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    Dimer diol (meth)acrylates uses as a matting agent
    1.
    发明申请
    Dimer diol (meth)acrylates uses as a matting agent 审中-公开
    二聚二醇（甲基）丙烯酸酯用作消光剂

    公开(公告)号：US20070173593A1

    公开(公告)日：2007-07-26

    申请号：US10553183

    申请日：2004-04-08

    申请人： Matthias Fies ,  Holger Endres ,  Jan-Mirco Stachowiak ,  Ronald Klagge

    发明人： Matthias Fies ,  Holger Endres ,  Jan-Mirco Stachowiak ,  Ronald Klagge

    IPC分类号： C08L31/00

    CPC分类号： C09D7/42

    摘要： A new flatting agent for self-curing or radiation-curing coating systems is disclosed. The flatting agent is a liquid dimerdiol (meth)acrylate with a degree of esterification of at least 50%. The dimerdiol (meth)acrylate ester is introduced into the coating system in an amount of 1-25% by weight based on the coating system as a whole. The coating system can have additional solid flatting agents in the system.

    摘要翻译： 公开了一种用于自固化或辐射固化涂料体系的新型压平剂。 该消光剂是酯化度至少为50％的液体二聚二醇（甲基）丙烯酸酯。 基于涂料体系整体，将二聚二醇（甲基）丙烯酸酯酯以1-25重量％的量引入涂料体系中。 涂层系统可以在系统中具有附加的固体平整剂。

    Radiation-cured substances
    2.
    发明申请
    Radiation-cured substances 审中-公开
    辐射固化物质

    公开(公告)号：US20070167645A1

    公开(公告)日：2007-07-19

    申请号：US10553483

    申请日：2004-04-08

    申请人： Matthias Fies ,  Holger Endres ,  Jan-Mirco Stachowiak ,  Ronald Klagge

    发明人： Matthias Fies ,  Holger Endres ,  Jan-Mirco Stachowiak ,  Ronald Klagge

    IPC分类号： C07C69/52

    CPC分类号： G03F7/027 ,  C08G63/47 ,  C08G65/2615 ,  C08L63/00 ,  C08L71/02 ,  C08L2666/02

    摘要： The disclosed invention relates to mixtures of acrylic or methacrylic compounds containing 1 to 35% by weight and, more particularly, 5 to 25% by weight epoxy (meth)acrylates, based on the total quantity of acrylic or methacrylic compounds, the mixture being obtainable by a process comprising the following steps: a) esterifying hydroxyl compounds with acrylic acid and/or methacrylic acid, b) optionally adding more acrylic acid and/or methacrylic acid and c) reacting the excess acrylic acid and/or methacrylic acid with epoxides in the presence of the esterification product of a). Said mixtures are suitable for use as radiation-curable compositions for coating systems, such as paints, coating compositions and the like.

    摘要翻译： 所公开的本发明涉及基于丙烯酸或甲基丙烯酸酯化合物的总量，含有1至35重量％，更特别为5至25重量％的环氧（甲基）丙烯酸酯的丙烯酸或甲基丙烯酸酯化合物的混合物，所述混合物可获得 通过包括以下步骤的方法：a）用丙烯酸和/或甲基丙烯酸酯化羟基化合物，b）任选地加入更多的丙烯酸和/或甲基丙烯酸，和c）使过量的丙烯酸和/或甲基丙烯酸与环氧化物反应 a）的酯化产物的存在。 所述混合物适合用作涂料体系的辐射固化组合物，例如涂料，涂料组合物等。

    Monitoring the stability of vinylog compounds
    3.
    发明申请
    Monitoring the stability of vinylog compounds 审中-公开
    监测vinylog化合物的稳定性

    公开(公告)号：US20060019401A1

    公开(公告)日：2006-01-26

    申请号：US10523278

    申请日：2003-07-24

    申请人： Matthias Fies ,  Ronald Klagge ,  Jan Stachowiak

    发明人： Matthias Fies ,  Ronald Klagge ,  Jan Stachowiak

    IPC分类号： G01N33/00

    CPC分类号： C07C67/08 ,  B01J19/002 ,  B01J2219/00186 ,  B01J2219/002 ,  B01J2219/00213 ,  B01J2219/00231 ,  B01J2219/00254 ,  B01J2219/00268 ,  B01J2219/00272 ,  C07C67/62 ,  G01N21/3504 ,  G01N27/404 ,  Y10T436/201666 ,  C07C69/54

