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公开(公告)号:US20130248754A1
公开(公告)日:2013-09-26
申请号:US13824572
申请日:2011-05-13
申请人: Noritsugu Sakuma , Hidefumi Kishimoto , Akira Kato , Tetsuya Shoji , Dominique Givord , Nora Dempsey , Thomas George Woodcock , Oliver Gutfleisch , Gino Hrkac , Thomas Schrefl
发明人: Noritsugu Sakuma , Hidefumi Kishimoto , Akira Kato , Tetsuya Shoji , Dominique Givord , Nora Dempsey , Thomas George Woodcock , Oliver Gutfleisch , Gino Hrkac , Thomas Schrefl
CPC分类号: H01F41/00 , B22F2003/248 , B22F2998/00 , B22F2998/10 , B22F2999/00 , C22C38/002 , C22C38/005 , C22C38/06 , C22C38/16 , C22C2202/02 , H01F1/01 , H01F1/0576 , H01F1/0577 , H01F10/126 , H01F41/005 , H01F41/0273 , H01F41/32 , B22F9/08 , B22F1/0055 , B22F3/10 , B22F3/24 , B22F1/0044 , B22F3/105
摘要: The method of the present invention produces a rare earth magnet, which is represented by a neodymium magnet (Nd2Fe14B) and neodymium magnet films with applications in micro-systems, by using a heat treatment method capable of enhancing the magnetic characteristics, particularly the magnetic coercive force. A method for producing a rare earth magnet, comprising: (a) quenching a molten metal having a rare earth magnet composition to form quenched flakes of nanocrystalline structure; sintering the quenched flakes; subjecting the sintered body obtained to an orientation treatment; and applying a heat treatment with pressurization at a temperature sufficiently high to enable diffusion or fluidization of a grain boundary phase and at the same time, low enough to prevent coarsening of the crystal grains. (b) thick films deposited on a substrate, applying an annealing to crystallize with pressurization at a temperature sufficiently high to enable diffusion or fluidization of a grain boundary phase and, at the same time, low enough to prevent coarsening of the crystal grains. Preferably, an element capable of lowering the temperature at which the grain boundary phase can be diffused or fluidized, is added to the rare earth magnet composition.
摘要翻译: 本发明的方法通过使用能够增强磁特性,特别是磁矫顽力的热处理方法来生产由钕磁体(Nd2Fe14B)和钕磁体薄膜表示的稀土磁体,其应用在微系统中 力。 一种稀土类磁体的制造方法,其特征在于,包括:(a)使具有稀土类磁铁组合物的熔融金属淬火,形成骤冷的纳米晶体结构的片状物; 烧结淬火片; 对获得的烧结体进行取向处理; 在足够高的温度下进行加压热处理,使晶界相扩散或流化,同时低至足以防止晶粒粗大化。 (b)沉积在基板上的厚膜,施加退火以在足够高的温度下加压结晶,以使晶界相扩散或流化,同时足够低以防止晶粒粗化。 优选地,能够将能够使晶界相扩散或流化的温度降低的元素添加到稀土类磁体组合物中。
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公开(公告)号:US09520230B2
公开(公告)日:2016-12-13
申请号:US13824572
申请日:2011-05-13
申请人: Noritsugu Sakuma , Hidefumi Kishimoto , Akira Kato , Tetsuya Shoji , Dominique Givord , Nora Dempsey , Thomas George Woodcock , Oliver Gutfleisch , Gino Hrkac , Thomas Schrefl
发明人: Noritsugu Sakuma , Hidefumi Kishimoto , Akira Kato , Tetsuya Shoji , Dominique Givord , Nora Dempsey , Thomas George Woodcock , Oliver Gutfleisch , Gino Hrkac , Thomas Schrefl
IPC分类号: H01F41/00 , H01F41/02 , H01F41/32 , C22C38/00 , C22C38/06 , C22C38/16 , H01F1/01 , H01F1/057 , H01F10/12 , B22F3/24
CPC分类号: H01F41/00 , B22F2003/248 , B22F2998/00 , B22F2998/10 , B22F2999/00 , C22C38/002 , C22C38/005 , C22C38/06 , C22C38/16 , C22C2202/02 , H01F1/01 , H01F1/0576 , H01F1/0577 , H01F10/126 , H01F41/005 , H01F41/0273 , H01F41/32 , B22F9/08 , B22F1/0055 , B22F3/10 , B22F3/24 , B22F1/0044 , B22F3/105
摘要: A rare earth magnet, which is represented by a neodymium magnet (Nd2Fe14B) and neodymium magnet films with applications in micro-systems. A method for producing a rare earth magnet, comprising: (a) quenching a molten metal having a rare earth magnet composition to form quenched flakes of nanocrystalline structure; sintering the quenched flakes; subjecting the sintered body obtained to an orientation treatment; and applying a heat treatment with pressurization at a temperature sufficiently high to enable diffusion or fluidization of a grain boundary phase and at the same time, low enough to prevent coarsening of the crystal grains, (b) thick films deposited on a substrate, applying an annealing to crystallize with pressurization at a temperature sufficiently high to enable diffusion or fluidization of a grain boundary phase and, at the same time, low enough to prevent coarsening of the crystal grains.
