Method for carrying out polycondensation reactions
    1.
    发明授权
    Method for carrying out polycondensation reactions 有权
    进行缩聚反应的方法

    公开(公告)号:US06187898B1

    公开(公告)日:2001-02-13

    申请号:US09367457

    申请日:1999-08-13

    IPC分类号: C08G6904

    CPC分类号: C08G73/0611

    摘要: The invention relates to a method for carrying out polycondensation reactions, according to which the polycondensation of a monomeric starting material is carried out with external supply of heat in a reactor combination which has at least two stages and is composed of a pre-reactor and a high-viscosity reactor, where the low-molecular-weight elimination products produced are removed by evaporation. In the pre-reactor, the reaction product is concentrated to give a high-viscosity preliminary product. The high-viscosity preliminary product is then fed to the high-viscosity reactor, in which it reacts to completion with simultaneous introduction of thermal and mechanical energy and with a residence time of from 20 s to 60 min to give a polycondensation product.

    摘要翻译: 本发明涉及一种进行缩聚反应的方法,根据该方法,单体原料的缩聚是在具有至少两个阶段的反应器组合中进行外部供热,并由预反应器和 通过蒸发除去生成的低分子量消除产物的高粘度反应器。 在预反应器中,将反应产物浓缩,得到高粘度的初步产物。 然后将高粘度的初步产物进料到高粘度反应器中,其中反应完成,同时引入热和机械能,停留时间为20秒至60分钟,得到缩聚产物。