    摘要： The process is used to monitor the stability of compositions and reaction mixtures which contain vinylog compounds, more especially (meth)acrylic acid and/or (meth)acrylates. The content of dissolved oxygen in the composition or in the reaction mixture is determined and compared with predetermined reference values. Incipient or threatening polymerization is detected as early as possible and well before polymerization actually begins. Monitoring can be carried out simply, inexpensively and, in particular, safely both during storage and transportation and during the course of reactions, more particularly during the esterification of (meth)acrylic acid with mono- or polyhydric alcohols.

    摘要翻译： 该方法用于监测含有维林格化合物，更特别是（甲基）丙烯酸和/或（甲基）丙烯酸酯的组合物和反应混合物的稳定性。 确定组合物或反应混合物中溶解氧的含量并与预定的参考值进行比较。 在聚合实际开始之前，尽可能早地检测到初始或威胁性聚合。 特别是在（甲基）丙烯酸与一元醇或多元醇的酯化反应过程中，尤其是在储存和运输过程中以及反应过程中，特别是安全地进行监测。

    Ionic N-Containing Compounds
    5.
    发明申请
    Ionic N-Containing Compounds 审中-公开
    离子含氮化合物

    公开(公告)号：US20100179260A1

    公开(公告)日：2010-07-15

    申请号：US12665816

    申请日：2008-06-12

    申请人： Stefan Busch ,  Paul Birnbrich ,  Joachim Meyer ,  Ronald Klagge

    发明人： Stefan Busch ,  Paul Birnbrich ,  Joachim Meyer ,  Ronald Klagge

    IPC分类号： C08K5/3445 ,  C07D233/06

    CPC分类号： C07D233/10 ,  B01F17/0042 ,  C08F2/28

    摘要： Ionic N-containing compounds of formula (I), wherein the index n is the number 0 or 1 and R1 to R5 independently are hydrogen, C1-C25 alkyl, C3-C25 cycloalkyl or C6-C25 aryl, wherein the alkyl groups can be saturated or unsaturated, straight-chained or branched, and the cycloalkyl groups can be saturated or unsaturated, with the following stipulations: (1) when n=1, at least one of R1 to R5 must contain 8 to 25 carbon atoms, (2) when n=0, at least one of R1, R2, R3 and R5 must contain 8 to 25 carbon atoms, (3) the carbon atoms carrying R2 and R3 are linked via a C—C single bond or a C═C double bond, (4) when R1 to R5 are alkyl or cycloalkyl, a hydrogen atom linked to a carbon atom can be replaced with OH or NH2, or an —O—, —COO— or —NH— group can be inserted between two neighboring carbon atoms linked via a C—C single bond, (5) when R1 to R5 are aryl, a hydrogen atom linked to a carbon atom can be optionally replaced with C1-C12 alkyl or C3-C12 cycloalkyl, with the stipulation that the following applies to the alkyl or cycloalkyl group: optionally a hydrogen atom linked to a carbon atom can be replaced with OH or NH2, or an —O—, —COO— or —NH— group can be inserted between two neighboring carbon atoms linked via a C—C-single bond; said compounds being suitable as temporary surfactants, particularly for the production of aqueous emulsions or dispersions.