摘要翻译: 一种稀土磁体,由钕磁铁(Nd2Fe14B)和钕磁体薄膜组成,应用于微系统。 一种稀土类磁体的制造方法,其特征在于,包括:(a)使具有稀土类磁铁组合物的熔融金属淬火,形成骤冷的纳米晶体结构的片状物; 烧结淬火片; 对获得的烧结体进行取向处理; 并且在足够高的温度下进行加压热处理以使晶界相扩散或流化,同时低至足以防止晶粒粗大化,(b)沉积在基板上的厚膜, 在足够高的温度下通过加压结晶退火以使晶界相扩散或流化,同时足够低以防止晶粒粗化。
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公开(公告)号:US08636853B2
公开(公告)日:2014-01-28
申请号:US12532856
申请日:2008-03-26
申请人: Tetsuya Shoji , Akira Kato , Toshiji Mukai , Hidetoshi Somekawa
发明人: Tetsuya Shoji , Akira Kato , Toshiji Mukai , Hidetoshi Somekawa
IPC分类号: C22C23/06
摘要: An Mg alloy provided with high strength and high ductility by matching the strength and ductility in tensile deformation and compressive deformation at the same levels is provided. The Mg alloy of the present invention is characterized by having a chemical composition consisting of Y: 0.1 to 1.5 at % and a balance of Mg and unavoidable impurities and having a microstructure with high Y regions with Y concentrations higher than an average Y concentration distributed at nanometer order sizes and intervals. The present invention further provides an Mg alloy characterized by having a chemical composition consisting of Y: more than 0.1 at % and a valance of Mg and unavoidable impurities, having a microstructure with high Y regions with Y concentrations higher than an average Y concentration distributed at nanometer order sizes and intervals and having an average recrystallized grain size within the range satisfying the following formula 1: −0.87c+1.10
摘要翻译: 提供了通过将拉伸变形和压缩变形的强度和延展性在相同水平上匹配而具有高强度和高延展性的Mg合金。 本发明的Mg合金的特征在于,具有由以下组成的化学组成:Y:0.1〜1.5原子%,余量为Mg和不可避免的杂质,并且具有Y浓度高于分布在 纳米尺寸和间隔。 本发明还提供一种Mg合金,其特征在于具有以下组成的化学组成:Y:大于0.1原子%,Mg和不可避免的杂质,具有Y浓度高于分布在 纳米级尺寸和间隔,其平均重结晶晶粒尺寸在满足下列公式1的范围内:-0.87c + 1.10
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公开(公告)号:US20110135532A1
公开(公告)日:2011-06-09
申请号:US13055214
申请日:2009-07-22
申请人: Toshiji Mukai , Hidetoshi Somekawa , Tetsuya Shoji , Akira Kato
发明人: Toshiji Mukai , Hidetoshi Somekawa , Tetsuya Shoji , Akira Kato
摘要: The present invention has as its object to provide an Mg-based alloy cold worked member which can remarkably lower the load weight required for cold plastic working and enables practical usage of the same. The present invention is an Mg-based alloy cold worked member obtained by cold working an Mg-based alloy to form it into a predetermined shape, characterized by having a microstructure which includes crystal grains divided and made finer by cold working.
