 0, 1, 2, or 3, and (D) water, and the heat treatment.
摘要翻译： 一种缩短混合时间制备硅橡胶化合物的方法，其具有优异的耐回缩性，并且不经热处理制备的固化的硅橡胶具有优异的耐压缩变形性。 该方法包括混合组分：（A）聚合度为至少为100的由以下平均组成式（I）表示的聚合度的有机聚硅氧烷：R1aSiO（4-a）/ 2（I）其中R1独立地为取代或未取代的单价 烃基，a为1.95〜2.05; （B）通过BET吸收法测定的比表面积为至少50m 2 / g的增强二氧化硅，（C）由下式（II）表示的烷氧基硅烷：R2mSi（OR3）4-m（II）其中 R2独立地为氢原子或取代或未取代的单价烃基，R3独立地为取代或未取代的烷基，m为0,1,2或3，（D）水和热处理。
-
公开(公告)号：US06288196B1
公开(公告)日：2001-09-11
申请号：US09453468
申请日：1999-12-02
IPC分类号： B29B700
摘要： An organopolysiloxane gum is continuously prepared by (I) mixing at least one cyclopolysiloxane with an end capping agent, (II) feeding the mixture to a self-cleaning reactor along with an alkaline polymerization catalyst, and effecting polymerization at a temperature of 100 to 250° C. and under subatmospheric pressure, (III) continuously adding a neutralizing agent to the reaction mixture of step (II), thereby terminating the polymerization reaction, and (IV) continuously removing the cyclopolysiloxane and volatile components from the reaction mixture.
摘要翻译： 通过（I）将至少一种环状聚硅氧烷与封端剂混合来连续制备有机聚硅氧烷胶，（II）将该混合物与碱性聚合催化剂一起进料到自清洁反应器中，并在100-250℃的温度下进行聚合 ℃，并且在低于大气压的压力下，（III）向步骤（II）的反应混合物中连续加入中和剂，从而终止聚合反应，和（IV）从反应混合物中连续除去环状聚硅氧烷和挥发性组分。
-
公开(公告)号：US07114394B2
公开(公告)日：2006-10-03
申请号：US11022675
申请日：2004-12-28
申请人： Mayumi Fukuyama , Takao Konno , Kazuhiro Umekita , Yoshihiro Dozono , Toshihiko Horiuchi , Michiya Sakai , Yutaka Hagiwara , Keizo Ohtomo
发明人： Mayumi Fukuyama , Takao Konno , Kazuhiro Umekita , Yoshihiro Dozono , Toshihiko Horiuchi , Michiya Sakai , Yutaka Hagiwara , Keizo Ohtomo
CPC分类号： G01N29/4418 , G01N29/045 , G01N2291/02491
摘要： A vibration test system for structures comprises a vibration exciter that vibrates a real model portion, a load meter that measures a load, and a computer that receives a numerical model representing a numerical model portion. The computer includes a block that calculates a displacement, which is made in a predetermined time after completion of measurement, according to a load value and an external force value. A signal production block produces a command signal using as a target value the displacement calculated by the displacement calculation block. A step control block controls the displacement calculation block and signal production block so that they will act cyclically. The displacement calculation block uses an αOS method to time integrate a solution of a vibrational equation.
摘要翻译： 用于结构的振动测试系统包括振动实际模型部分的振动激励器，测量负载的负载计量器和接收表示数字模型部分的数值模型的计算机。 计算机包括根据负载值和外力值计算在完成测量之后的预定时间内的位移的块。 信号产生块产生使用由位移计算块计算的位移作为目标值的命令信号。 步进控制块控制位移计算块和信号产生块，使它们周期性地起作用。 位移计算块使用αOS方法来对振动方程的解进行时间积分。
-
10.发明授权公开(公告)号：US08460798B2
公开(公告)日：2013-06-11
申请号：US12610197
申请日：2009-10-30
申请人： Muneo Ishida , Yutaka Hagiwara
发明人： Muneo Ishida , Yutaka Hagiwara
IPC分类号： B32B21/04
CPC分类号： G10C9/00 , G10D1/005 , Y10T428/31989
摘要： A wood member for a musical instrument, which is capable of preventing occurrence of damage, such as cracking, to thereby ensure smooth and stable operation of the musical instrument and maintain excellent appearance of the same over a long time period. The wood member has compressive internal stress remaining at least in an outer peripheral portion thereof by being subjected to heating processing, cooling processing, and moisture conditioning processing, in advance. A wood workpiece as a workpiece for the wood member is heated at a predetermined temperature, and the heated wood workpiece is cooled. The cooled wood workpiece is subjected to moisture conditioning such that compressive internal stress is generated at least in an outer peripheral portion of the wood workpiece.
摘要翻译： 一种用于乐器的木构件，其能够防止诸如破裂的损坏的发生，从而确保乐器的平稳和稳定的操作并且在长时间内保持其良好的外观。 预先通过进行加热处理，冷却处理和湿度调节处理，至少在其外周部分残留有内部应力。 作为木质构件的工件的木材工件在预定温度下被加热，并且加热的木材工件被冷却。 冷却的木工件经受湿度调节，使得至少在木工件的外周部分产生压缩内应力。
-
-
-
-
-
-
-
-
-
搜索结果
20 条记录 (耗时 0.023 秒)