    摘要翻译： 式（I）的离子型含N的化合物，其中指数n为数字0或1且R 1至R 5独立地为氢，C 1 -C 25烷基，C 3 -C 25环烷基或C 6 -C 25芳基，​​其中烷基可以 饱和或不饱和的直链或支链，并且环烷基可以是饱和或不饱和的，具有以下规定：（1）当n = 1时，R 1至R 5中的至少一个必须含有8至25个碳原子，（2 ）当n = 0时，R 1，R 2，R 3和R 5中的至少一个必须含有8至25个碳原子，（3）携带R2和R3的碳原子通过C-C单键或C = C双键连接 键，（4）当R 1至R 5为烷基或环烷基时，与碳原子连接的氢原子可以被OH或NH 2取代，或者可以在两个邻位之间插入-O-，-COO-或-NH-基团 通过C-C单键连接的碳原子，（5）当R 1至R 5为芳基时，与碳原子连接的氢原子可任选被C 1 -C 12烷基或C 3 -C 12环烷基取代，与st 以下适用于烷基或环烷基：任选地，与碳原子连接的氢原子可以被OH或NH 2代替，或者可以在两个相邻碳之间插入-O-，-COO-或-NH-基团 通过C-C单键连接的原子; 所述化合物适合作为临时表面活性剂，特别是用于生产水性乳液或分散体。

    Copolymerizable surfactants (1)
    6.
    发明授权
    Copolymerizable surfactants (1) 有权
    可共聚表面活性剂（1）

    公开(公告)号：US08183320B2

    公开(公告)日：2012-05-22

    申请号：US12824394

    申请日：2010-06-28

    申请人： Ronald Klagge ,  Uwe Held ,  Thomas Mausberg ,  Katharina Hömberg ,  Thomas Schliwka

    发明人： Ronald Klagge ,  Uwe Held ,  Thomas Mausberg ,  Katharina Hömberg ,  Thomas Schliwka

    IPC分类号： C08L31/06

    CPC分类号： C08F2/24 ,  C08F222/20

    摘要： The invention is directed to the use of maleic esters selected from compounds of formulae (I), (II) and (III), as copolymerizable emulsifiers in the emulsion polymerization of olefinically unsaturated monomers, in which A is a C3-C40 alkyl group; X, Y and Z independently are hydrogen or methyl; B and D independently are sulfate, phosphate or hydrogen; n and p independently are numbers in the range from 0 to 40; and m is a number in the range from 2 to 40.

    摘要翻译： 本发明涉及在烯属不饱和单体的乳液聚合中使用选自式（I），（II）和（III）的化合物的马来酸酯作为可共聚的乳化剂，其中A为C 3 -C 40烷基; X，Y和Z独立地是氢或甲基; B和D独立地是硫酸根，磷酸根或氢原子; n和p独立地为0至40的数字; m为2〜40的数。

    Use Of Nonionic Surfactants As Emulsifiers For Emulsion Polymerization (III)
    7.
    发明申请
    Use Of Nonionic Surfactants As Emulsifiers For Emulsion Polymerization (III) 失效
    用作乳液聚合乳化剂的非离子表面活性剂（III）

    公开(公告)号：US20120029131A1

    公开(公告)日：2012-02-02

    申请号：US13259846

    申请日：2010-03-13

    申请人： Markus Scherer ,  Thomas Schliwka ,  Katharina Hömberg ,  Uwe Held ,  Thomas Mausberg ,  Ronald Klagge

    发明人： Markus Scherer ,  Thomas Schliwka ,  Katharina Hömberg ,  Uwe Held ,  Thomas Mausberg ,  Ronald Klagge

    IPC分类号： C08K9/04 ,  C08L9/10 ,  C08L13/02 ,  C08L19/02

    CPC分类号： C08F2/30

    摘要： The invention relates to the use of aqueous solutions of nonionic surfactants as gel phase free emulator systems for the emulsion polymerization, wherein said nonionic surfactants are chosen from the group (a) of the addition products from 1 to 40 mol ethylene and/or propylene oxide per mol of allyl alcohol, and (b) of the addition products from 1 to 40 mol ethylene and/or propylene oxide per mol of allyl alcohol, wherein the OH-group of said addition products is end-capped in the sense that it is substituted by a group OR, wherein R is an alkyl group with 1 to 20 C-atoms, which can be saturated or unsaturated, straight chained or branched.