摘要翻译: 本发明的目的是提供一种能够显着降低冷塑性加工所需的负荷重量的Mg系合金冷加工部件,能够实际应用。 本发明是一种通过将Mg基合金冷加工成为预定形状而获得的Mg基合金冷加工构件,其特征在于,具有通过冷加工分割成细晶的微结构。
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公开(公告)号:US20100215851A1
公开(公告)日:2010-08-26
申请号:US12596994
申请日:2007-04-25
申请人: Tetsuya Shoji , Naoki Nakamura , Akira Kato , Shinpei Yamamoto , Mikio Takano , Teruo Ono
发明人: Tetsuya Shoji , Naoki Nakamura , Akira Kato , Shinpei Yamamoto , Mikio Takano , Teruo Ono
IPC分类号: B05D7/00
CPC分类号: B22F1/025 , B22F1/0018 , B22F9/24 , B22F9/305 , B82Y30/00
摘要: A method of producing core/shell composite nano-particles exhibiting superior characteristics, by using as cores nano-particles heat treated in advance so as to give them a specific crystal structure in a state using a barrier layer to prevent sintering and forming shells on their surface, which eliminates hindrances to the shell forming reaction due to the phase transfer catalyst or other strongly sticky dispersant, is provided. A method of producing core/shell composite nano-particles comprising nano-sized core particles covered by shells, the method comprising dispersing core particles heat treated in advance to give them a crystal structure expressing the necessary characteristics in a first organic solvent by a first dispersant to prepare a first solution, adding a polar solvent to peel off the first dispersant from the core particles and making the nano-particles agglomerate to recover them, making the recovered core particles disperse in a second organic solvent by a second dispersant to form a second solution, and adding a precursor of the shells to the second solution and forming shells on the surfaces of the core particles.
摘要翻译: 通过使用预先热处理的核心纳米粒子来制造具有优异特性的核/壳复合纳米粒子的方法,以便在使用阻挡层的状态下给予其特定的晶体结构,以防止烧结和形成壳体 表面,其消除了由于相转移催化剂或其它强粘性分散剂而导致的壳形成反应的障碍。 一种制造核壳复合纳米颗粒的方法,其包括由壳覆盖的纳米尺寸的核心颗粒,该方法包括将预先热处理的芯颗粒分散在第一有机溶剂中,通过第一分散剂给予它们表达必要特性的晶体结构 制备第一溶液,加入极性溶剂以从芯颗粒上剥离第一分散剂并使纳米颗粒凝聚回收,使回收的芯颗粒通过第二分散剂分散在第二有机溶剂中以形成第二溶剂 溶液,并将壳的前体添加到第二溶液中并在芯颗粒的表面上形成壳。
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公开(公告)号:US20100163141A1
公开(公告)日:2010-07-01
申请号:US12532856
申请日:2008-03-26
申请人: Tetsuya Shoji , Akira Kato , Toshiji Mukai , Hidetoshi Somekawa
发明人: Tetsuya Shoji , Akira Kato , Toshiji Mukai , Hidetoshi Somekawa
摘要: An Mg alloy provided with high strength and high ductility by matching the strength and ductility in tensile deformation and compressive deformation at the same levels is provided. The Mg alloy of the present invention is characterized by having a chemical composition consisting of Y: 0.1 to 1.5 at % and a balance of Mg and unavoidable impurities and having a microstructure with high Y regions with Y concentrations higher than an average Y concentration distributed at nanometer order sizes and intervals. The present invention further provides an Mg alloy characterized by having a chemical composition consisting of Y: more than 0.1 at % and a valance of Mg and unavoidable impurities, having a microstructure with high Y regions with Y concentrations higher than an average Y concentration distributed at nanometer order sizes and intervals and having an average recrystallized grain size within the range satisfying the following formula 1: −0.87c+1.10
摘要翻译: 提供了通过将拉伸变形和压缩变形的强度和延展性在相同水平上匹配而具有高强度和高延展性的Mg合金。 本发明的Mg合金的特征在于,具有由以下组成的化学组成:Y:0.1〜1.5原子%,余量为Mg和不可避免的杂质,并且具有Y浓度高于分布在 纳米尺寸和间隔。 本发明还提供一种Mg合金,其特征在于具有以下组成的化学组成:Y:大于0.1原子%,Mg和不可避免的杂质的含量,具有Y浓度高于分布在 纳米级尺寸和间隔,其平均重结晶晶粒尺寸在满足下列公式1的范围内:-0.87c + 1.10
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公开(公告)号:US09523141B2
公开(公告)日:2016-12-20
申请号:US14356502
申请日:2012-11-06
申请人: Kota Washio , Akira Kato , Toshiji Mukai , Alok Singh , Hidetoshi Somekawa
发明人: Kota Washio , Akira Kato , Toshiji Mukai , Alok Singh , Hidetoshi Somekawa
摘要: Provided is an Mg alloy and a method for producing same able to demonstrate high strength without requiring an expensive rare earth element (RE). The high-strength Mg alloy containing Ca and Zn within a solid solubility limit and the remainder having a chemical composition comprising Mg and unavoidable impurities is characterized in comprising equiaxial crystal particles, there being a segregated area of Ca and Zn along the (c) axis of a Mg hexagonal lattice within the crystal particle, and having a structure in which the segregated area is lined up by Mg3 atomic spacing in the (a) axis of the Mg hexagonal lattice. The method for producing the high-strength Mg alloy is characterized in that Ca and Zn are added to Mg in a compounding amount corresponding to the above composition and, after homogenization heat treating an ingot formed by dissolution and casting, the above structure is formed by subjecting the ingot to hot processing.
摘要翻译: 提供一种Mg合金及其制造方法,能够显示高强度而不需要昂贵的稀土元素(RE)。 含有固溶度极限中的Ca和Zn的高强度Mg合金和其中包含Mg和不可避免的杂质的化学组成的其余部分的特征在于包括等轴晶体颗粒,沿着(c)轴具有Ca和Zn的偏析面积 的晶体粒子内的Mg六角形晶格,并且具有在Mg六方晶格的(a)轴上偏析区域被Mg 3原子间隔排列的结构。 高强度Mg合金的制造方法的特征在于,以与上述组成相对应的配合量将Mg和Ca添加到Mg中,在通过溶解和铸造形成的锭均质化热处理后,上述结构通过 对锭进行热加工。
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公开(公告)号:US08792308B2
公开(公告)日:2014-07-29
申请号:US13634403
申请日:2011-03-23
申请人: Akira Kato , Takushi Hagita , Tadashi Yasuoka
发明人: Akira Kato , Takushi Hagita , Tadashi Yasuoka
IPC分类号: G04C11/02
摘要: Provided is a radio-controlled watch capable of performing leap second correction even when information on a leap second is not received from a satellite. Provided is a radio-controlled watch that adjusts time by receiving a signal containing time information from a satellite, the radio-controlled watch being configured to: store a leap second correction value to be used for leap second correction with respect to the time information; display a numerical value corresponding to the leap second correction value; receive an instruction operation of changing the leap second correction value from a user in a state in which the numerical value is displayed; and change the leap second correction value in response to the received instruction operation.