    摘要翻译： 本发明涉及非离子表面活性剂的水溶液用作乳液聚合的无凝胶相模拟器系统，其中所述非离子表面活性剂选自1-40mol乙烯和/或环氧丙烷加成产物（a）组 每摩尔烯丙醇，和（b）每摩尔烯丙醇1至40摩尔乙烯和/或环氧丙烷的加成产物，其中所述加成产物的OH-基是在上述意义上被封端 被OR取代，其中R是具有1-20个碳原子的烷基，其可以是饱和或不饱和的，直链或支链的。

    Low-viscosity aqueous compositions
    9.
    发明授权
    Low-viscosity aqueous compositions 失效
    低粘度水性组合物

    公开(公告)号：US08519071B2

    公开(公告)日：2013-08-27

    申请号：US13298468

    申请日：2011-11-17

    申请人： Thomas Schliwka ,  Ronald Klagge ,  Uwe Held ,  Thomas Mausberg

    发明人： Thomas Schliwka ,  Ronald Klagge ,  Uwe Held ,  Thomas Mausberg

    IPC分类号： C08F2/00 ,  C08F210/00 ,  C08F20/06 ,  C08F118/02 ,  B01F3/08

    CPC分类号： C08F2/26 ,  C08F212/08 ,  C08F218/08 ,  C08F218/10 ,  C08F220/06 ,  C08F2220/1825 ,  C08F220/14

    摘要： Provided are low-viscosity aqueous compositions comprising compounds of Formula (III) and (IV). These compositions are prepared by jointly ethoxylating a mixture of the compounds of the Formula (I) and (II) to give an intermediate which represents a mixture of compounds of Formulas (I*) and (II*). The intermediate is then converted by sulfation or phosphation and subsequent neutralization, into an aqueous composition comprising the compounds of Formula (III) and (IV). The aqueous compositions are notable for having, at 20° C., a Brookfield viscosity of 3000 mPas or less (measured at 20° C. with spindle 2 and 20 rpm), and are suitable as emulsifiers for emulsion polymerization.

    摘要翻译： 提供包含式（III）和（IV）的化合物的低粘度水性组合物。 这些组合物通过将式（I）和（II）的化合物的混合物共聚乙氧基化以得到表示式（I *）和（II *）的化合物的混合物的中间体来制备。 然后通过硫酸化或磷酸化并随后中和将中间体转化成包含式（III）和（IV）的化合物的水性组合物。 含水组合物在20℃下的Brookfield粘度为3000mPa·s以下（在20℃下用纺锤2和20rpm测量）是显着的，并且适用于乳液聚合的乳化剂。

    Use of nonionic surfactants as emulsifiers for emulsion polymerization
    10.
    发明申请
    Use of nonionic surfactants as emulsifiers for emulsion polymerization 审中-公开
    使用非离子表面活性剂作乳液聚合乳化剂

    公开(公告)号：US20090292072A1

    公开(公告)日：2009-11-26

    申请号：US12469226

    申请日：2009-05-20

    申请人： Ronald Klagge ,  Markus Scherer ,  Thomas Schliwka ,  Katharina Homberg ,  Uwe Held ,  Thomas Mausberg

    发明人： Ronald Klagge ,  Markus Scherer ,  Thomas Schliwka ,  Katharina Homberg ,  Uwe Held ,  Thomas Mausberg

    IPC分类号： C08F2/22

    CPC分类号： B01F17/0021 ,  B01F17/0028 ,  C08F2/26

    摘要： Disclosed is the use of nonionic surfactants as emulsifiers for emulsion polymerization, one or more nonionic surfactants being selected from the group consisting of (a) addition products of from 1 to 40 mol of ethylene oxide and/or propylene oxide per mole onto allyl alcohol, and (b) addition products of from 1 to 40 mol of ethylene oxide and/or propylene oxide per mole onto allyl alcohol, where the OH group of these addition products is terminally capped in the sense that it is replaced by a group OR, where R is an alkyl group having 1 to 20 carbon atoms which may be saturated or unsaturated, straight-chain or branched.

    摘要翻译： 公开了使用非离子表面活性剂作为乳液聚合的乳化剂，一种或多种非离子表面活性剂选自（a）每摩尔1至40摩尔环氧乙烷和/或环氧丙烷加成产物至烯丙醇， 和（b）每摩尔1至40摩尔环氧乙烷和/或环氧丙烷加成的烯丙醇，其中这些加成产物的OH基团被末端封端，其被替换为OR，其中 R是具有1至20个碳原子的烷基，其可以是饱和或不饱和的，直链或支链的。