摘要翻译: 提供了即使在没有从卫星接收到关于闰秒的信息的情况下也能够执行闰秒校正的无线电控制的手表。 提供一种无线电控制手表,其通过从卫星接收到包含时间信息的信号来调整时间,该无线电控制手表被配置为:存储用于相对于时间信息的闰秒校正的闰秒校正值; 显示对应于闰秒校正值的数值; 在显示数值的状态下接收从用户改变闰秒校正值的指令操作; 并且响应于接收到的指令操作来改变闰秒校正值。
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公开(公告)号:US08653067B2
公开(公告)日:2014-02-18
申请号:US12597470
申请日:2008-04-23
申请人: Naotake Kobayashi , Kazuo Ueda , Naohiro Itoh , Gaku Sakaguchi , Akira Kato , Akihiro Hori , Hidekazu Haraguchi , Ken Yasui
发明人: Naotake Kobayashi , Kazuo Ueda , Naohiro Itoh , Gaku Sakaguchi , Akira Kato , Akihiro Hori , Hidekazu Haraguchi , Ken Yasui
IPC分类号: A61K31/554 , A61K31/541 , A61K31/426 , A61K31/506 , C07D417/02 , C07D279/06 , C07D277/18 , C07D239/02
CPC分类号: C07D471/04 , A61K9/0019 , A61K9/1623 , A61K9/2018 , A61K31/426 , A61K31/506 , A61K31/535 , A61K31/54 , A61K31/541 , A61K31/554 , C07D239/14 , C07D265/08 , C07D277/18 , C07D279/06 , C07D281/02 , C07D285/36 , C07D295/155 , C07D295/192 , C07D405/04 , C07D417/04 , C07D417/10 , C07D417/12 , A61K2300/00
摘要: A pharmaceutical composition for treating Alzheimer's disease containing a compound represented by the general formula (I); wherein ring A is an optionally substituted carbocyclic group or an optionally substituted heterocyclic group; E is lower alkylene, etc.; X is S, O, or NR1; R1 is a hydrogen atom or lower alkyl; R2a, R2b, R3a, R3b, R4a and R4b are each independently a hydrogen atom, halogen, hydroxy, etc.; n and m are each independently an integer of 0 to 3; n+m is an integer of 1 to 3; and R5 is a hydrogen atom, optionally substituted lower alkyl, etc.; its pharmaceutically acceptable salt, or a solvate thereof as an active ingredient.
摘要翻译: 一种用于治疗含有由通式(I)表示的化合物的阿尔茨海默病的药物组合物; 其中环A是任选取代的碳环基团或任选取代的杂环基团; E为低级亚烷基等; X是S,O或NR1; R1是氢原子或低级烷基; R2a,R2b,R3a,R3b,R4a和R4b各自独立地为氢原子,卤素,羟基等; n和m各自独立地为0〜3的整数, n + m为1〜3的整数, R5为氢原子,任意取代的低级烷基等; 其药学上可接受的盐或其溶剂合物作为活性成分。
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公开(公告)号:US20140016440A1
公开(公告)日:2014-01-16
申请号:US14008403
申请日:2012-03-13
申请人: Akira Kato , Takushi Hagita
发明人: Akira Kato , Takushi Hagita
IPC分类号: G04R20/04
摘要: Provided is a radio-controlled wristwatch that receives a radio wave including day-related information from a satellite within a global positioning system, in which a cycle number of the day-related information is correctly updated even in a case where a power supply voltage drops. A radio-wave wristwatch (1) according to the present invention includes: reception means (11) for receiving a radio wave from a satellite and extracting day-related information therefrom; timekeeping-circuit halting means for halting an operation of a timekeeping circuit based on a power supply voltage; timekeeping-circuit halt detection means for detecting that the operation of the timekeeping circuit (13) has been halted by the timekeeping-circuit halting means; a nonvolatile memory (23) for storing the day-related information and a cycle number of the day-related information; and cycle-number updating means for updating, when the timekeeping-circuit halt detection means detects that the operation of the timekeeping circuit has been halted, the cycle number of the day-related information based on a comparison result between the day-related information extracted by the reception means (11) and the day-related information stored in the nonvolatile memory (23).
摘要翻译: 提供一种无线电控制的手表,其在全球定位系统内接收包括来自卫星的日常相关信息的无线电波,其中即使在电源电压下降的情况下,日相关信息的周期数也被正确更新 。 根据本发明的无线电波手表(1)包括:接收装置(11),用于从卫星接收无线电波并从其中提取日期信息; 计时电路停止装置,用于基于电源电压停止计时电路的操作; 计时电路停止检测装置,用于检测计时电路(13)的运行已经被计时电路停止装置停止; 非易失性存储器(23),用于存储日期相关信息和日期相关信息的周期数; 以及循环次数更新装置,用于当计时电路停止检测装置检测到计时电路的操作已经停止时,更新基于提取的日间相关信息之间的比较结果的日期相关信息的循环次数 通过接收装置(11)和存储在非易失性存储器(23)中的日期相关信息。
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